Micromeritics TriStar II 3020 Manuals

Manuals and User Guides for Micromeritics TriStar II 3020. We have 4 Micromeritics TriStar II 3020 manuals available for free PDF download: Operator's Manual, Installation Instructions And Checklist, Service Manual, Maintenance Instructions Manual

Micromeritics TriStar II 3020 Operator's Manual (439 pages)

Brand: Micromeritics | Category: Measuring Instruments | Size: 23 MB

Table of Contents
5
1 General Information

13
- Introduction
  13
- Organization of the Operator's Manual
  13
- Conventions
  15
- Equipment Description
  15
  - Krypton Option
    16
  - Vacuum Pump
    16
  - Degasser
    17
- Software
  17
  - User-Defined Reports
    17
    
    Report Features
    17
- Specifications
  18
2 User Interface

21
- Introduction
  21
- Instrument Components and Connectors
  21
  - Rear Panel
    23
  - Side Panel
    24
- Turning the Analyzer on and off
  24
  - Turning the Analyzer on
    24
  - Turning the Analyzer off
    25
- Using the Software
  25
  - Shortcut Menus
    25
  - Shortcut Keys
    26
  - Files
    27
    
    File Status and Description
    27
    
    File Name Conventions
    28
  - Menu Structure
    29
  - Main Menu Bar
    29
  - Window Menu
    30
  - Help Menu
    31
3 Operating Procedures

33
- Introduction
  33
- Specifying Sample Defaults
  33
  - Advanced Format
    34
  - Basic Format
    35
  - Restricted Format
    37
- Defining Sample Information Files
  38
- Defining Parameter Files
  42
  - Sample Tube
    43
  - Degas Conditions
    44
  - Analysis Conditions
    45
  - Adsorptive Properties
    46
  - Report Options
    47
- Preparing for Analysis
  49
- Performing an Analysis
  56
  - Sample Analysis
    57
  - Quickstart Analysis
    58
  - Krypton Analysis
    59
  - Blank Analysis
    60
- Generating Reports
  61
- Printing Files
  63
- Listing Files
  64
- Exporting Isotherm Data
  65
  - Format of Exported Data
    66
- Converting Files
  67
- Generating Graph Overlays
  69
  - Multiple Sample Overlays
    69
  - Multiple Graph Overlays
    73
4 Software and Setup Modifications

77
5 File Menu

111
- Introduction
  111
- Common Fields and Buttons - File Menu Options
  111
- Open
  114
- Save
  114
- Save as
  115
  - Save as (T-Curve or Alpha-S Curve)
    115
- Save All
  116
- Close
  116
- Close All
  116
- Print
  116
- List
  116
- Export
  116
- Convert
  117
- Exit
  117
- Sample Information Files
  118
- Sample Tube Files
  120
- Degas Conditions File
  121
- Analysis Conditions Files
  122
- Adsorptive Properties File
  134
- Report Options Files
  136
  - Summary Report
    138
  - Isotherm Report Options
    140
  - Bet/Langmuir Surface Area Report Options
    142
  - Freundlich Report Options
    145
  - Temkin Isotherm Report Options
    146
  - T-Plot Report Options
    148
  - Alpha-S Method
    151
  - F-Ratio Method
    152
  - BJH Adsorption/Desorption Report Options
    154
    
    Tabular Report Options
    156
    
    Plot Options
    158
  - Dollimore-Heal Adsorption/Desorption Report Options
    159
    
    Tabular Report Options
    163
    
    Plot Options
    163
  - DFT Pore Size Report Options
    164
  - DFT Surface Energy Report Options
    167
  - Dubinin Report Options
    167
    
    Tabular Report Options
    168
    
    Transformed Isotherm Plot Options
    169
    
    Pore Volume Options
    170
  - MP-Method Report Options
    171
    
    Tabular Report Options
    172
    
    Plot Options
    172
  - Options Report
    173
  - Sample Log Report
    173
  - Validation Report
    174
- Entered or Collected Data File
  175
6 Unit Menu

177
- Introduction
  177
- Common Fields and Buttons - Unit Menu Options
  178
- Sample Analysis
  178
- Quickstart Analysis
  181
- Krypton Analysis
  182
- Blank Analysis
  183
- Enable Manual Control
  184
  - Instrument Schematic Components
    185
  - System Valves
    186
  - Instrument Schematic Shortcut Menus
    187
- Show Instrument Schematic
  188
- Show Status
  189
- Show Instrument Log
  190
- Unit Configuration
  191
- Diagnostics
  192
- Calibration
  195
  - Zero Pressure
    195
  - Match Transducers
    196
  - Servo Valve
    196
  - Save to File
    197
  - Load from File
    198
- Service Test
  198
7 Reports Menu

