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Summary of Contents for Thermo Scientific HAAKE
- Page 1 Thermo Scientific HAAKE Falling Ball Viscometer Type C Instruction Manual March 2020 002-7585 Version 2.4...
- Page 2 © 2020 Thermo Fisher Scientific Inc. All rights reserved. Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.
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Page 3: Table Of Contents
Table of Contents Quality Assurance ......Your Contacts at Thermo Fisher Scientific ..Key to Symbols . - Page 4 Table of Contents 14. Appendix ........14.1 Example: Evaluation .
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Page 5: Quality Assurance
Quality Assurance/Contacts at Thermo Fisher Scientific Quality Assurance Dear customer, Thermo Fisher Scientific implements a Quality Manage- ment System certified according to ISO 9001:2008. This guarantees the presence of organizational structures which are necessary to ensure that our products are deve- loped, manufactured and managed according to our cu- stomers expectations. -
Page 6: Key To Symbols
Safety Notes and Warnings Key to Symbols Warns the user of possible damage to the unit, draws attention to the risk of injury or contains safety notes and warnings. Denotes an important remark. Indicates the next operating step to be carried out and ... - Page 7 Safety Notes and Warnings Thermo Fisher Scientific does not assume respon- sibility for independent repairs and consequences of improper use. Do not clean the unit with solvents (fire risk!) - - a wet cloth soaked in household detergent is nor- mally sufficient.
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Page 8: Unpacking
Unpacking / Setting Up Unpacking 5.1 Transportation damage? Notify carrier (forwarding merchant, railroad, post office etc.), Compile a damage report. 5.2 Before return delivery: Inform dealer or manufacturer (Small problems can often be dealt with on the spot). 5.3 Contents of Delivery The following standard accessory is delivered together with the falling ball viscometer:... -
Page 9: Material For Use
Unpacking / Setting Up 5.4 Material for use No other material except for cleaning material (800-0125 cleaning piston, 800-0131 cleaning brush) is necessary at normal use. 5.5 Spare parts See chapter 13. 5.6 Waste disposal The transportation packing is made out of paper and can be recycled. -
Page 10: Setting Up
Unpacking / Setting Up Setting Up 6.1 Assembly Insert the measuring tube into the stand and fasten it with the knurled nut. -
Page 11: Unit Description
Unit Description Unit Description 7.1 Principle of the measurement The HAAKE Falling Ball Viscometer measures the viscosity of transparent newtonian liquids. This viscosity is correlated to the time a ball requires to fall a defined distance. The rol- ling and sliding movement of the ball through the sample filled into a slightly inclined cylindrical measuring tube is de- scribed by means of the fall time. -
Page 12: Functional Elements
Functional Elements Functional Elements 1 Falling tube 12 Jacket tube 2 Ball 13 Hollow stopper 3 Tempering room 14 Stopper 4 Screw 15 Capillary 7 Set screw 16 Closing plate 8 Gasket 17 Gasket for falling tube 9 Cover 18 Threaded bush 11 Brace 20 Connecting rod... -
Page 13: Measuring
Measuring 9.1 Preparation for a test 9.1.1 Temperature control The HAAKE Falling Ball Viscometer may be temperature controlled in a temperature range from --20 C up to +150C using liquid circulators. Ensure that the sample to be measured is homogeneously tempered. -
Page 14: Selection Of The Balls
Measuring 9.1.3 Selection of the balls The standard ball set contains 6 balls, which pass through the measuring tube of an inner diameter of approximately 15.94 0.01 mm. Order- Ball Made of Density Diameter Constant K Recomm. (standard of the ball (approx.) measuring values) -
Page 15: Measurement Of The Falling Times
Measuring 9.2 Measurement of the falling times The jacket tube snaps into a defined 10-position at the bot- tom of the instrument. By turning over the jacket tube, the ball is set to the measu- ring position. The falling time of the ball moving from the ring mark A to ring mark B is determined by using a stop watch. -
Page 16: Evaluation Of The Test Results
Measuring 9.3 Evaluation of the test results The dynamic viscosity (in mPas) is calculated using the following equation: = K ( -- ) ¡ t where: K = ball constant in mPascm /gs (see chapter 11) = density of the ball in g/cm (see chapter 11) ... -
Page 17: Reproducibility
Measuring To evaluate the reliability of the results the following criteria may be used: 9.3.1 Reproducibility (one person, one instrument) If one person determines two test results under identical test conditions, these results are supposed to be acceptable if they do not vary more than the figures stated in the table below from the average value. -
Page 18: Viscosity Determination Of Gases
Measuring 9.4 Viscosity determination of gases The viscosity determination of gases has to be done with ball G which is made out of glass. The measuring tube must be closed with rubber stop- pers fitted with glass stopcocks. Measuring tube, glass ball and gas must be clean and dry. -
Page 19: Cleaning The Measuring Tube
Cleaning the Measuring Tube 10. Cleaning the Measuring Tube Usually the tube is cleaned by rinsing it with a suitable solvent. High viscous liquids (glue and heavy oils, etc.) have to be removed with the cleaning piston which is supplied with the instrument. -
Page 20: Calibration Of The Falling Ball Viscometer
Calibration 11. Calibration of the Falling Ball Viscometer The falling ball viscometer is checked according to the HAAKE regulations before delivery. The geometry relates strictly on the DIN 53015/ISO 12058 and therefore the listed ball constants can be used. The calibration of the instrument can be done using nation- ally recyclable calibration fluids. - Page 21 Calibration The calibration fluids should be stored in dark rooms and be used within 3 months after their date of expiry. The disposal depends of the composition of the substance which is listed in the “EC - - SAFETY DATA SHEET”. It is absolutely essential that for calibration the instructions for filling the tube and cleaning are closely adhered to.
