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Thermo Scientific TSQ Quantum XLS Ultra Manuals
Manuals and User Guides for Thermo Scientific TSQ Quantum XLS Ultra. We have
1
Thermo Scientific TSQ Quantum XLS Ultra manual available for free PDF download: User Manual
Thermo Scientific TSQ Quantum XLS Ultra User Manual (176 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 12.68 MB
Table of Contents
Table of Contents
9
Preface
13
Related Documentation
13
Safety and Special Notices
14
Contacting Us
15
Chapter 1 Introduction
17
Ionization Modes
19
Electron Ionization Mode
20
Chemical Ionization Mode
20
Ion Polarity Modes
21
Scan Modes
21
Q1MS and Q3MS Scan Modes
23
Product Scan Mode
23
Parent Scan Mode
24
Neutral Loss Scan Modes
25
Data-Dependent Scan Mode
27
Scan Types
28
Full Scan
28
Selected Ion Monitoring (SIM)
28
Selected Reaction Monitoring (SRM)
29
Highly-Selective Reaction Monitoring (HSRM)
29
Intelligent Selected Reaction Monitoring (Isrm)
29
Quantitation-Enhanced, Data-Dependent MS (QED MS)
30
Autosim
30
Data Types
30
Profile Data Type
30
Centroid Data Type
31
Mass/Charge Range
31
Chapter 2 Functional Description
33
Autosampler
34
Gas Chromatograph
35
Direct Sample Probes
35
Transfer Line
36
Mass Spectrometer
37
Controls and Indicators
38
EI/CI Ion Source
42
Inlet Valve
44
Ion Optics
45
Mass Analyzer
47
Ion Detection System
54
Vacuum System and Inlet Gasses Hardware
56
Electronic Assemblies
61
Data System
62
Computer Hardware
63
Data System/Mass Spectrometer/Gc Interface
63
Data System/Local Area Network Interface
63
Chapter 3 System Shutdown, Startup, and Reset
65
Shutting down the System in an Emergency
65
Placing the System in Standby Mode
67
Shutting down the System Completely
67
Starting up the System after a Complete Shutdown
69
Restoring Power to the TSQ Quantum XLS Series System
70
Starting up the GC
70
Starting up the Data System
70
Starting up the Mass Spectrometer
70
Starting up the Autosampler
72
Setting up Conditions for Operation
72
Resetting the Mass Spectrometer
73
Resetting the Data System
73
Turning off Selected Mass Spectrometer Components
74
Chapter 4 Tuning and Calibrating
77
Displaying the FC-43 Mass Spectrum
78
Running Auto Tune and Calibration
80
Saving the Tune and Calibration Report
83
Running Maintenance Tune
86
Creating a Quality Control (QC) Tune Report
87
Chapter 5 Changing Ionization Modes
89
Removing the Ion Volume
89
Installing the Ion Volume
96
Maintenance
99
Chapter 6 Maintenance
99
Cleaning Ion Source Components
101
Cleaning Ion Volumes
103
Cleaning the Lenses of the Ion Source
103
Replacing the Filament of the Ion Source
109
Completely Disassembling and Reassembling the Ion Source
111
Complete Disassembly and Reassembly of the Ion Source
112
Cleaning Stainless Steel Parts
114
Cleaning Non-Stainless Steel or Hybrid Parts
116
Maintaining the Forepump
117
Adding Calibration Compound
118
Replacing the Ball Valve Seal
121
Removing and Installing a GC Capillary Column
123
Removing a GC Capillary Column
123
Installing a GC Capillary Column
125
Chapter 7 Diagnostics and Troubleshooting
129
Diagnostics
129
Troubleshooting
130
Communication Issues
130
Contamination Issues
133
Filament and Lens Control Issues
135
Heated Zone Issues
136
High Vacuum Issues
137
Linearity Issues
139
Power Supply Issues
140
Sensitivity Issues
140
Stability Issues
143
Tuning Issues
144
Replacing Fuses
146
Replacing Pcbs and Power Supplies
146
Appendix A Using the Direct Sample Probe
147
Creating an Instrument Method
147
Creating a Sequence
150
Preparing the Probe and Inlet Valve
151
Preparing the Mass Spectrometer
151
Running the Sequence
153
Examining the Raw Data in Qual Browser
157
Removing the Probe
158
Appendix B Replaceable Parts and Consumables
161
EI/CI Ion Source Replaceable Parts
161
Miscellaneous Replaceable Parts and Consumables
163
Accessory Kit
164
Chemicals Kit
165
Index
167
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