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Thermo Scientific TSQ Series Manuals
Manuals and User Guides for Thermo Scientific TSQ Series. We have
3
Thermo Scientific TSQ Series manuals available for free PDF download: Hardware Manual, Pre-Installation Requirements Manual
Thermo Scientific TSQ Series Hardware Manual (122 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 14 MB
Table of Contents
Table of Contents
11
Cleaning
13
Reinstalling
13
Removing
13
About this Guide
15
Preface
15
Related Documentation
15
Safety and Special Notices
15
Safety Precautions
16
Level of Repair
17
Replaceable Parts
17
Service Philosophy
17
Solvent and Gas Purity Requirements
17
Contacting Us
18
Chapter 1 Introduction
19
Data Types
19
Ion Polarity Modes
19
Ionization Modes
21
Ion Polarity Modes
21
Scan Modes
21
Q1MS and Q3MS Scan Modes
22
Product Scan Mode
23
Parent Scan Mode
24
Neutral Loss Scan Modes
25
Data Dependent Scan Mode
26
Scan Types
27
Full Scan
27
Selected Ion Monitoring
27
Selected Reaction Monitoring
28
Autosim
28
Data Types
28
Profile Data Type
28
Centroid Data Type
28
Mass/Charge Range
29
Chapter 2 Functional Description
31
Autosampler
31
Figure
31
Autosampler
32
Functional Description
32
Syringe Pump
32
Vacuum System
32
Liquid Chromatograph
33
Syringe Pump
33
Divert/Inject Valve
34
Divert/Inject Valve
35
Mass Spectrometer
36
Controls and Indicators
36
Front Panel Leds
36
Vent Valve
38
API Source
39
Ion Source Interface
40
Tube Lens
40
Ion Optics
41
Q0 Ion Optics
41
Mass Analyzer
45
Ion Detection System
51
Conversion Dynode
51
Vacuum System and Inlet Gases Hardware
53
Vacuum Manifold
53
Auxiliary Gas Valve
53
Collision Gas Valve
53
Ion Gauge
53
Sheath Gas Valve
53
Vent Valve
53
Collision Cell Chamber
54
Electronic Assemblies
58
Data System
59
Computer Hardware
59
Data System / Mass Spectrometer / LC Interface
60
Data System / Local Area Network Interface
60
Printer
60
Chapter 3 System Shutdown, Startup, and Reset
63
Shutting down the System in an Emergency
63
Placing the System in Standby Condition
65
Shutting down the System Completely
66
Starting up the System after a Complete Shutdown
67
Starting up the LC
67
Starting up the Data System
67
Starting up
67
Starting up the Mass Spectrometer
68
Starting up the Autosampler
69
Setting up Conditions for Operation
69
Resetting the Mass Spectrometer
70
Resetting the Data System
70
Resetting the Data System by Using the Windows Shutdown and Restart Procedure
70
Resetting the Data System by Turning the Personal Computer off then on
71
Turning off Selected Mass Spectrometer Components
71
On/Off Status
72
Vacuum Service Switch
72
Vacuum Service Switch
73
Chapter 4 Daily Operation
75
Things to Do before Operating the TSQ System
75
Checking the Argon and Nitrogen Supplies
76
Checking the ESI Fused-Silica Sample Tube for Elongation
76
Checking the System Vacuum Levels
76
Things to Do after Operating the TSQ System
77
Flushing the Sample Transfer Line, Sample Tube, and API Probe
78
Placing the System in Standby Condition
79
Cleaning the Ion Sweep Cone and Ion Transfer Tube
79
Emptying the Solvent Waste Bottle
80
Chapter 5 Removing and Reinstalling the Ion Source Housing
81
Removing the Ion MAX or Ion MAX-S Ion Source Housing
81
Installing the Ion MAX or Ion MAX-S Ion Source Housing
83
Ion MAX and Ion MAX-S Housing Maintenance
84
Chapter 6 Maintenance
85
Frequency of Cleaning
87
Mass Spectrometer Maintenance Procedures
87
Maintaining the Ion Sweep Cone and Ion Transfer Tube
88
Removing and Cleaning the Ion Transfer Tube
88
Maintaining the Ion Source Interface Assembly
90
Shutting down and Venting the System
91
