Thermo Scientific Prima PRO Manuals

Thermo Scientific Prima PRO Manuals

Manuals and User Guides for Thermo Scientific Prima PRO. We have 1 Thermo Scientific Prima PRO manual available for free PDF download: User Manual

Thermo Scientific Prima PRO User Manual

Thermo Scientific Prima PRO User Manual (203 pages)

Mass Spectrometers

Brand: Thermo Scientific | Category: Measuring Instruments | Size: 4 MB

Table of Contents

Table of Contents
6
Chapter 1 Introduction

14
Chapter 2 Safety Information

16
- Overview
  16
- Safety Conventions and Symbols
  17
- System Safety
  18
- Connecting the Instrument to the Electrical Supply
  19
- Repair & Maintenance
  19
- Changing the Rotary Pump Oil
  19
- Switching on the Rotary Pump
  19
- Rotary Pump Exhaust Outlet
  20
- Inlet System Exhaust
  20
- Gas Mixtures in the Inlet System
  21
- Protective Clothing
  21
- Hazardous Materials
  21
- Hazardous Area Systems
  22
- Fan Noise
  22
Chapter 3 Site Requirements

24
- Physical Installation
  24
- Cable Entries
  25
- Safe Area Systems
  25
- Hazardous Area Systems
  25
- Computer and Communications
  25
- Fibre Optic Communication
  26
- Hazardous Area Systems
  26
- Environment
  27
- General
  27
- Temperature
  27
- Humidity
  27
- Vibration
  27
- Particulate Contamination
  27
- Altitude
  28
- Inlet Gas Connections
  28
- Calibration Gases
  28
- Sample Gases
  29
- Exhaust Gas Connections
  30
- Power
  31
- Voltage and Frequency
  31
- Requirements
  31
- Over-Current Protection
  33
- Power Quality
  33
- Power Connection
  33
- Other Services
  33
- Safe Area Systems
  33
- Dry Gas Vent
  33
- Enclosure Purge
  33
- Hazardous Area Systems
  34
- Dry Gas Vent
  34
- Rotary Pump Purge
  34
- Compressed Air Requirements
  35
- Options
  36
- Pump Purge Gas
  36
- Rotary Oil Box Purge
  36
- Rotary Pump Ballast
  36
- Turbo Pump Bearing Purge
  36
- External I/O Unit
  37
Chapter 4 Handling & Storage

38
- Receiving the Instrument
  38
- Unpacking the Instrument
  39
- Storing the Instrument
  39
Chapter 5 Installation & Interconnection

40
- Introduction
  40
- Positioning the Instrument
  40
- Cable Connections
  40
- General Requirements
  40
- Safe Area Systems
  40
- Hazardous Area Systems
  41
- Power Connection
  41
- Safe Area Systems
  41
- Sentinel PRO Sample Pump Power Connection
  43
- Safe Area Systems
  43
- Hazardous Area Systems
  43
- Gas Connections
  43
- Computer System
  44
Chapter 6 Commissioning

46
- General
  46
- Procedure
  46
Chapter 7 Startup & Shutdown

50
- Startup
  50
- Procedure
  50
- Vacuum Gauge Trip Level
  53
- Checking Instrument Tuning and Mass Alignment
  54
- Emission
  55
- Peak Shape
  55
- Sensitivity
  56
- Detectors
  57
- Mass Alignment
  57
- Heaters
  59
- Shutdown
  60
- Introduction
  60
- Shutdown Procedure
  60
- Emergency Shutdown
  61
Chapter 8 Status & Tuning Parameters

62
- Instrument Status
  62
- Source Tab
  63
- Electron Energy
  63
- Emission
  63
- Filament Current
  63
- Filament Current Limit
  63
- Filament Integrity
  64
- In Current Limit
  64
- Ion Energy
  64
- Repeller Voltage
  65
- Source Current
  65
- Source Temperature
  65
- Trap Current
  65
- Analyser Tab
  66
- ASU Controller Status
  66
- Cabinet Temperature
  66
- Electronics Temperature
  66
- Magnet Controller Status
  66
- Mass Filter
  67
- Pressure Set Point
  67
- System Pressure
  67
- System Pressure Trip
  68
- Turbo Motor Current
  68
- Turbo Operating Hours
  68
- Turbo Speed
  68
- Turbo Speed Interlock
  69
- Vacuum
  69
- Vent Valve
  69
- Inlet
  69
- Pressure Raw
  69
- RMS Ambient Temperature
  69
- RMS Body Temp
  69
- RMS Controller Status
  69
- RMS Sample Flow Sensor
  69
- RMS Flow Zero
  69
- Sample Tube Temperature
  70
- Collector Tab
  70
- Faraday Deflector
  70
- Multiplier Deflector
  70
- Multiplier Voltage
  70
- Negative and Positive Quad Lens Voltages
  70
- Resolution
  70
- Power
  71
- Amplifier +24V
  71
- Analyser Supplies +24V
  71
- Instrument CPU 24V
  71
- Fan 24V
  71
- Inlet Probe Current
  71
- Magnet Supply Current
  72
- Magnet Sync AC
  72
- Power Controller Status
  72
- Turbo 24V
  72
- User IO 24V
  72
- Vent Valve 24V
  72
- Communications
  72
- Host Comms Quiet
  72
- User I/O 0 Comms Quiet
  78
- User I/O 1 Comms Quiet
  78
- User I/O 2 Comms Quiet
  78
Chapter 9 Fault Diagnosis

