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1260 Infinity
Agilent Technologies 1260 Infinity Manuals
Manuals and User Guides for Agilent Technologies 1260 Infinity. We have
21
Agilent Technologies 1260 Infinity manuals available for free PDF download: User Manual, Service Manual, Quick Start Manual, Operator's Quick Manual
Agilent Technologies 1260 Infinity User Manual (282 pages)
Infinity Diode Array and Multiple Wavelength Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 10.16 MB
Table of Contents
Table of Contents
5
1 Introduction
9
Introduction to the Detector
10
Optical System
11
Optical System
12
Early Maintenance Feedback (EMF)
14
Instrument Layout
15
Electrical Connections
16
Electrical Connections
17
Interfaces
18
Interfaces
19
Interfaces Overview
20
Setting the 8-Bit Configuration Switch
24
Setting the 8-Bit Configuration Switch
25
Communication Settings for RS-232C
28
Special Settings
30
2 Site Requirements and Specifications
33
Site Requirements
34
Physical Specifications
37
Performance Specifications
38
Specifications
38
Specification Conditions
41
3 Installing the Module
43
Unpacking the Detector
44
Damaged Packaging
44
Delivery Checklist
45
Optimizing the Stack Configuration
46
Two Stack Configuration
48
Installing the Detector
50
Flow Connections to the Detector
53
Setting up the LAN Access
56
4 LAN Configuration
57
What You Have to Do First
58
TCP/IP Parameter Configuration
59
Configuration Switch
60
Initialization Mode Selection
61
Link Configuration Selection
65
Automatic Configuration with Bootp
66
About Agilent Bootp Service
66
How Bootp Service Works
67
Situation: Cannot Establish LAN Communication
67
Installation of Bootp Service
68
Two Methods to Determine the MAC Address
70
Assigning IP Addresses Using the Agilent Bootp Service
71
Changing the IP Address of an Instrument Using the Agilent Bootp Service
74
Storing the Settings Permanently with Bootp
76
Manual Configuration
77
With Telnet
78
With the Instant Pilot (G4208A)
82
5 Using the Detector
83
Setting up an Analysis
84
Before Using the System
84
Requirements and Conditions
86
Optimization of the System
89
Preparing the HPLC System
90
Running the Sample and Verifying the Results
99
Special Settings of the Detector
100
Control Settings
100
Configuration Settings
101
Online Spectra (DAD Only)
102
Run Recovery Settings
103
Automated Run Recovery in Case of Temporary Communication Failures
104
Manual Run Recovery in Case of Permanent Communication Failures
106
Analog Output Settings
107
Spectrum Settings (DAD Only)
108
Peakwidth Settings
110
Slit Settings
112
Margin for Negative Absorbance Settings
113
Optimizing the Detector
113
Special Setups with Multiple DAD-Mwds
114
Two Detectors of same Type (E.g. G1315C/D and G1315C/D)
114
Two Detectors of Similar Type (E.g. G1315C/D and G1315A/B)
114
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Agilent Technologies 1260 Infinity User Manual (252 pages)
Binary Pump
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 3.98 MB
Table of Contents
Table of Contents
5
1 Introduction to the Binary Pump
9
Instrument and Operation
10
Introduction to the Pump
10
Principle of Operation
11
Overview of the Hydraulic Path
13
Leak and Waste Handling
18
2 Site Requirements and Specifications
21
Site Requirements
22
Physical Specifications
25
Performance Specifications
26
3 Installing the Pump
29
Unpacking the Binary Pump
30
Optimizing the Stack Configuration
33
Installation Information on Leak and Waste Handling
41
Installing the Binary Pump
45
Flow Connections with Solvent Selection Valve
48
Flow Connections Without Solvent Selection Valve
51
Priming the System
54
Initial Priming
54
Regular Priming
56
Changing Solvents
57
4 Using the Pump
59
Leak and Waste Handling
60
Hints for Successful Use of the Binary Pump
61
Setting up the Pump with the G4208A Instant Pilot
62
Setting up the Agilent 1260 Infinity Binary Pump G1312B with the Instrument Control Interface
63
Overview
63
Setup of Basic Pump Parameters
64
Pump Control
65
Auxiliary Pump Parameters
66
Data Curves
67
Bottle Filling
67
Solvent Information
69
Algae Growth in HPLC Systems
74
How to Prevent And/Or Reduce the Algae Problem
75
Prevent Blocking of Solvent Filters
76
Checking the Solvent Filters
77
Cleaning the Solvent Filters
77
5 Optimizing Performance
79
When to Use a Vacuum Degasser
80
Operational Hints for the Vacuum Degasser
80
When to Use the Active Seal Wash Option
81
When to Use Alternative Seals
82
When to Use the Low Volume Mixer
83
When to Remove Damper and Mixer
84
Convert the Binary Pump to Low Delay Volume Mode
85
How to Optimize the Compressibility Compensation Setting
87
Solvent Compressibility Calibration
87
Optimization of Legacy Compressibility Settings
88
6 Troubleshooting and Diagnostics
91
Overview of the Module's Indicators and Test Functions
92
Status Indicators
94
Power Supply Indicator
94
Module Status Indicator
95
User Interfaces
96
Agilent Lab Advisor Software
97
Agilent Technologies 1260 Infinity User Manual (244 pages)
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 7.95 MB
Table of Contents
Table of Contents
5
Introduction to the Variable Wavelength Detector
9
Introduction to the Detector
10
Optical System Overview
11
System Overview
16
2 Site Requirements and Specifications
19
Site Requirements
20
Physical Specifications
23
Performance Specifications G1314D