199
- Introduction
  199
- Common Fields and Buttons - Reports Menu Options
  200
- Start Report
  200
- Close Reports
  201
- Open Report
  201
- SPC Report Options
  201
- Regression Report
  203
- Control Chart
  205
- Heat of Adsorption Report
  208
- Report Features and Shortcuts
  210
  - Report Header
    211
  - Report Tool Bar
    212
  - Report Shortcut Menus
    215
    
    Report Header Shortcuts
    215
    
    Tabular Reports Shortcuts
    215
    
    Graph Shortcuts
    217
  - Other On-Screen Features
    221
    
    Zoom Feature
    221
    
    Axis Cross-Hair
    221
- Report Examples
  222
  - Isotherm Linear Plot
    223
  - BET Surface Area Report
    224
  - BET Surface Area Plot
    225
  - T-Plot
    226
  - BJH Adsorption Cumulative Pore Volume
    227
  - BJH Adsorption DV/Dlog(W) Pore Volume
    228
8 Options Menu

229
- Introduction
  229
- Option Presentation
  229
- Sample Defaults
  230
  - Restricted Format
    230
- Units
  231
- Graph Grid Lines
  231
- Live Graph
  232
- Parameter Files Directory
  232
- Service Test Mode
  233
9 Troubleshooting and Maintenance

235
- Introduction
  235
- Troubleshooting
  235
- Preventive Maintenance
  237
  - Recovering from a Power Failure
    237
  - Lubricating Elevator Drive Assembly
    238
  - Cleaning the Analyzer
    238
  - Cleaning the Analysis Dewar
    238
  - Replacing Port Filter (Frit) and O-Ring
    239
  - Replacing the Sample Tube O-Ring
    240
  - Inspecting and Changing Vacuum Pump Oil
    241
    
    Inspecting the Oil
    241
    
    Changing or Adding Oil
    241
  - Replacing the Alumina in the Oil Vapor Trap
    244
  - Changing the Vacuum Pump Exhaust Filter
    248
- Performing a Leak Test
  249
- Connecting Gases
  251
- Specifying Gas Ports
  259
- Calibrating the System
  259
  - Zero Pressure
    260
  - Match Transducers
    260
  - Servo Valve
    261
10 Ordering Information

263
Forms

269
- Sample Data Worksheet
  271
Error Messages

273
- 2400 Series
  273
- 2500 Series
  282
- 4000 Series
  286
- 6000 Series
  300
Calculations

309
- Saturation Pressure
  309
- Quantity Adsorbed Calculations
  310
  - Free Space
    310
    
    Measured
    310
    
    Calculated
    311
- Thermal Transpiration Correction
  313
- BET Surface Area
  314
- Langmuir Surface Area
  315
- T-Plot
  316
- BJH Pore Volume and Area Distribution
  318
  - Explanation of Terms
    318
  - Calculations
    319
  - Compendium of Variables
    326
- Horvath-Kawazoe
  327
  - Slit Pore Geometry (Original HK
    327
  - Cylinder Pore Geometry (Saito/Foley
    328
  - Sphere Pore Geometry (Cheng/Yang
    329
  - Cheng/Yang Correction
    330
  - Interaction Parameter
    331
    
    Additional Calculations
    332
  - Interaction Parameter Components
    333
- Dubinin-Radushkevich
  335
- Dubinin-Astakhov
  337
- MP-Method
  341
- Freundlich Isotherm
  343
- Temkin Isotherm
  343
- DFT (Density Functional Theory
  344
  - The Integral Equation of Adsorption
    344
    
    Application to Surface Energy Distribution
    345
    
    Application to Pore Size Distribution
    345
  - Performing the Deconvolution
    346
    
    Regularization
    346
- SPC Report Variables
  347
  - Regression Chart Variables
    347
  - Control Chart Variables
    348
- Summary Report
  348
- References
  350
Ethernet Configuration

351
- Configuring the Ethernet Port
  351
  - Windows 7
    351
  - Windows Vista
    355
Free Space Correction

357
- Measure
  357
- Calculate
  358
- Enter
  358
Dft Models

359
- Models Based on Statistical Thermodynamics
  359
- Models Based on Classical Theories
  371
  - Surface Energy
    371
  - Pore Size
    371
  - Models Included
    372
    