78
- Alarm Conditions
  78
- Leak Detection
  79
- Mass Spectrometer Faults
  80
- No Peaks
  80
- Poor Sensitivity
  81
- Poor Stability on Startup
  81
- Poor Results Following Calibration
  82
- Ion Source and Magnet Pole Pieces Assembly
  83
- Filament Failure
  83
Chapter 10 Maintenance

86
- Maintenance Schedule
  86
- Procedures
  86
- Rotary Pump Oil Level
  86
- Cleaning the Cooling Fans
  87
- Lubricating the Turbo Molecular Pump
  88
- Dismantling and Cleaning Procedures
  88
- Filament
  88
- Ion Source
  90
- Magnet Pole Piece Assembly
  93
- Fuses
  95
Appendix A Hazardous Area Operation

98
- Introduction
  98
- Installation
  99
- General Hazardous Area Work
  100
- Commissioning and Maintenance
  100
- Routine Checks
  101
- Hazardous Area - General
  101
- Area Classification
  101
- Gas Classification
  102
- Methods of Protection
  102
- Purge/Pressurisation
  103
- Flameproof (Europe) or Explosion Proof (North America
  103
- Increased Safety
  104
- Non-Electrical
  104
- Purge Operation
  105
- Purge Overview
  105
- Purge Operation Requirements
  106
- Parameter Measurement
  107
- Sample Containment System
  108
- Definition and Description
  108
- Parameters
  108
- Leakage Handling
  108
- Inspection and Testing
  110
- Enclosure Leak Testing
  111
- Purge Operation and Testing
  112
- All System Types
  112
- ATEX, Iecex and X-Purge Systems
  112
- Z-Purge Systems
  113
- Other Hazardous Area Considerations
  113
- Temperature
  113
- Over-Temperature Protection
  113
- Batteries
  114
- Dry Gas Vent
  114
- Rotary Vacuum Pump
  115
- General
  115
- Thermal Trip
  115
- Purge
  115
- Calibration Panels
  116
- Air Conditioner
  117
- Remote / Dual RMS
  117
- RMS and Instrument in Hazardous Area
  117
- RMS in Hazardous Area and Instrument in Safe Area
  117
- Sample Pump (Sentinel PRO Applications
  118
- Fibre Optic Communications
  118
- Service Replacement Items
  118
- Troubleshooting
  120
- Standards Conformance
  122
- Introduction to the Prima PRO Hardware
  130
- Main Components
  130
- Principle of Operation
  131
- Vacuum System
  133
- Ion Source
  134
- Filaments
  136
- Mass Analyser
  138
- Collector
  138
- Ion Detection
  139
- MCP Detector Assembly
  139
- MCP Operation
  140
- Faraday Detector
  142
- Introduction of a Gas Sample
  142
- Mass Spectrometer Parameters
  144
- Sensitivity
  144
- Resolution
  144
- Cracking Patterns
  146
- Ion Types
  146
- Molecular Ion
  146
- Isotope Ions
  146
- Fragment Ions
  147
- Multiple-Charged Ions
  147
- Rearrangement and Recombination Peaks
  147
- Definitions
  148
Appendix C Technical Description: Inlet

150
- Rapid Multi-Stream Sampler (RMS
  150
- Introduction
  150
- Safety
  150
- Inlet Specification
  151
- Inlet Operation
  152
- General Description
  152
- Connection to the Mass Spectrometer
  153
- Seals
  153
- Inlet Selection
  154
- Calibration Gas Control
  154
- Gas Connection
  155
- Exhaust Connection
  156
- Heating
  157
- Main Body Heater
  157
- Sample Tube Heater
  157
- Flow Sensor
  160
- Digital Inputs
  160
- Vginet
  160
- Inlet Testing
  161
- Functional Testing
  161
- Cross Port Leakage
  163
- External Leakage
  164
- Maintenance
  164
- Routine Maintenance
  165
- Sample Tube Removal
  168
- Inlet Ports
  170
- Cleaning Procedure
  170
- Inlet Options
  171
- Remote Mounting
  171
- Dual RMS
  172
- Solenoid Inlet
  176
- Introduction
  176
- Inlet Operation
  177
- Valve Operation
  179
- Capillary Connection
  179
- Heating
  180
- Inlet Controller
  180
- General
  180
- Valve Drives
  181
- Manifold Heater
  181
- Microcapillary Block Heater
  181
- Flow Sensor
  181
- Digital Inputs
  181
- Vginet
  182
- Testing
  182
- Capillary Testing
  182
- Valve Function
  183
- Cross Seat Leakage
  183
- External Leakage
  184
- Maintenance
  185
- Calibration Inlet
  185
- Sample Inlet
  187
- Cleaning Procedure
  188
Appendix D Local I/O

190
- Introduction
  190
- Serial I/O
  190
- Serial Link Type Selection
  190
- Indicators
  191
- Fibre Optic Serial Connection
  191
- Supplying Power to the External I/O Circuit
  193
- Indicators
  193
- Analogue I/O
  194
Appendix E Air Conditioner

196
- Normal Operation
  196
- Fault Conditions
  197
- Fault Diagnosis
  198
Appendix F Regulatory

200
- Fcc
  200
- Weee
  201
- China Rohs
  202

Advertisement

Advertisement

Related Products

Thermo Scientific Categories

Laboratory Equipment Measuring Instruments

Freezer

Freezer Accessories

Refrigerator

More Thermo Scientific Manuals