24
Performance Specifications G1314E
27
Performance Specifications G1314F
30
3 Installing the Detector
33
Damaged Packaging
34
Unpacking the Detector
34
Delivery Checklist
35
Detector Accessory Kit Contents
35
Optimizing the Stack Configuration
36
One Stack Configuration
37
Two Stack Configuration
41
Installation Information on Leak and Waste Handling
45
Installing the Detector
49
Flow Connections to the Detector
52
4 Using the Detector
55
Leak and Waste Handling
56
Before Using the System
57
Setting up an Analysis
57
Requirements and Conditions
59
Optimization of the System
61
Preparing the HPLC System
61
Running the Sample and Verifying the Results
70
Control Settings
71
Special Settings of the Detector
71
Configuration Settings
72
Online Spectra
73
Scanning with the VWD
74
Analog Output Settings
75
Special Setpoints
76
Run Recovery (G1314E)
80
How to Optimize the Detector
83
Optimizing the Detector Performance
84
Match the Flow Cell to the Column
85
Set the Detector Parameters
88
6 Troubleshooting and Diagnostics
89
Overview of the Detector's Indicators and Test Functions
90
Power Supply Indicator
91
Status Indicators
91
Module Status Indicator
92
Available Tests Versus Interfaces
93
Agilent Lab Advisor Software
94
7 Error Information
95
What Are Error Messages
97
General Error Messages
98
Shutdown
98
Timeout
98
Remote Timeout
99
Leak
100
Lost CAN Partner
100
Leak Sensor Open
101
Leak Sensor Short
101
Compensation Sensor Open
102
Compensation Sensor Short
102
Fan Failed
103
Open Cover
103
Detector Error Messages
104
UV Lamp: no Current
104
Ignition Failed
105
UV Lamp: no Voltage
105
No Heater Current
106
Wavelength Calibration Setting Failed
106
Wavelength Holmium Check Failed
107
Grating or Filter Motor Errors
108
Cutoff Filter Doesn't Decrease the Light Intensity at 250 Nm
109
Wavelength Test Failed
109
ADC Hardware Error
110
Illegal Temperature Value from Sensor on Main Board
110
Heater at Fan Assembly Failed
111
Illegal Temperature Value from Sensor at Air Inlet
111
Heater Power at Limit
112
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Agilent Technologies 1260 Infinity User Manual (234 pages)
Fluorescence Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 6.53 MB
Table of Contents
Table of Contents
5
1 Introduction to the Fluorescence Detector
9
Introduction to the Detector
10
How the Detector Operates
11
Raman Effect
14
Optical Unit
15
Analytical Information from Primary Data
23
Early Maintenance Feedback
28
Instrument Layout
29
Electrical Connections
30
Interfaces
32
Setting the 8-Bit Configuration Switch
38
2 Site Requirements and Specifications
45
Site Requirements
46
Physical Specifications
49
Performance Specifications
50
3 Installing the Module
53
Unpacking the Module
54
Optimizing the Stack Configuration
56
One Stack Configuration
57
Two Stack Configuration
59
Installing the Module
61
Flow Connections to the Module
64
Installing the Module Flow Connections to the Module
64
4 Using the Fluorescence Detector
69
Before You Start
70
Getting Started and Checkout
71
Starting Your Detector
71
Setting the Chromatographic Conditions
72
Observe the Maxima Via the Isoabsorbance Plot
74
Method Development
75
Step 1: Check the LC System for Impurities
76
Step 2: Optimize Limits of Detection and Selectivity
78
Step 3: Set up Routine Methods
89
Example: Optimization for Multiple Compounds
93
5 Optimizing the Detector
103
Optimization Overview
104
Design Features Help Optimization
106
Check Performance before You Start
106
Finding the Best Wavelengths
107
A Real Example
108
Finding the Best Signal Amplification
109
FLD Scaling Range and Operating Conditions
110
Changing the Xenon Flash Lamp Frequency
115
Lamp Life Savings
116
Selecting the Best Response Time
117
Reducing Stray Light
120
6 Troubleshooting and Diagnostics
123
Overview of the Module's Indicators and Test Functions
124
Status Indicators
125
Power Supply Indicator
125
Module Status Indicator
126
User Interfaces
127
Agilent Lab Advisor Software
128
Agilent Technologies 1260 Infinity User Manual (190 pages)
Brand:
Agilent Technologies
| Category:
Analytical Instruments
| Size: 2.38 MB
Table of Contents
Table of Contents
5
Introduction to the 1260 Infinity MDS
9
Introduction
10
Instrument Overview
12
The 1260 Infinity MDS Refractive Index Detector
19
The 1260 Infinity MDS Viscometer
21
The 1260 Infinity MDS Dual Angle Light Scattering Detector
24
The 1260 Infinity MDS Dynamic Light Scattering Detector
25
Site Requirements and Specifications
27
Pre-Installation Requirements
28
Site Requirements
29
Physical Specifications
33
Performance Specifications
34
3 Installation
37
Unpacking the Module
38
Installing the Instrument
42
The MDS with the Agilent 1200 Infinity Series
42
Dual Stack Configuration
43
Connection to a 3Rd-Party LC System
44
Installing the G7800 MDS
45
Powering the Instrument on or off
46
Detector Output Channel Assignment
47
Fluid Connections
49
Single Detector System
50
Dual Detector System
51
Triple Detector System
53
Other Connections
54
Analog Inputs
55
Analog Outputs
55
USB Port
55
Auxiliary I/O Port
56
Serial RS232 Port
56
Service Port and Switch
57
Agilent Technologies
59
Controlling the 1260 Infinity MDS
59
Controlling the Instrument
60
The Keypad
61
The Instrument Display
64
The Start-Up Screen
64
The Home Screen
65
The Menu System
69
The RI Detector Menus
76
