Thermo Scientific TSQ 8000 Manuals

Manuals and User Guides for Thermo Scientific TSQ 8000. We have 2 Thermo Scientific TSQ 8000 manuals available for free PDF download: User Manual, Preinstallation Manual

Thermo Scientific TSQ 8000 User Manual

Thermo Scientific TSQ 8000 User Manual (151 pages)

Mass Spectrometer

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 7.4 MB

Table of Contents

Table of Contents
3
About Your System
9
Preface

9
Chapter 1 Introduction

23
Chapter 2 Changing the Column

37
Chapter 3 Tuning

53
- Tuning the Mass Spectrometer
  54
  - TSQ Series Dashboard
    54
  - Tuning Categories
    55
  - Tune Types
    55
  - EI Standard Tune
    55
  - EI Standard Quick Tune
    56
  - EI SRM Tune
    56
  - EI Tune Check
    56
  - EI Target Tune/Ei Initial Tune
    56
  - Fast Scan Tune
    57
  - CI- Tune
    57
  - CI+ Tune
    57
  - Displaying a Report
    58
  - Sample Tune Report
    59
  - Tune Report Options
    60
  - Printing a Tune Report
    61
- Updating Tunes for New RF Lens
  62
- Creating a Method
  67
  - Accessing the Method Editor
    67
Chapter 4 Creating a Method

67
Chapter 5 Optimizing Your Method

111
- Changing the Chromatographic Separation
  111
- Finding the Best Way to Make an Injection
  112
- Improving the Way You Prepare Samples
  112
- Changing the Dwell Time or Scan Rate
  112
- To Prioritize the Dwell Times of the Problem Analytes
  112
- Narrowing the Mass Range
  113
- Adjusting the Transfer Line and Ion Source Temperature
  113
- Optimizing an SRM Method
  114
- Optimizing an NCI Tune
  114
  - To Optimize the CI Ion Volume Position Using Methane
    117
  - Saving a New NCI Tune File
    117
- Modifying an Automatic Tune
  118
  - Configuring General Tuning Parameters
    118
  - Starting Tune File
    119
  - Configuring the Ion Source Parameters
    120
  - Electron Energy
    121
  - Electron Lens Positive Voltage
    121
  - Electron Lens Negative Voltage
    121
  - Set Ion Source Temperature
    122
  - Configuring Tuning Targets
    122
  - Configuring the Detectors
    123
  - Set Initial Detector Gain
    123
  - Tune Detector
    123
  - Adjust Detector Sensitivity
    123
  - Setting Diagnostics
    124
  - Selecting Data Report Options
    124
  - Acquire Full-Scan Spectrum
    124
  - Renaming a Tune Type
    125
  - To Modify Advanced Tune Settings
    126
  - Changing a Tune File Name
    126
  - Tuning the Q1 Lenses
    126
  - Repeller
    127
  - Ion Guide Voltage
    127
  - Ion Guide RF
    127
  - Q1 Voltage
    127
  - Step
    128
  - Max Width
    128
  - Threshold
    128
  - On Error
    128
  - Configuring Q1 Resolution
    129
  - Tuning the Q3 Lenses
    130
  - Q3 Voltage
    130
  - Resolution
    130
  - To Configure the Resolution of Your Tune
    131
  - Configuring the Q3 Resolution
    132
  - Tune High Scan Rate
    132
- Computer Settings
  133
- To Use the Power Save Feature
  133
Chapter 6 Computer Settings

133
- System Requirements
  133
- Excluding the Xcalibur Directory from Virus Scan
  136
Chapter 7 Troubleshooting

137
- Diagnostics Checks
  138
- How to Know When Your System Needs Maintenance
  139
  - Diagnostics and Corrective Actions
    139
  - Common Contaminants
    140
- Investigating Baseline Issues
  141
  - Drifting Baseline
    141
  - Noisy Chromatographic Peaks
    142
- Investigating Peak Issues
  143
  - Troubleshooting Peak Issues in Your Data
    143
  - Broadening
    143
  - Fronting
    143
  - Tailing
    144
  - Ghost Peaks
    145
  - Missing Peaks
    145
- Investigating Results Issues
  146
  - Low Reproducibility of Peaks Area
    146
  - Poor Sensitivity
    147
  - Retention Times
    147
Index

149

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Thermo Scientific TSQ 8000 Preinstallation Manual

Thermo Scientific TSQ 8000 Preinstallation Manual (64 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 1.04 MB

Table of Contents

Table of Contents

7
- Preface
  
  13
  - About Your System
    13
  - Related Documentation
    14
  - System Requirements
    15
  - Safety and Special Notices
    15
    
    Special Notices
    15
    
    Safety Symbols and Signal Words
    15
  - Hydrogen Safety Precautions
    17
    
    Using Hydrogen with TSQ 8000
    18
    
    Hydrogen Connection Guidelines
    19
    
    Building
    19
    
    Purchasing Hydrogen
    20
    
    Properly Storing Hydrogen
    21
    
    Hydrogen Safety Codes, Standards and References
    23
  - Hazardous Substances Precautions
    24
    
    Biological Hazard Warning Note
    24
    
    Venting Toxic Gases
    25
  - Contacting Us
    25
- Site Preparation
  
  27
  - Chapter 1 Site Preparation
    27
  - Entrance Requirements
    28
Workbench and Space Requirements

29
- Foreline Pump
  30
- Tsq 8000 89 35 40 16 45
  30
- Lighting Requirements
  31
- Power Requirements
  31
  - Computer
    31
  - Monitor
    31
- Direct Probe Controller
  32
- Triplus 300 Headspace
  32
- Environmental Requirements
  35
- Gas Equipment Requirements
  37
  - GC Carrier Gas
    37
  - CI Gas
    38
  - Collision Gas
    39
  - Other Gas Specifications
    40
  - Using Hydrogen
    41
- Receiving Requirements
  41
- What Happens Next
  42

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