Thermo Scientific TSQ 8000 Manuals

Manuals and User Guides for Thermo Scientific TSQ 8000. We have 3 Thermo Scientific TSQ 8000 manuals available for free PDF download: Hardware Manual, User Manual, Preinstallation Manual

Thermo Scientific TSQ 8000 Hardware Manual (432 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 16 MB

Table of Contents
3
Preface

13
- About Your System
  13
- Related Documentation
  14
- System Requirements
  15
- Safety and Special Notices
  15
  - Special Notices
    15
  - Safety Symbols and Signal Words
    16
- Hydrogen Safety Precautions
  17
- Hazardous Substances Precautions
  24
  - Biological Hazard Warning Note
    24
  - Venting Toxic Gases
    25
- Contacting Us
  25
Chapter 1 Performing Routine Maintenance

27
Chapter 2 Troubleshooting

103
- Troubleshooting
  103
- Using Diagnostics
  104
  - Running a Diagnostic Tune
    107
- Investigating Communication Issues
  109
- Investigating Contamination Issues
  112
- Investigating Filament and Lens Control Issues
  115
- Investigating Temperature Issues
  116
  - Lens/Source Heater Does Not Heat
    117
  - Lens/Source Heater Overheats
    117
  - Transfer Line Does Not Heat
    117
  - Transfer Line Overheats
    117
- Investigating Vacuum Issues
  118
- Investigating Power Supply Issues
  121
  - TSQ 8000 Evo System Does Not Power on
    121
    
    Breaker
    121
  - RF DC Supply Is Outside the Acceptable Range
    121
- Investigating RF/DC Issues
  122
  - RF Dip Is Incorrect
    122
  - RF/DC System Check Diagnostic Fails
    122
- Investigating Sensitivity Issues
  123
- Investigating Stability Issues
  125
  - Mass Assignment Is Unstable
    125
  - Signal Response Is Unstable or Shows Unexpected Drop-Out
    125
- Investigating Tuning Issues
  126
- Contacting Technical Support
  129
- Advanced Troubleshooting
  131
Chapter 3 Advanced Troubleshooting

131
- Replacing Components of the Analyzer
  132
  - Analyzer Tray
    133
  - Ion Guide
    147
  - Q1 Entrance Lens and Q1 Entrance Lens Endcap
    152
  - Ion Guide Wire Set
    157
  - Q1 Quad, Q3 Quad, and Collision Cell Assemblies
    158
  - Quad 1 and Quad 3 Wire Sets
    162
  - Q3 Exit Lens Assembly
    165
- Replacing Components of the Ion Source
  167
  - Source Heater Block, Lens Heater Block, and Lens/Source Heater
    168
  - Source-Repeller Thumbscrews
    178
  - Thumbscrew-Repeller Spacers
    180
  - Insulating Spacers
    182
  - Repeller Plate
    185
  - Lens Heater Block Grounding Strap
    188
  - Lens Plate and Springs
    189
  - Source to Ion Guide Spacer
    191
  - Ion Source Cartridge
    196
  - Reinserting the Ion Source Cartridge
    213
- Replacing Components of the Source Exchange Tool
  220
- Replacing Components of the Vacuum Interlock
  224
- Replacing Components of the Manifold
  238
  - Manifold Door Hinge
    239
  - Front Manifold Plate
    245
  - Back Manifold Plate
    255
    
    Magnets
    258
    
    Shut down Your System by Following the Steps in System" on Page
    258
  - Vent Valve Knob and O-Ring
    260
  - Delivery Tubes
    261
  - Slide the Top Cover Panel Toward the Back of the Instrument and Lift It off
    261
- Replacing Components of the Electron Multiplier
  263
- Reinstalling the TSQ 8000 Evo System Software
  274
  - Updating the Firmware on the Instrument
    274
  - Upgrading Software on the Computer
    275
  - System Requirements
    276
  - Installing the Software Set
    277
- Replacing the Covers of the TSQ 8000 Evo Instrument
  280
- Replacing Components of the Front Door
  288
  - Front Door Hinges and Supports
    289
  - Front Door Latch
    291
  - Restarting the System
    292
- Replacing the Boards in the TSQ 8000 Evo Instrument
  293
  - Front and Rear RF Boards and Front and Rear Rod Driver Boards
    294
  - RF Board/Rod Driver Board Kits
    300
  - 4- Pin Feedthrough
    303
  - Lens Driver Board
    308
  - 20-Pin Feedthrough
    312
  - PC Communication Board, Controller Interface Board, and Support
    320
    