The RI Detector Menu Screen
77
The RI Parameters Menu Screen
79
The Viscometer Menus
82
The VS Detector Menu Screen
84
The VS Parameters Menu Screen
86
The LS Detector Menus
87
The LS and LS/DLS Detector Menu Screen
88
The LS Parameters Menu Screen
89
The Analog Input Menus
90
The Analog Input Menu Screen
91
The Analog Input Parameters Menu Screen
92
The System Options Menus
93
The System Options Menu Screen
94
The System Options Parameters Menu Screen
95
Multi-Detector Suite (Mds)
97
Operating the 1260 Infinity Multi-Detector Suite (MDS)
97
Preparing the 1260 Infinity Multi Detector Suite
98
Using the Instrument
98
Preparing the RI Detector
99
Preparing the Viscometer
99
Preparing the LS and DLS Detector
100
Mobile Phase Priming
101
Pumping Systems
101
Solvent Information
102
Agilent Technologies 1260 Infinity User Manual (200 pages)
Nanoflow Pump
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 4.81 MB
Table of Contents
Table of Contents
3
1 Introduction to the 1260 Infinity Nanoflow Pump
7
Introduction to the Pump
8
Early Maintenance Feetback
16
Instrument Layout
17
Electrical Connections
18
Interfaces
20
Setting the 8-Bit Configuration Switch (On-Board LAN)
26
2 Site Requirements and Specifications
33
Site Requirements
34
Physical Specifications
37
Performance Specifications
38
3 Installing the Module
41
Unpacking the Module
42
Delivery Checklist
42
Nanoflow Pump Accessory Kit
43
Optimizing the Stack Configuration
44
One Stack Configuration
44
Two Stack Configuration
47
Installing the Pump
49
Connecting Modules and Control Software
52
Connecting Modules
52
Connecting a Vacuum Degasser
52
Connecting Control Software And/Or G4208 a Instant Pilot
53
Flow Connections
54
Get the System Ready for the First Injection
58
Manually Priming the Solvent Channels
58
Priming Your System with the Pump
59
4 Using the Pump
61
Hints for Successfully Using the Pump
62
Solvent Information
64
Algae Growth in HPLC Systems
65
How to Prevent And/Or Reduce the Algae Problem
66
Checkout Procedure for a G2229A Nano LC System
67
Method Parameters
68
Test Results and Evaluation
70
5 Optimizing Performance
71
Hints for the Micro Vacuum Degasser
72
Choosing the Right Pump Seals
73
How to Choose the Primary Flow
74
The Standard Filter
75
How to Optimize the Compressibility Compensation Setting
76
6 Troubleshooting and Diagnostics
79
Overview of the Module's Indicators and Test Functions
80
Status Indicators
82
Power Supply Indicator
82
Module Status Indicator
83
User Interfaces
84
Agilent Lab Advisor Software
85
7 Error Information
87
What Are Error Messages
89
General Error Messages
90
Timeout
90
Shut-Down
90
Remote Timeout
91
Synchronization Lost
91
Leak Sensor Short
92
Leak Sensor Open
92
Compensation Sensor Open
93
Compensation Sensor Short
93
Fan Failed
94
Leak
94
Module Error Messages
95
Zero Solvent Counter
95
Pressure above Upper Limit
95
Pressure below Lower Limit
96
Pressure Signal Missing
96
Valve Failed
97
Missing Pressure Reading
98
Pump Configuration
98
Valve Fuse
99
Inlet-Valve Fuse
99
Temperature out of Range
100
Temperature Limit Exceeded
100
Motor-Drive Power
101
Encoder Missing
102
Inlet-Valve Missing
102
Electro-Magnetic-Proportional-Valve (EMPV) Missing
103
Flow Sensor Missing
103
Leak Sensor Missing
103
Servo Restart Failed
104
Pump Head Missing
105
Index Limit
105
Index Adjustment
106
Index Missing
106
Stroke Length
107
Initialization Failed
107
Wait Timeout
108
Electronic Fuse of SSV
108
Agilent Technologies 1260 Infinity User Manual (200 pages)
Variable Wavelength Detector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 4.22 MB
Table of Contents
Table of Contents
5
1 Introduction to the Variable Wavelength Detector
12
Introduction to the Detector
12
Optical System Overview
13
Flow Cell
14
Electrical Connections
17
Serial Number Information
19
Instrument Layout
20
Early Maintenance Feedback (EMF)
21
EMF Counter
21
Using the EMF Counters
21
Interfaces
23
Overview Interfaces
25
RS-232 Cable
26
Setting the 8-Bit Configuration Switch
29
Setting the 8-Bit Configuration Switch (On-Board LAN)
29
Setting the 8-Bit Configuration Switch (Without On-Board LAN)
31
Communication Settings for RS-232C
32
Special Settings
34
2 Site Requirements and Specifications
37
Site Requirements
38
Power Consideration
38
Power Cords
39
Bench Space
40
Environment
40
Physical Specifications
42
Performance Specifications
43
Specification Conditions
45
3 Installing the Detector
47
Unpacking the Detector
48
Delivery Checklist
49
Detector Accessory Kit Contents
49
Optimizing the Stack Configuration
50
One Stack Configuration
50
Two Stack Configuration
53
Installing the Detector
55
Flow Connections to the Detector
58
4 Using the Detector
62
Setting up an Analysis
62
Before Using the System
62
Requirements and Conditions
64
Optimization of the System
66
Preparing the HPLC System
67
Running the Sample and Verifying the Results
76
Special Settings of the Detector
77
Control Settings
77
Online Spectra
78
Scanning with the VWD
79
Analog Output Settings
81
Special Setpoints
82
Peakwidth Settings
83
Optimizing the Detector
85
Agilent Technologies 1260 Infinity User Manual (194 pages)
Isocratic Pump and Quaternary Pump
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 6.03 MB
Table of Contents
Table of Contents
3
1 Introduction
7
Introduction to the Pump
8
Overview of the Hydraulic Path
10
