Micromeritics ACCUPYC III Operator's Manual page 68

Gas displacement pycnometer
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2 About the Software
Calibration
Description
Fields
Specifies the size of the cup placed in the chamber along with the cup. The pre-set
Volume
volumes of those items are subtracted out of the measurement to obtain the cup
Standard
volume.
Key in the Fill Pressure. For most applications, the default of 19.500 psig (134.45
Fill
kPag) is adequate.
Pressure
Tap
Next
to continue the calibration process.
If the prompt, "Make sure the sample chamber is empty" displays, verify the sample chamber is
n
empty and tap Next. The process continues.
If the prompt, "Insert the Calibration Standard" displays, insert the calibration standard and tap
n
Next. The process continues.
When the calibration is complete, the results are displayed. The chamber volumes are shown in
comparison to the values that were in place prior to the current calibration. One of the following
occurs:
Rejected by system condition. The calibration is rejected and an error displays if any of the
n
measured volumes change by more than 0.2% compared to the initial factory calibration or the
most recent volume calibration. Refer to the Appendix C -
suggested corrective actions, check the system and try again, or contact your Micromeritics
Service Representative.
If the operation is within system limits, the system prompts, "Do you want to accept the new
n
calibration?" Tap
Yes
2 - 38
to apply the calibration. Tap
Error Messages on page C - 1
No
to reject the calibration.
AccuPyc III Operator Manual
135-42800-01 (Rev -) — Nov 2023
for

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