    Bracket
    320
  - Distribution Board
    326
  - Source Interface Board and Heat Shield
    340
  - Electrometer Board Cable
    342
  - Electrometer Board and Shield
    344
- Replacing the Power Supplies
  346
  - Power Module
    347
  - Dynode and Multiplier Power Supply
    351
- Replacing the Calibration Gas Components
  356
  - Calibration Gas Module
    357
  - Calibrant Reservoir Kit
    365
  - Gas Mixing Chamber
    367
  - Transfer Line
    368
- Replacing the Collision Gas Components
  372
- Replacing Fans and Filters
  380
  - Front Wire Mesh Filter
    382
  - Left Rear Wire Mesh Filter
    383
  - Chassis Cooling Fan and Fan Plenum
    384
  - Air Deflector
    390
  - Turbo Cooling Fan and Turbo Cooling Fan Filter
    392
- Replacing the Turbomolecular Pump
  400
- Convectron Gauge and Foreline Adapter with Hose
  406
Chapter 4 Upgrade Equipment

409
- Dust Filter
  410
- CI Reagent Gas Flow Module
  411
- CI Ion Volume
  419
- EI/CI Ion Volume
  420
- Ion Gauge and Tube Shield
  421
- Probe Controller
  424

Thermo Scientific TSQ 8000 User Manual (151 pages)

Mass Spectrometer

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 7 MB

Table of Contents
3
About Your System
9
Preface

9
Chapter 1 Introduction

23
Chapter 2 Changing the Column

37
Chapter 3 Tuning

53
- Tuning the Mass Spectrometer
  54
  - TSQ Series Dashboard
    54
  - Tuning Categories
    55
  - Tune Types
    55
  - EI Standard Tune
    55
  - EI Standard Quick Tune
    56
  - EI SRM Tune
    56
  - EI Tune Check
    56
  - EI Target Tune/Ei Initial Tune
    56
  - Fast Scan Tune
    57
  - CI- Tune
    57
  - CI+ Tune
    57
  - Displaying a Report
    58
  - Sample Tune Report
    59
  - Tune Report Options
    60
  - Printing a Tune Report
    61
- Updating Tunes for New RF Lens
  62
- Creating a Method
  67
  - Accessing the Method Editor
    67
Chapter 4 Creating a Method

67
Chapter 5 Optimizing Your Method

111
- Changing the Chromatographic Separation
  111
- Finding the Best Way to Make an Injection
  112
- Improving the Way You Prepare Samples
  112
- Changing the Dwell Time or Scan Rate
  112
- To Prioritize the Dwell Times of the Problem Analytes
  112
- Narrowing the Mass Range
  113
- Adjusting the Transfer Line and Ion Source Temperature
  113
- Optimizing an SRM Method
  114
- Optimizing an NCI Tune
  114
  - To Optimize the CI Ion Volume Position Using Methane
    117
  - Saving a New NCI Tune File
    117
- Modifying an Automatic Tune
  118
  - Configuring General Tuning Parameters
    118
  - Starting Tune File
    119
  - Configuring the Ion Source Parameters
    120
  - Electron Energy
    121
  - Electron Lens Positive Voltage
    121
  - Electron Lens Negative Voltage
    121
  - Set Ion Source Temperature
    122
  - Configuring Tuning Targets
    122
  - Configuring the Detectors
    123
  - Set Initial Detector Gain
    123
  - Tune Detector
    123
  - Adjust Detector Sensitivity
    123
  - Setting Diagnostics
    124
  - Selecting Data Report Options
    124
  - Acquire Full-Scan Spectrum
    124
  - Renaming a Tune Type
    125
  - To Modify Advanced Tune Settings
    126
  - Changing a Tune File Name
    126
  - Tuning the Q1 Lenses
    126
  - Repeller
    127
  - Ion Guide Voltage
    127
  - Ion Guide RF
    127
  - Q1 Voltage
    127
  - Step
    128
  - Max Width
    128
  - Threshold
    128
  - On Error
    128
  - Configuring Q1 Resolution
    129
  - Tuning the Q3 Lenses
    130
  - Q3 Voltage
    130
  - Resolution
    130
  - To Configure the Resolution of Your Tune
    131
  - Configuring the Q3 Resolution
    132
  - Tune High Scan Rate
    132
- Computer Settings
  133
- To Use the Power Save Feature
  133
Chapter 6 Computer Settings