Early Maintenance Feetback
17
Instrument Layout
18
Electrical Connections
19
Interfaces
21
Setting the 8-Bit Configuration Switch
27
2 Site Requirements and Specifications
35
Site Requirements
36
Physical Specifications
39
Performance Specifications
40
3 Installing the Pump
43
Unpacking the Pump
44
Delivery Checklist
44
Accessory Kit G1311-68755
46
Optimizing the Stack Configuration
47
One Stack Configuration
47
Installing the Pump
50
Connecting Modules and Control Software
53
Connecting Modules
53
Connecting a Vacuum Degasser
54
Connecting Control Software And/Or G4208 a Instant Pilot
55
Flow Connections of the Pump
56
Priming the System
59
Initial Priming
59
Regular Priming
61
Changing Solvents
62
4 Using the Pump
65
Hints for Successful Use of the Isocratic Pump
66
Prevent Blocking of Solvent Filters
68
Algae Growth in HPLC Systems
69
5 Optimiziming Performance
71
When to Use a Vacuum Degasser
72
Operational Hints for the Multi Channel Gradient Valve (MCGV)
73
When to Use the Seal Wash Option
74
Choosing the Right Pump Seals
76
Optimize the Compressibility Compensation Setting
77
6 Troubleshooting and Diagnostics
79
Overview of the Module's Indicators and Test Functions
80
Status Indicators
82
Power Supply Indicator
82
Module Status Indicator
83
User Interfaces
84
Agilent Lab Advisor Software
85
7 Error Information
87
What Are Error Messages
89
General Error Messages
90
Timeout
90
Shut-Down
90
Remote Timeout
91
Synchronization Lost
92
Leak
92
Leak Sensor Open
93
Leak Sensor Short
93
Compensation Sensor Open
94
Compensation Sensor Short
94
Fan Failed
95
Open Cover
95
Module Error Messages
96
Restart Without Cover
96
Solvent Zero Counter
96
Pressure above Upper Limit
97
Pressure below Lower Limit
97
Pressure Signal Missing
98
Missing Pressure Reading
98
Pump Configuration
99
Valve Fuse
99
Inlet-Valve Fuse
100
Valve Failed (MCGV/SSV)
100
Motor-Drive Power
101
Encoder Missing
102
Inlet-Valve Missing
102
Temperature out of Range
103
Temperature Limit Exceeded
103
Servo Restart Failed
104
Pump Head Missing
104
Index Limit
105
Index Adjustment
105
Index Missing
106
Stroke Length
106
Initialization Failed
107
Wait Timeout
107
Degasser: Cannot Read Signal
108
Degasser: Limit Not Reached
109
Agilent Technologies 1260 Infinity User Manual (184 pages)
Preparative
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 3.74 MB
Table of Contents
Table of Contents
3
Installing
3
1 Introduction to the Preparative Pump
7
Interface
7
Introduction to the Preparative Pump
8
Hydraulic Path Overview
9
How Does Compressibility Compensation Work
10
Early Maintenance Feedback (EMF)
11
Instrument Layout
12
The Electronics
13
Electrical Connections
14
Rear View
15
Interfaces
16
REMOTE Connector
17
Shut-Down
19
Special Interface
21
2 Site Requirements and Specifications
23
Site Requirements
23
Performance
23
Physical
23
Site Requirements
24
Physical Specifications
27
Wide-Ranging Capability
27
Performance Specifications
28
Recommended Ph Range
28
3 Installing the Pump
29
Priming
29
Unpacking the Preparative Pump
30
Damaged Packaging
30
Delivery Checklist
30
Solvent Cabinet
31
Basic Kit Contents
32
Gradient Kit Contents
33
Optimizing the Stack Configuration
34
Preparative System
34
Installing the Preparative Pump
36
Voltage Selector
39
Connecting Modules and Control Software
40
Connecting Agilent 1260 Infinity Modules
40
Connecting Control Software Control Module
41
Flow Connections for a Single (Isocratic) Preparative Pump
42
Flow Connections for a Dual (Binary Gradient) Preparative Pump
45
Purge Valve
47
Seal Wash
47
Get the System Ready for the First Analysis
49
4 Using the Preparative Pump
51
Prevent Blocking
51
Hints for Successful Use of the Preparative Pump
52
Solvent Filters
52
Solvent Information
53
Prevent Blocking of Solvent Filters
54
Algae Growth in HPLC Systems
55
How to Prevent And/Or Reduce the Algae Problem
56
Setting up the Pump
57
Setting up the Preparative Pump (Agilent Chemstation)
57
5 Optimizing Performance
65
How to Configure the Seal Wash Function
66
Seal Wash Function
66
How to Optimize the Compressibility Compensation Setting
67
Agilent Technologies 1260 Infinity User Manual (190 pages)
Standard Autosampler
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 3.1 MB
Table of Contents
Table of Contents
5
Introduction to the Autosampler (ALS)
9
Introduction to the Autosampler (ALS)
10
Site Requirements and Specifications
21
Site Requirements
22
Physical Specifications
25
Performance Specifications Standard Autosampler
26
3 Installing the Autosampler
27
Unpacking the Autosampler
28
Optimizing the Stack Configuration
29
Installing the Autosampler
32
Flow Connections
35
Installing the Sample Tray
37
Transporting the Autosampler
38
Using the Autosampler
39
Sample Trays
40
Choice of Vials and Caps
42
5 Optimizing Performance
45
Optimization for Lowest Carry-Over
46
Using the Automated Needle Wash
46
Using an Injector Program
47
General Recommendation to Lowest Carry-Over
48
Fast Injection Cycle and Low Delay Volume
49
Overlapped Injection Mode
49
General Recommendations for Fast Injection Cycle Times
50
Draw and Eject Speed
51
Precise Injection Volume
51
Choice of Rotor Seal
53
6 Troubleshooting and Diagnostics
55
Overview of the Module's Indicators and Test Functions
56
Power Supply Indicator
57
Status Indicators
57
Module Status Indicator
58
Maintenance Functions
59
User Interface
