Micromeritics TRISTAR II PLUS Manuals

Manuals and User Guides for Micromeritics TRISTAR II PLUS. We have 2 Micromeritics TRISTAR II PLUS manuals available for free PDF download: Operator's Manual, Pre-Installation Manual

Micromeritics TRISTAR II PLUS Operator's Manual

Micromeritics TRISTAR II PLUS Operator's Manual (310 pages)

SURFACE AREA AND POROSITY ANALYZER

Brand: Micromeritics | Category: Measuring Instruments | Size: 16 MB

Table of Contents

About this Manual

6
General Safety

7
- Table of Contents
  11
1 Analyzer Components for Tristar II Plus

17
2 About the Software

27
- Menu Structure
  28
- Common Fields and Buttons
  29
- File Status, Description, and Location
  32
- Keyboard Shortcuts
  34
- Option Presentation
  36
- Libraries
  38
- Methods
  39
- Configure the Analyzer
  41
  - Specify Gas Ports and Unit Configuration
    41
  - Unit Selection
    42
- Instrument Status
  43
  - Show Dashboard
    43
  - Show Instrument Log
    45
  - Show Instrument Schematic
    47
  - Show Status
    48
- Convert Files
  48
- Export Files
  49
- List Files
  50
- Software Uninstall
  51
- Software Updates
  51
- Software in 21CFR11 Environments
  53
  - Uninstall Software in 21CFR11 Environments
    56
3 Sample Files

57
- Create Sample Files
  58
- Open a Sample File
  61
- Manually Enter Data
  63
4 Parameter Files

69
- Adsorptive Properties
  70
- Analysis Conditions
  73
- Degas Conditions
  81
- Report Options
  84
- Sample Tube
  86
5 Degassing

89
- Degas on the Smart Vacprep
  89
- Transfer a Degassed Sample to an Analysis Port
  89
6 Perform an Analysis

93
- Dewar Precautions
  93
  - For Glass Dewars
    94
- Prepare for Analysis
  95
  - Clean and Label Sample Tubes
    95
  - Create the Sample File
    97
  - Determine the Sample Mass
    97
  - Degas the Sample
    99
  - Sample Tube Installation
    100
  - Fill and Install the Dewar
    103
- Perform a Krypton Analysis
  105
- Perform a Quickstart Analysis
  107
- Perform a Sample Analysis
  109
- Perform a Sample Tube Free Space Analysis
  113
- Perform an Empty Tube Analysis
  115
- Perform a Reference Material Analysis
  116
7 About Reports

117
- Start Reports
  117
- Heat of Adsorption Report
  118
- SPC Report
  120
- Regression Report
  121
- Control Chart Report
  123
- Microactive Reports
  126
- Interactive Reports
  127
- Evaluate Report Results
  128
- Report Features and Shortcuts
  134
- Graph Features and Shortcuts
  139
- Graph and Sample Overlays
  143
- Report Examples
  151
  - BET Report
    151
  - BET Surface Area Plot
    152
  - BJH Adsorptive Cumulative Pore Volume
    153
  - BJH Desorption Cumulative Pore Volume
    154
  - Isotherm Linear Plot
    155
  - Isotherm Log Report
    156
  - T-Plot
    157
8 Selected Report Options

159
- Advanced Reports - Python Module
  159
- Alpha-S Method Report
  162
- BET Surface Area Report
  164
- BJH Adsorption/Desorption Report
  166
- DFT Pore Size Report
  172
- DFT Surface Energy Report
  175
- Dollimore-Heal Adsorption/Desorption Report
  176
- Dubinin Report
  180
- F-Ratio Method Report
  185
- Freundlich Report
  187
- Horvath-Kawazoe Report
  189
- Isotherm Report
  193
- Langmuir Report
  195
- MP-Method Report
  197
- NLDFT Advanced PSD Report
  201
- Options Report
  205
- Sample Audit Trail Report
  206
- Summary Report
  207
- T-Plot Report
  209
- Temkin Report
  212
- Validation Report
  214
9 Diagnostics

215
- Show All Readings
  215
- Start Diagnostic Test
  215
10 Calibration

217
- Match Transducers
  218
- Pressure Offset
  219
- Servo Valve
  220
- Save Calibration to File
  220
- Load Calibration from File
  221
11 Troubleshooting

223
- Power
  225
- Guidelines for Connecting Gases
  226
  - Replace a Gas Cylinder
    227
  - Clean and Verify the Gas Line
    231
- Enable Manual Control
  233
- Perform a Leak Test
  234
- Preventive Maintenance
  236
  - Check and Clean the Dewar
    237
  - Clean the Instrument
    238
  - Clean the Gas Delivery Tubes
    238
  - Lubricate the Elevator Drive Assembly
    238
  - Power Instrument on and off
    239
  - Sample Port Frit Replacement
    240
  - Sample Tube O-Ring Replacement
    241
- Recover from a Power Failure
  242
- Service Test Mode
  243
- Oil-Based Vacuum Pump
  243
- Parts and Accessories
  243
- Advanced Reports a
  246
  - Scripts a
    248
  - Python Reports a
    250
  - Acquire Basic Information a
    254
  - Acquire Report Results a
    256
  - Acquire Overlay Sample Data a
    258
  - Enable the Use of Overlay Data a
    260
B DFT Models

275
C Free-Space Correction

293

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Micromeritics TRISTAR II PLUS Pre-Installation Manual

Micromeritics TRISTAR II PLUS Pre-Installation Manual (18 pages)

Brand: Micromeritics | Category: Measuring Instruments | Size: 0 MB

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