Contamination - Agilent Technologies 5975C TAD VL MSD Troubleshooting And Maintenance Manual

2
General Troubleshooting

Contamination

Contamination is usually identified by excessive background in the mass
spectra. It can come from the GC or from the MSD. The source of the
contamination can sometimes be determined by identifying the contaminants.
Some contaminants are much more likely to originate in the GC. Others are
more likely to originate in the MSD.
Contamination originating in the GC typically comes from one of these
sources:
• Column or septum bleed
• Dirty GC inlet
• GC inlet liner
• Contaminated syringe
• Poor quality carrier gas
• Dirty carrier gas tubing
• Fingerprints (improper handling of clean parts)
Contamination originating in the MSD typically comes from one of the
following sources:
• Air leak
• Cleaning solvents and materials
• Diffusion pump fluid
• Foreline pump oil (standard foreline pump)
• Fingerprints (improper handling of clean parts)
Table 5
of those contaminants, and the likely sources of those contaminants.
54
lists some of the more common contaminants, the ions characteristic
5975 Series MSD Troubleshooting and Maintenance Manual