Removing the Ion MAX or Ion MAX-S Ion Source Housing
91
Removing the Ion Source Interface
91
Removing the S-Lens and Exit Lens (TSQ Vantage)
92
Cleaning the S-Lens and Exit Lens (TSQ Vantage)
93
Removing the Tube Lens and Skimmer (TSQ Quantum Access and TSQ Quantum Ultra)
94
Cleaning the Tube Lens and Skimmer (TSQ Quantum Access and TSQ Quantum Ultra)
95
Reinstalling the S-Lens and Exit Lens (TSQ Vantage)
95
Reinstalling the Tube Lens and Skimmer (TSQ Quantum Access and TSQ Quantum Ultra)
96
Reinstalling the Ion Source Interface Assembly
97
Reinstalling the Ion MAX or Ion MAX-S Ion Source Housing
97
Starting up the System
97
Cleaning the Q00 Ion Optics
97
Shutting down and Venting the System
98
Removing the Ion MAX-S Ion Source Housing
98
Removing the Ion Source Interface Assembly
98
Removing the Ion Optics Cage Assembly
98
Disassembling the Ion Optics Cage Assembly
102
Cleaning Q00 and L0
103
Reassembling the Ion Optics Cage Assembly
104
Reinstalling the Ion Optics Cage Assembly
105
Reinstalling the Ion Source Interface Assembly
106
Reinstalling the Ion MAX-S Ion Source Housing
106
Starting up the System
106
Maintaining the Forepump
107
Cleaning the Fan Filters
107
Chapter 7 Diagnostics and PCB and Assembly Replacement
109
Running the TSQ System Diagnostics
109
Replacing a Fuse
111
Replacing Pcbs and Power Supplies
111
Chapter 8 Replaceable Parts
113
MS Accessory Kit
113
TSQ Vantage Instrument Specific Accessory Kit
114
TSQ Quantum Ultra, Ultra AM, and Ultra EMR Instrument Specific Accessory Kit
114
TSQ Quantum Access Instrument Specific Accessory Kit
114
Fittings, Ferrules, and Sample Loops
115
Index
117
Tuning
122
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Thermo Scientific TSQ Series Hardware Manual (140 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 14 MB
Table of Contents
Table of Contents
13
Preface
17
Related Documentation
17
Safety and Special Notices
18
Safety Precautions
18
Solvent and Gas Purity Requirements
19
Service Philosophy
20
Level of Repair
20
Contacting Us
21
Chapter 1 Introduction
23
Ionization Modes
25
Ion Polarity Modes
25
Scan Modes
25
Q1MS and Q3MS Scan Modes
27
Product Scan Mode
27
Parent Scan Mode
28
Neutral Loss Scan Modes
29
Data Dependent Scan Mode
31
Scan Types
32
Full Scan
32
Selected Ion Monitoring
32
Selected Reaction Monitoring
33
Autosim
33
Data Types
33
Profile Data Type
34
Centroid Data Type
34
Mass/Charge Range
34
Chapter 2 Functional Description
35
Autosampler
36
Liquid Chromatograph
37
Syringe Pump
37
Divert/Inject Valve
38
Mass Spectrometer
40
Controls and Indicators
41
API Source
44
Ion Source Interface
44
Ion Optics
46
Mass Analyzer
50
Ion Detection System
57
Vacuum System and Inlet Gases Hardware
59
Electronic Assemblies
65
Data System
66
Computer Hardware
67
Data System / Mass Spectrometer / LC Communication, Contact Closure, and Line Power Connections
67
Data System / Local Area Network Interface
68
Printer
68
Chapter 3 System Shutdown, Startup, and Reset
71
Shutting down the System in an Emergency
71
Placing the System in Standby Condition
73
Shutting down the System Completely
74
Starting up the System after a Complete Shutdown
76
Starting up the LC
76
Starting up the Data System
76
Starting up the Mass Spectrometer
76
Starting up the Autosampler
77
Setting up Conditions for Operation
78
Resetting the Mass Spectrometer
79
Resetting the Data System
79
Resetting the Data System by Using the Windows Shutdown and Restart Procedure
80
Then on
80
Turning off Selected Mass Spectrometer Components
81
Chapter 4 Daily Operation
85
Things to Do before Operating the TSQ System
85
Checking the Argon and Nitrogen Supplies