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Page 22: Maintenance By The User
Maintenance by the User 12. Maintenance by the User 12.1 Exchange of the measuring tube and the jacket tube Unscrew the screws 4 and remove brace 11. Loosen threaded bush 18 with socket spanner no. 003-2110. Unscrew connecting rods 20. Now remove both cover lids 7 and 9. -
Page 23: Order Numbers
Maintenance by the User 12.2 Order numbers 002-7575 Stand (cast iron) 002-2917 Levelling screws of the stand 002-6968 Falling tube (1) 800-0190 Balls (2) 002-8746 Screws M 6x12 (4) 003-2108 Cover (7) 003-2109 Cover (9) 002-9391 Brace, mounted (11) 800-0030 Jacket tube(12) 800-0012 Hollow plug (13) (15) 800-0013 Plug, brass goldplated (14) 800--0016 Plug, viton (14) -
Page 24: Spare Parts
Spare Parts 13. Spare Parts 13.1 Recommended spare parts for a period of 3 years 800-0119 Ball tweezers 800-0131 Cleaning brush (3 x) 800-0125 Cleaning piston (3 x) 800-0182 Set of balls 1 -- 6 002-6968 Falling tube 800-0030 Jacket tube 800-0015 Hollow plug, Viton 800-0090... -
Page 25: Single Parts
Spare Parts 13.2 Single parts 800- -0027 003-2110 gasket 15.6 socket spanner (teflon) 002- -5176 gasket 10.0 (viton) 800- -0119 800- -0131 800- -0125 ball tweezers cleaning brush cleaning piston... -
Page 26: High--Resolution Thermometer
Spare Parts 13.3 High- -resolution thermometer Control thermometers: 222--2322 --35 to 1 C, scaling 0.2 C, accuracy 0.2 C 222--2323 --1 to 26 C, scaling 0.1 C, accuracy 0.1 C 222--2324 24 to 51 C, scaling 0.1 C, accuracy 0.1 C 222--2325 49 to 76 C, scaling 0.1 C, accuracy 0.1 C 222--2326... - Page 27 Spare Parts peratures, then no further pretreatment is needed. Before every new measurement at a lower tempera- ture than just indicated by the thermometer, there has to be proceeded as described at point 2. In case that parts of separated filling are noticed, follow once more point 1 and 2.
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Page 28: Contents Of The Ball Box
Spare Parts 13.4 Contents of the ball box 800-0012 Hollow plug (brass) 800-0014 Cover plate 800-0118 Ball gauge to differ between the balls G, 1 and 2 Balls: 800-0002 Ball 1; 15.81; boron silica glass 800-0003 Ball 2; 15.6; boron silica glass 800-0004 Ball 3;... - Page 29 Appendix 14. Appendix 14.1 Example: Evaluation (sugar solution of 40 %) Density of ball 2: 2.2 (g/cm Density of the solution: 1.18 (g/cm Ball constant K : 0.09 (mPascm /gs) Falling time: 61 s Measuring temperature: 20.0C The absolute viscosity is ... = 0,09 ...
- Page 30 Contacting us If you have any questions regarding installation or technical issues, please contact the helpdesk. You will find the contact form at: https://tfs-3.secure.force.com/materialcharacterization/ There are several ways to contact Thermo Fisher Scientific for the information you need. To contact Technical Support or Sales, Germany and International Company Therm Electron (Karlsruhe) GmbH Part of Thermo Fisher Scientific...
- Page 31 Contacting us To contact Technical Support or Sales, China Company Thermo Fisher Scientific Adress Building 6, No. 27 XinJinqiao Rd., Shanghai 201206 Phone +86(21) 68654588 +86(21) 64457830 E-mail info.mc.china@thermofisher.com To contact Technical Support or Sales, Japan Company Thermo Fisher Scientific Adress C-2F, 3-9, Moriya-cho, Kanagwa-KU Yokohama, 221-022...