59
Change Needle
60
Change Piston
62
Park Arm
63
Change Gripper
65
Tray Alignment
65
ALS Step Commands
66
Troubleshooting
68
Troubleshooting Guide for the Sample Transport Assembly
70
Intermittent Lock-Ups with or Without Vial in the Gripper Fingers
71
Jittery (Shaky) Movement in X And/Or Theta Axes And/Or When the Needle Goes through the Gripper Arm into the Vial
73
Poor Alignment
75
Agilent Lab Advisor Software
77
7 Error Information
79
What Are Error Messages
81
General Error Messages
82
Shutdown
82
Timeout
82
Lost CAN Partner
83
Remote Timeout
83
Leak
84
Leak Sensor Open
84
Compensation Sensor Open
85
Leak Sensor Short
85
Compensation Sensor Short
86
Fan Failed
86
Open Cover
87
Restart Without Cover
87
Autosampler Error Messages
88
Front Door Open
88
Arm Movement Failed
89
Valve to Bypass Failed
90
Valve to Mainpass Failed
90
Needle up Failed
91
Needle down Failed
92
Missing Vial
93
Initialization Failed
94
Metering Home Failed
95
Motor Temperature
96
Initialization with Vial
97
Safety Flap Missing
97
Vial in Gripper
98
Agilent Technologies 1260 Infinity User Manual (184 pages)
Standard Autosampler
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 5.02 MB
Table of Contents
Table of Contents
5
1 Introduction to the Autosampler
9
Introduction to the Autosampler
10
Sampling Sequence
12
Sampling Unit
15
Transport Assembly
18
Early Maintenance Feedback (EMF)
20
Instrument Layout
21
Electrical Connections
22
Serial Number Information (ALL)
23
Interfaces
24
Overview Interfaces
26
Setting the 8-Bit Configuration Switch (On-Board LAN)
30
Communication Settings for RS-232C
34
Special Settings
36
2 Site Requirements and Specifications
39
Site Requirements
40
Physical Specifications
44
Performance Specifications Standard Autosampler
45
3 Installing the Autosampler
47
Unpacking the Autosampler
48
Optimizing the Stack Configuration
49
Installing the Autosampler
53
Installing the Thermostatted Autosampler
56
Flow Connections
60
Installing the Sample Tray
62
Transporting the Autosampler
63
4 Using the Autosampler Sample Trays
66
List of Compatible Vials and Caps
68
5 Optimizing Performance
71
Optimization for Lowest Carry-Over
72
Using the Automated Needle Wash
72
Using an Injector Program
73
General Recommendation to Lowest Carry-Over
74
Fast Injection Cycle and Low Delay Volume
75
Overlapped Injection Mode
75
General Recommendations for Fast Injection Cycle Times
76
Precise Injection Volume
77
Draw and Eject Speed
77
Choice of Rotor Seal
79
6 Troubleshooting and Diagnostics
81
Overview of the Sampler's Indicators and Test Functions
82
Status Indicators
83
Power Supply Indicator
83
Module Status Indicator
84
Maintenance Functions
85
User Interface
85
Change Needle
86
Change Piston
87
Park Arm
89
Change Gripper
90
Tray Alignment
91
Standard Autosampler Step Commands
92
Troubleshooting
94
Troubleshooting Guide for the Sample Transport Assembly
96
Intermittent Lock-Ups with or Without Vial in the Gripper Fingers
97
Jittery (Shaky) Movement in X And/Or Theta Axes And/Or When the Needle Goes through the Gripper Arm into the Vial
99
Poor Alignment
101
Agilent Lab Advisor Software
103
Agilent Technologies 1260 Infinity User Manual (174 pages)
Refractive Index Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 3.97 MB
Table of Contents
Table of Contents
5
Installing the Refractive Index Detector
3
1 Introduction to the Refractive Index Detector
9
Introduction to the Refractive Index Detector
10
How the Detector Operates
11
Detection Principle
13
Flow Path
16
Early Maintenance Feedback
21
Instrument Layout
22
Electrical Connections
23
Interfaces
25
Setting the 8-Bit Configuration Switch (On-Board LAN)
31
2 Site Requirements and Specifications
39
Site Requirements
40
Physical Specifications
43
Performance Specifications
44
3 Installing the Refractive Index Detector
47
Unpacking the Detector
48
Delivery Checklist
48
Optimizing the Stack Configuration
51
Optimizing the One Stack Configuration
52
Optimizing the Two Stack Configuration
54
Installing the Detector
56
Flow Connections
59
4 Using the Refractive Index Detector
63
Operation of the Refractive Index Detector
64
Before Using the System
64
Refractive Index Detector Control
66
Refractive Index Detector Settings
68
Refractive Index Detector more Settings
70
Running a Checkout Sample
72
Checking Baseline Noise and Drift
76
Setting the Test Conditions
76
Evaluation
82
5 Optimizing the Refractive Index Detector
83
Refractive Index Detector Optimization
84
6 Troubleshooting and Diagnostics
89
Overview of the Module's Indicators and Test Functions
90
Status Indicators
92
Power Supply Indicator
92
Module Status Indicator
93
User Interfaces
94
Agilent Lab Advisor Software
95
7 Error Information
97
What Are Error Messages
99
General Error Messages
100
Timeout
100
Shut-Down
101
Remote Timeout
101
Synchronization Lost
102
Leak
102
Leak Sensor Open
103
Leak Sensor Short
103
Compensation Sensor Open
104
Compensation Sensor Short
104
Fan Failed
105
Open Cover
105
Cover Violation
106
Refractive Index Detector Specific Error Messages
107
Thermal Fuse Open
107
Heater Resistance too High
107
Heater Fuse
108
Wrong Temperature Profile
108
Undecipherable Temperature Signal
109
Maximum Temperature Exceeded
109
Purge Valve Fuse Blown
110
Recycle Valve Fuse Blown
110
Purge Valve Not Connected
111
Recycle Valve Missing
111
Lamp Voltage too Low
112
