Hints on Measurement
14.4 Determination of the massmoment of inertia
(RheoStress1)
Oscillation measurements are influenced very much by the
mass moment of inertia of the sensor system at higher fre-
quencies. This is why an exact determination of this value is
very important.
Because the measurement of the mass moment of inertia by
the jump-answer-method is not precise enough, another
method was developed which is described here briefly.
If the mechanical system motor--sensor--Newtonian--oil is
excited periodically by Torque Md,0 with frequency f , the fol-
lowing
formula
results
for
the
angle
amplitude
:
(1)
0
in which I represents the mass moment of inertia , the vis-
cosity of the Newtonian--oil,
and = 2 f. At
the oscillation in air, 0 is valid. This means that at fre-
quencies that are high enough the second term under the
root in (1) can be neglected towards the first term. Equation
(1) can be changed to:
(2)
If you now measure the resulting angle amplitudes at differ-
ent torque amplitudes (OSC--Stress--Sweep) and the mea-
suring results are described as 0 = f(M
), from the as-
d,0
cending gradient
of this function the mass moment of inertia I can be deter-
mined.
(3)
or
(4)
This processing is implemented in the Thermo Fisher Scien-
tific rheometer software. For increasing the accuracy it is rec-
ommended to repeat the determination of the mass moment
of inertia for each rotor (once) five times and to enter the av-
erage value of the determined values of the mass moment
of inertia manually into the sensor file.
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