    Kelvin Equation with Halsey Thickness Curve
    372
    
    Kelvin Equation with Harkins and Jura Thickness Curve
    373
    
    Kelvin Equation with Broekhoff-De Boer Thickness Curve
    374
- References
  375
Maintaining High Purity Gases

377
- Using Metal Gas Lines
  377
  - Removing Trapped Air
    377
    
    Purge Method
    378
    
    Evacuation Method
    379
Index

439

Micromeritics TriStar II 3020 Installation Instructions And Checklist (74 pages)

SURFACE AREA AND POROSITY ANALYZER

Brand: Micromeritics | Category: Measuring Instruments | Size: 8 MB

Contact Us

3
About this Manual

4
- Table of Contents
  5
1 Overview

7
- Prepare for Installation
  7
- Dewar Precautions
  8
2 Equipment Installation

9
3 Application Installation

11
4 Analyzer Preparation

25
- Manifold Evacuation
  25
- Specify Unit Selections
  27
- Gas Connections
  28
5 Operational Verification

39
6 Installation Checklists

55
- Exceptions
  61
- Signatures
  62
- Final Documentation
  62
A Run Conditions a

63
- Manual Blank Run Conditions a
  65
- Carbon Reference Material Run Conditions a
  67
B Worksheets B

71
- Sample Data Worksheet B
  72
- User Information Worksheet B
  73

Micromeritics TriStar II 3020 Service Manual (48 pages)

Brand: Micromeritics | Category: Measuring Instruments | Size: 1 MB

Table of Contents
3
1 General Information

5
- Organization of the Manual
  5
- Using this Manual
  6
2 Functional Description

7
- Overview
  7
- New Product Features
  8
  - Cabinetry & Sample Chamber
    8
  - Interior Modules
    8
  - Software
    8
- Instrument Components
  9
- Cabinetry/Sample Chamber
  9
  - Top Panel
    9
  - Front
    9
  - Instrument Back
    10
  - Side Panels
    11
- Interior Modules
  12
  - Gas Entrance Manifold
    12
  - Dosing Volume Manifold
    12
  - Sample Analysis Manifold
    13
- Schematic Board & Software
  14
- Printed Circuit Boards (Pcbs)
  15
  - Analysis Transducer Interface PCB
    15
  - Card Cage
    15
    
    Dsp-Isa Cpu
    16
    
    Digital Interface
    16
    
    Backplane
    16
- Power Module
  17
3 The Analysis Sequence

19
- Analysis Technique
  20
- Analysis Sequence
  21
4 Preinstallation

27
6 Operator Training

31
7 Maintenance Documents

33
8 Calibration Procedure

35
9 Mechanical and Electrical Drawings

37
- Mechanical
  37
- Electrical
  37
10 Service Parts

39
11 Software

43
12 Operator's Manual

45
13 Service Training

47

Micromeritics TriStar II 3020 Maintenance Instructions Manual (42 pages)

Brand: Micromeritics | Category: Measuring Instruments | Size: 5 MB

Micromeritics Categories

Measuring Instruments Laboratory Equipment Industrial Equipment Test Equipment Recording Equipment

More Micromeritics Manuals

Micromeritics TriStar II 3020 Manuals

Micromeritics TriStar II 3020 Operator's Manual (439 pages)

Table of Contents

1 General Information

2 User Interface

3 Operating Procedures

4 Software and Setup Modifications

5 File Menu

6 Unit Menu

7 Reports Menu

8 Options Menu

9 Troubleshooting and Maintenance

10 Ordering Information

Forms

Error Messages

Calculations

Ethernet Configuration

Free Space Correction

Dft Models

Maintaining High Purity Gases

Index

Micromeritics TriStar II 3020 Installation Instructions And Checklist (74 pages)

Table of Contents

Contact Us

About this Manual

1 Overview

2 Equipment Installation

3 Application Installation

4 Analyzer Preparation

5 Operational Verification

6 Installation Checklists

A Run Conditions a

B Worksheets B

Micromeritics TriStar II 3020 Service Manual (48 pages)

Table of Contents

1 General Information

2 Functional Description

3 The Analysis Sequence

4 Preinstallation

6 Operator Training

7 Maintenance Documents

8 Calibration Procedure

9 Mechanical and Electrical Drawings

10 Service Parts

11 Software

12 Operator's Manual

13 Service Training

Micromeritics TriStar II 3020 Maintenance Instructions Manual (42 pages)

Table of Contents

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