86
Checking the ESI Fused-Silica Sample Tube for Elongation
86
Checking the System Vacuum Levels
86
Things to Do after Operating the TSQ System
88
Flushing the Sample Transfer Line, Sample Tube, and API Probe
88
Placing the System in Standby Condition
89
Cleaning the Ion Sweep Cone and Ion Transfer Tube
90
Emptying the Solvent Waste Bottle
90
Chapter 5 Removing and Reinstalling the Ion Source Housing
91
Removing the Ion Max or Ion Max-S Ion Source Housing
91
Installing the Ion Max or Ion Max-S Ion Source Housing
93
Ion Max and Ion Max-S Housing Maintenance
95
Chapter 6 Maintenance
97
Frequency of Cleaning
99
Maintaining the Ion Sweep Cone and Ion Transfer Tube
101
Removing and Cleaning the Ion Transfer Tube
101
Maintaining the Ion Source Interface Assembly
106
Shutting down and Venting the System
106
Removing the Ion Max or Ion Max-S Ion Source Housing
106
Removing the Ion Source Interface
107
Removing the S-Lens and Exit Lens (TSQ Vantage)
108
Cleaning the S-Lens and Exit Lens (TSQ Vantage)
109
Removing the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
109
Cleaning the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
110
Reinstalling the S-Lens and Exit Lens (TSQ Vantage)
111
Reinstalling the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
111
Reinstalling the Ion Source Interface Assembly
112
Reinstalling the Ion Max or Ion Max-S Ion Source Housing
112
Starting up the System
112
Cleaning the Q00 Ion Optics
113
Shutting down and Venting the System
113
Removing the Ion Max or Ion Max-S Ion Source Housing
113
Removing the Ion Source Interface Assembly
113
Removing the Ion Optics Cage Assembly
114
Disassembling the Ion Optics Cage Assembly
118
Cleaning Q00 and L0
119
Reassembling the Ion Optics Cage Assembly
120
Reinstalling the Ion Optics Cage Assembly
121
Reinstalling the Ion Source Interface Assembly
122
Reinstalling the Ion Max or Ion Max-S Ion Source Housing
122
Starting up the System
122
Maintaining the Forepump
123
Cleaning the Fan Filters
123
Chapter 7 Diagnostics and PCB and Assembly Replacement
125
Running the TSQ System Diagnostics
126
Replacing a Fuse
127
Replacing Pcbs and Power Supplies
127
Chapter 8 Replaceable Parts
129
MS Accessory Kit
129
TSQ Vantage Instrument Specific Accessory Kit
130
TSQ Quantum Ultra, Ultra AM, and Ultra EMR Instrument Specific
130
Accessory Kit
130
HESI-II Probe Kit
131
TSQ Quantum Access Instrument Specific Accessory Kit
131
TSQ Accurate Mass Calibration Compounds Kit
131
Fittings, Ferrules, and Sample Loops
131
Index
133
Thermo Scientific TSQ Series Pre-Installation Requirements Manual (50 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
11
Preface
13
Related Documentation
13
Safety and Special Notices
14
Contacting Us
14
Chapter 1 Introduction
17
Chapter 2 Site Preparation
19
Entrance
20
Space and Load Requirements
20
Telephone
24
Chapter 3 Operating Environment
25
Temperature
26
Humidity
27
Vibration
27
Lighting
27
Particulate Matter
27
Electrostatic Discharge
28
Chapter 4 Line Power
29
Quality of Power
31
Power Monitoring Devices
32
Power Conditioning Devices
32
Available Outlets
33
Connecting the TSQ Quantum XLS or TSQ Quantum GC Mass Spectrometer, GC, and Other Modules to Wall Outlets
35
Uninterruptible Power Supply
35
Technical Assistance
36
Chapter 5 Waste and Exhaust
37
Exhaust System
37
Solvent Waste
38
Chapter 6 Gas and Plumbing Requirements
39
Gases
40
Plumbing
40
Chapter 7 Installation
41
Preinstallation Survey
42
Installation Kits
43
Installation
44
Preventive Maintenance
44
Chapter 8 Instrument Arrival
45
Index
47
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