Lamp Voltage too High
112
Lamp Current too High
112
Lamp Current too Low
113
Wait Function Timed out
113
Not-Ready Messages
114
Purge Time Running
114
Wait for Purge
114
Unbalanced Diodes
115
Not Enough Light
115
Too Much Light
115
8 Test Functions
117
Refractive Index Calibration
118
Optical Balance
123
Using the Build-In Test Chromatogram
126
Agilent Technologies 1260 Infinity User Manual (156 pages)
Infinity Thermostatted Column Compartment
Brand:
Agilent Technologies
| Category:
Heater
| Size: 2.5 MB
Table of Contents
Table of Contents
5
1 Introduction to the Column Compartment
9
Introduction
10
System Overview
13
Leak and Waste Handling
13
Column-Identification System
16
Column Switching Valve (Optional)
18
2 Site Requirements and Specifications
21
Site Requirements
22
Physical Specifications
25
Performance Specifications
26
3 Installing the Column Compartment
27
Unpacking the Column Compartment
28
Delivery Checklist
28
Optimizing the Stack Configuration
29
One Stack Configuration
29
Two Stack Configuration
32
Installation Information on Leak and Waste Handling
34
Installing the Column Compartment
38
Flow Connections of the Column Compartment
41
Placing Columns
45
Column-Identification Tag
45
Column Clip
46
4 Using the Module
47
Leak and Waste Handling
48
Solvent Information
49
5 How to Optimize the Column Compartment
51
Optimizing the Performance of Your Column Compartment
52
6 Troubleshooting and Diagnostics
53
Overview of the Module's Indicators and Test Functions
54
Status Indicators
56
Power Supply Indicator
56
Module Status Indicator
57
Available Tests Depending on User Interfaces
58
Agilent Lab Advisor Software
59
7 Error Information
61
What Are Error Messages
62
General Error Messages
63
Timeout
63
Shutdown
63
Remote Timeout
64
Lost CAN Partner
65
Leak
66
Leak Sensor Open
67
Leak Sensor Short
67
Compensation Sensor Open
68
Compensation Sensor Short
68
TCC Error Messages
69
Left Fan Failed
69
Right Fan Failed
70
Open Cover
70
Cover Violation
71
Left Temperature Timeout
71
Right Temperature Timeout
72
Defective Temperature Sensor
72
Heater Profile
73
Valve Failed
74
Column Temperature
75
Heatsink Temperature
75
Defective Heater Circuit
76
Agilent Technologies 1260 Infinity User Manual (144 pages)
Thermostatted Column Compartment
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 3.87 MB
Table of Contents
Table of Contents
5
1 Introduction to the Column Compartment
9
Main Features
10
System Overview
11
Column-Identification System
13
Column Switching Valve (Optional)
15
Instrument Layout
18
Electrical Connections
19
Interfaces
21
Setting the 8-Bit Configuration Switch (Without On-Board LAN)
27
2 Site Requirements and Specifications
33
Site Requirements
34
Physical Specifications
37
Performance Specifications
38
3 Installing the Column Compartment
39
Unpacking the Column Compartment
40
Delivery Checklist
40
Optimizing the Stack Configuration
41
One Stack Configuration
41
Two Stack Configuration
44
Installing the Column Compartment
46
Flow Connections of the Column Compartment
49
Placing Columns
53
Column-Identification Tag
53
Column Clip
54
4 How to Optimize the Column Compartment
55
Optimizing the Performance of Your Column Compartment
56
5 Troubleshooting and Diagnostics
57
Overview of the Module's Indicators and Test Functions
58
Status Indicators
59
Power Supply Indicator
59
Module Status Indicator
60
Available Tests Depending on User Interfaces
61
Agilent Lab Advisor Software
62
6 Error Information
63
What Are Error Messages
64
General Error Messages
65
Timeout
65
Shut-Down
65
Remote Timeout
66
Synchronization Lost
67
Leak
67
Leak Sensor Open
68
Leak Sensor Short
68
Compensation Sensor Open
69
Compensation Sensor Short
69
TCC Error Messages
70
Left Fan Failed
70
Right Fan Failed
71
Open Cover
71
Cover Violation
72
Left Temperature Timeout
72
Right Temperature Timeout
73
Defective Temperature Sensor
73
Heater Profile
74
Valve Failed
74
Column Temperature
75
Heatsink Temperature
76
Defective Heater Circuit
76
Agilent Technologies 1260 Infinity User Manual (120 pages)
Infinity Evaporative Light Scattering Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 1.68 MB
Table of Contents
Table of Contents
5
1 Introduction
9
The Low Temperature Evaporative Light Scattering Detector
10
Principle of Operation
12
Nebulization
14
Evaporation of the Solvent
17
Detection
17
2 Site Requirements and Specifications
19
Site Requirements
20
Power Considerations
20
Gas Considerations
21
Power Cords
21
Exhaust Venting and Drain Requirements
22
Location of the Detector in the Laboratory
23
Environment
23
Specifications
24
3 Installing the Detector
27
Lifting and Carrying the Module
28
Unpacking the System
30
Installing the Detector
32
Gas Supply
33
Vent the Exhaust Line to a Fume Hood
37
Electrical Connections
38
Additional Options
40
Installing the Nebulizer and Nebulization Chamber Assembly
43
Connecting the Siphon Overflow
46
Connecting the Nebulization Gas to the Nebulizer
47
Connecting the Column
47
Powering up the Unit
47
4 Using the System
49
Preparing the System for Operation
50
Auto-Zeroing the Detector
51
Manual Auto-Zeroing of the Detector
51
External Auto-Zeroing of the Detector
51
Routine Operation of the System
52
Installation Test Procedure
54
Powering down and Shutting down the System
56
5 Optimizing Performance
59
Selecting the Optimum Temperature
60
