Injector Program Lines - Agilent Technologies G1323B User Manual

12 Running an Injector Program
Entering Injector Program Settings

Injector Program Lines

Table 6
derivatization reaction.
Table 6
Line
1
2
3
4
5
6
7
8
9
152
describes the program lines which will complete the required
Injector Program Lines
Function Parameters
DRAW 2 µl (AMOUNT) from Air
(SOURCE)
DRAW 1 µl (AMOUNT) from vial
1(SOURCE)
WASH in vial 2 (VIAL), 1 time
(Cycles)
DRAW 2 µl (AMOUNT) from sample
(SOURCE)
WASH in vial 2 (VIAL), 1 time
(CYCLE)
DRAW 1 µl (AMOUNT) from vial 1
(SOURCE)
MIX 6 µl (AMOUNT) in seat
(SOURCE), at 500 µl/min
(SPEED), 8 times (REPEAT)
WAIT 0.5 minutes (WAIT)
INJECT
Comment
Draw 2 µl from air into the needle
capillary, to separate the mobile phase
sitting in the capillary from the sample.
Draw 1µl from derivatization reagent
from vial #1 in the autosampler tray into
the needle capillary.
Wash the needle tip in the wash vial #2.
Add 2 µl of the sample in the
autosampler tray to the derivatization
volume already in the needle capillary.
Wash the needle tip in the wash vial #2.
Add 1 µl of derivatization reagent from
vial #1 in the autosampler tray to the
derivatization reagent and sample
already in the needle capillary.
Mix 6 µl with a repetition of 8 times at a
speed of 500 µl/minute in the seat.
Wait for 0.5 minute for the mixture to
completely react.
Inject the mixture and start the analysis.
1200 Series Handheld Control Module Users's Guide