Correction Of Dynamic Measurement - Thermo Scientific HAAKE RotoVisco 1 Instruction Manual

Rheometer
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14.3 Correction of Dynamic Measurement

(RheoStress 1)
Description of the problem
There are two important influences:
Mechanical influence:
additional frequency dependent phase shift caused by
inertia I of the rotor (as well as by the damping D and
the spring constant K of the measuring system).
Electro-magnetic interactions:
frequency dependent phase shift  between the cur-
rent in the motor coil and the torque acting on the axis.
reduced motor torque (M
(and current) dependent induction effects in the coil.
Consequently, we have to correct two quantities in the rheo-
logical equations:
phase angle 
 corrects for electromagnetic effects,
mechanical influences on the phase shift can be
corrected by taking into account I, (D), (K).
acting torque on the axis M
 corrects for electromagnetic influences on the
torque amplitude.
Quantities we assume to be well-known or measured exactly:
inertia I (determined by a creep experiment without
sample),
damping constant D and spring constant K of the sys-
tems (both have only a negligable influence),
A- and M-factors of the measuring system (sensor),
rotation angle  measured with the optical encoder.
Indices used:
exp
me
(without)  corrected data
135
()<M
d
d
 original measuring data
 quantities corrected for electromagnetic
but not for mechanical (inertia) influences
) due to frequency
0

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