Optimizing the Mobile Phase
62
Sample Pre-Treatment
62
Column Treatment
63
Optimizing the Filter
64
6 Troubleshooting and Diagnostics
65
Basics of Troubleshooting
66
Initial Troubleshooting Activities
67
If There Is no Response from the System
68
Perform the Noise Tests
69
Specific Detector Troubleshooting
70
Noise Test Procedures
71
Preliminary Activities
72
Electronic Noise Test
73
Background Noise (Stray Light) Test
74
Solvent Noise Test
75
Column Noise Test
77
Troubleshooting Based on Diagnostic Tests
78
Electronic Noise Test
78
Stray Light Test
78
Failed Run of Standard Sample
78
Troubleshooting Based on Instrument Signals
79
No Signal Is Observed
79
Decrease in Sensitivity
80
A Noisy Signal Is Observed
80
Agilent Technologies 1260 Infinity User Manual (108 pages)
Sample Capacity Extension
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 1.74 MB
Table of Contents
Table of Contents
5
1 Overview
9
Description
10
Specifications
11
General Instrument
11
Robotic Arm
12
Physical Performance
12
Environmental
12
Physical
13
Electrical
14
Barcodes
14
2 Installation
15
Site Preparation
16
Bench Space Requirements
16
Contents of the G2257A Shipping Kit
17
Installation
19
Installing the Automation Interface
19
Setting up the Well-Plate Handler
25
Installing the Optional Rack Extension
33
Installing the Optional Fixed Barcode Reader
35
Installing the Optional Hand-Held Barcode Reader
38
Barcode Requirements
39
Making the Electrical Connections
41
Adjusting the Barcode Reader Position
42
Adjusting the Lateral Position of the Well-Plate Handler
44
Preliminary Adjustment of the Well-Plate Handler Position
45
Well-Plate Handler Teaching
47
Teaching Using the Chemstation
47
Fine Adjustment of the Well-Plate Handler Position
51
Adjusting the Radius
51
Adjusting for the Gripper Fingers
52
Adjusting the Centering Spring
53
De-Installation of the Automation Interface
54
Installing a New Automation Interface
55
3 G2257A Software Navigation
57
Using the Sample Capacity Extension with the Agilent Chemstation
58
Well-Plate Handler Configuration
58
4 Working with the Sample Capacity Extension
63
What Is a Hypersequence
64
Creating a Hypersequence
65
Hypersequence Parameters
65
Barcode Settings
69
The Hypersequence Table
70
Importing an Import File
72
Making an Import File
76
5 Troubleshooting and Error Handling
82
Well-Plate Handler Test
82
Testing with the Agilent Chemstation
82
Automation Interface Test
85
Testing with the Chemstation
85
Solving Problems
87
Well-Plate Handler Does Not Turn on When Switched on
87
The Well-Plate Handler Arm Does Not Move down Far Enough to Depress the Plate Sensor Switch
87
Error Messages
88
AI Door Error
88
Plate Error
88
AI Door Sensor Error
88
Power Failure on AI
89
High Performance Autosampler Thermostat Enabled Error
89
Maintenance
90
Cleaning the Well-Plate Handler
90
Changing the Fuse(S)
91
Moving the Well-Plate Handler
92
Long-Term Shutdown
93
Parts List
94
Agilent Technologies 1260 Infinity Service Manual (108 pages)
Infinity Micro Degasser
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 1.88 MB
Table of Contents
Table of Contents
3
1 Introduction
5
Introduction to the Micro Vacuum Degasser
6
2 Site Requirements and Specifications
7
Site Requirements
8
Physical Specifications
11
Performance Specifications
12
3 Installing the Micro Vacuum Degasser
13
Unpacking the Micro Vacuum Degasser
14
Accessory Kit Contents
14
Optimizing the Stack Configuration
16
Installing the Micro Vacuum Degasser
19
Flow Connections to the Micro Vacuum Degasser
21
Operational Hints for the Micro Vacuum Degasser
24
General Priming Instructions
24
Priming the Degasser
24
Priming with a Syringe (Only Recommended if Priming with the Pump Fails)
25
Transporting the Micro Vacuum Degasser
27
4 Using the Micro Vacuum Degasser
29
When to Use a Micro Vacuum Degasser
30
Prevent Blocking of Solvent Filters
32
Solvent Information
34
Material Information
34
5 Optimizing Performance Increasing the Degasser Performance and Degassing Level
42
6 Troubleshooting and Diagnostics
43
Overview of the Degasser's Indicators
44
Status Indicators
45
Instrument Status Indicator
45
Hardware Symptoms
47
All Lamps Are off
47
If the Status Indicator Is Red
48
If the Status Indicator Is Yellow and the Vacuum Pump Is Not Running
48
Status Indicator Becomes Red and Vacuum Pump was Running
49
7 Maintenance
51
Introduction to Maintenance and Repair
52
Simple Repairs
52
Warnings and Cautions
53
Cleaning the Instrument
54
Removing and Refitting the Top Cover
55
Assembling the Main Cover
58
Exchanging the Fuses of the Power Inline Filter
60
Exchanging the Status Light Pipe
62
8 Repairs
63
Exchanging Internal Parts
64
Overview of Repair Procedures
65
Overview of Internal Parts
66
Exchanging a Vacuum Chamber
68
Exchanging the Vacuum Pump
70
Exchanging the Proportional Valve
72
Exchanging the Vacuum Tubings
74
Exchanging the Degasser Control Assembly and the Sensor Assembly
76
Agilent Technologies 1260 Infinity User Manual (96 pages)
HPLC-Chip Cube Interface
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 2.72 MB
Table of Contents
Table of Contents
5
1 Introduction to HPLC-Chip Technology
9
Overview
10
Chip Types
13
The MS Calibration and Diagnosis Chip, Part No. G4240-61001
13
The Protein ID Chip, Part No. G4240-62001
14
Modes of Operation
14
More Chips
18
2 Introduction to the Chip Cube
19