133
- System Requirements
  133
- Excluding the Xcalibur Directory from Virus Scan
  136
Chapter 7 Troubleshooting

137
- Diagnostics Checks
  138
- How to Know When Your System Needs Maintenance
  139
  - Diagnostics and Corrective Actions
    139
  - Common Contaminants
    140
- Investigating Baseline Issues
  141
  - Drifting Baseline
    141
  - Noisy Chromatographic Peaks
    142
- Investigating Peak Issues
  143
  - Troubleshooting Peak Issues in Your Data
    143
  - Broadening
    143
  - Fronting
    143
  - Tailing
    144
  - Ghost Peaks
    145
  - Missing Peaks
    145
- Investigating Results Issues
  146
  - Low Reproducibility of Peaks Area
    146
  - Poor Sensitivity
    147
  - Retention Times
    147
Index

149

Thermo Scientific TSQ 8000 Preinstallation Manual (64 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 1 MB

Table of Contents

7
- Preface
  
  13
  - About Your System
    13
  - Related Documentation
    14
  - System Requirements
    15
  - Safety and Special Notices
    15
    
    Special Notices
    15
    
    Safety Symbols and Signal Words
    15
  - Hydrogen Safety Precautions
    17
    
    Using Hydrogen with TSQ 8000
    18
    
    Hydrogen Connection Guidelines
    19
    
    Building
    19
    
    Purchasing Hydrogen
    20
    
    Properly Storing Hydrogen
    21
    
    Hydrogen Safety Codes, Standards and References
    23
  - Hazardous Substances Precautions
    24
    
    Biological Hazard Warning Note
    24
    
    Venting Toxic Gases
    25
  - Contacting Us
    25
- Site Preparation
  
  27
  - Chapter 1 Site Preparation
    27
  - Entrance Requirements
    28
Workbench and Space Requirements

29
- Foreline Pump
  30
- Tsq 8000 89 35 40 16 45
  30
- Lighting Requirements
  31
- Power Requirements
  31
  - Computer
    31
  - Monitor
    31
- Direct Probe Controller
  32
- Triplus 300 Headspace
  32
- Environmental Requirements
  35
- Gas Equipment Requirements
  37
  - GC Carrier Gas
    37
  - CI Gas
    38
  - Collision Gas
    39
  - Other Gas Specifications
    40
  - Using Hydrogen
    41
- Receiving Requirements
  41
- What Happens Next
  42

Thermo Scientific Categories

Laboratory Equipment Measuring Instruments

Freezer Accessories

Refrigerator

More Thermo Scientific Manuals

Thermo Scientific TSQ 8000 Manuals

Thermo Scientific TSQ 8000 Hardware Manual (432 pages)

Table of Contents

Preface

Chapter 1 Performing Routine Maintenance

Chapter 2 Troubleshooting

Chapter 3 Advanced Troubleshooting

Chapter 4 Upgrade Equipment

Thermo Scientific TSQ 8000 User Manual (151 pages)

Table of Contents

Preface

Chapter 1 Introduction

Chapter 2 Changing the Column

Chapter 3 Tuning

Chapter 4 Creating a Method

Chapter 5 Optimizing Your Method

Chapter 6 Computer Settings

Chapter 7 Troubleshooting

Index

Thermo Scientific TSQ 8000 Preinstallation Manual (64 pages)

Table of Contents

Table of Contents

Preface

Site Preparation

Workbench and Space Requirements

Related Products

Thermo Scientific Categories