Intended Use
20
Introduction
21
Power Switch
22
Safety Features
23
Main Assemblies
24
Principle of Operation
26
Flow Connections
29
3 Site Preparation
31
Site Requirements for the G4240A Chip Cube
32
Power Considerations
32
Bench Space
32
Environment
33
Sound Emission
34
Specifications of the G4240A HPLC-Chip Cube
34
4 Installation
37
Unpacking the Agilent G4240A HPLC-Chip MS Interface
38
Damaged Packaging
38
Delivery Checklist
38
Accessory Kit
40
System Setup Considerations
42
Single Stack Setup
43
Twin Stacks
45
Preparation of Existing Systems
47
Chip Cube Hardware Installation
49
5 Operation
53
Chip Loading and Unloading
54
Configuration
55
Configure Loading Pump and Analytical Pump
55
Injection Flush Volume
56
Injector Flush Volume and the Use of Injector Programs
57
Operational Parameters
60
Setting up Chip Cube Parameters
61
Chip (Valve Positions / Tip)
61
Time
62
Time Table
63
Instrument Actuals
63
Chip Details Screen
64
Spray Ignition
66
Conditions to Avoid
69
6 Maintenance Procedures
71
Maintenance Overview
72
Replacing Capillaries
73
Cleaning the Valve Rotors (Quick Procedure)
76
Updating the Chip Cube Firmware
79
Agilent Technologies 1260 Infinity Quick Start Manual (98 pages)
Purification Solution
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 1.7 MB
Table of Contents
Table of Contents
4
1 The Role of the Method Developer
7
2 Preparing Default Purification Methods
9
General Method Settings
11
Analytical Method Settings
16
Preparative Method Settings
19
Agilent Active Splitter (G1968D/E/F)
23
Critical Method Parameters
24
3 Setting up an Analytical and Preparative System
27
Setting up an Analytical System
28
Setting up a Preparative System
30
4 Setting up and Running a Purification Task
33
Setting up a Purification Task
34
Configuring a New Task
35
System Suitability Tests
38
Running a Task
39
Processing Partial Data and Cloning Tasks
40
Reviewing Analytical Results
42
5 Reviewing Purification Results
43
6 Calibration Procedures
45
Characterizing the Delay Volumes: Mixing Point to UV Detector and Column to UV Detector
48
Tubing Volumes for Predefined Systems
48
Calculation of Delay Volume: Column to UV Detector
50
Calculation of Delay Volume: Mixing Point to UV Detector
52
Experimental Measurement of Delay Volume: Mixing Point to UV Detector
57
Determining the Elution Time of Acetone
60
Characterizing the Column Volume
63
Column Volume: Standard Analytical System
63
Combined Analytical and Preparative System
66
System Configuration and Delay Time Calibration
70
Running Conditions for Calibration Procedures
71
Configuring the Analytical and Preparative Systems
73
Delay Time Determination for Analytical Systems (MSD And/Or Auxiliary Detectors)
74
Configuring the Preparative System Parameters
75
Delay Time Calibration for Preparative Systems
77
Insufficient UV-To-FC Delay Time or MSD-To-FC Delay Time
80
7 Checkout Procedure
83
Acquire an Analytical Run Using the Chemstation Sequence
85
UV-Only Workflow: Focused Gradient in the Purification Software
89
Agilent Technologies 1260 Infinity User Manual (80 pages)
Micro Degasser
Brand:
Agilent Technologies
| Category:
Measuring Instruments
| Size: 1.41 MB
Table of Contents
Table of Contents
3
1 Introduction
5
Introduction to the Micro Vacuum Degasser
6
2 Site Requirements and Specifications
7
Site Requirements
8
Physical Specifications
11
Performance Specifications
12
3 Installing the Micro Vacuum Degasser
13
Unpacking the Micro Vacuum Degasser
14
Accessory Kit Contents
15
Optimizing the Stack Configuration
16
Installing the Micro Vacuum Degasser
19
Flow Connections to the Micro Vacuum Degasser
21
Operational Hints for the Micro Vacuum Degasser
24
General Priming Instructions
24
Priming the Degasser
25
Priming with a Syringe (Only Recommended if Priming with the Pump Fails)
26
Transporting the Micro Vacuum Degasser
27
4 Using the Micro Vacuum Degasser
29
When to Use a Micro Vacuum Degasser
30
Solvent Information
32
5 Optimizing Performance Increasing the Degasser Performance and Degassing Level
36
6 Troubleshooting and Diagnostics
37
Overview of the Degasser's Indicators
38
Status Indicators
39
Instrument Status Indicator
40
Hardware Symptoms
41
All Lamps Are off
41
If the Status Indicator Is Red
42
If the Status Indicator Is Yellow and the Vacuum Pump Is Not Running
42
Status Indicator Becomes Red and Vacuum Pump was Running
44
7 Maintenance
45
Introduction to Maintenance and Repair
46
Simple Repairs
46
Warnings and Cautions
47
Cleaning the Instrument
48
Using the ESD Strap
48
Removing and Refitting the Top Cover
49
Assembling the Main Cover
52
Exchanging the Fuses of the Power Inline Filter
54
Exchanging the Status Light Pipe
56
8 Parts and Materials for Maintenance
57
Cover Parts Cover
58
Sheet Metal Kit
59
Power and Status Light Pipes
60
Accessory Kit
61
9 Cable Overview
63
Overview
64
Remote Cable
66
Agilent Technologies 1260 Infinity Operator's Quick Manual (16 pages)
Purification Solution
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 0.46 MB
Table of Contents
Table of Contents
4
1 The Role of the Operator
5
2 Executing a Purification Task
7
Configuring a New Task
8
Running a Task
9
Processing Partial Data and Cloning Tasks
10
Reviewing the Analytical Results
12
Reviewing the Purification Results
13
Forcing the Purification Task to Close
14
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