Hitachi ZA3000 Series Manuals

Manuals and User Guides for Hitachi ZA3000 Series. We have 1 Hitachi ZA3000 Series manual available for free PDF download: Instruction Manual

Hitachi ZA3000 Series Instruction Manual (522 pages)

POLARIZED ZEEMAN ATOMIC ABSORPTION SPECTROPHOTOMETER

Brand: Hitachi | Category: Measuring Instruments | Size: 6.48 MB

Preface
3
About this Manual
3
Safety Summary
4
Definition of Alert Symbol and Signal Word
4
General Safety Guidelines
5
Warning Indications in this Manual
8
List of WARNING Indications
9
Beware of High Voltage
9
Explosion Due to Backfiring
9
Explosion Due to Acetylide Formation
9
Explosion Due to Perchloric Acid
10
List of CAUTION Indications
11
Strong Magnetic Fields
11
Beware of Intense Light
11
Do Not Touch Hot Parts
11
List of CAUTION Indications
12
Malfunction by Wrong Gas Type
12
Deterioration of Burner Chamber by Chemicals
12
Strong Magnetic Fields
12
Table of Contents
13
Start up
18
Check of Instrument
18
Mounting of Hollow Cathode Lamps
19
Supply of Gases
21
Power-On
22
Power-On of Exhaust Duct
23
Basic Operation Flow
23
Startup of Software
25
Startup of Atomic Absorption Spectrophotometer Program
25
Setting the Instrument Online
26
When
26
At Startup] Is Selected
27
When
28
At Startup] Is Not Selected
28
Fundamental Operation of Software Windows
29
Clicking and Double-Clicking
29
Names and Functions of Window Elements
29
How to Input Measurement Conditions
31
Opening Files
34
Saving Files
35
Asking for Help
37
Measurement with Conditions Input
40
Generation of Measurement Conditions
40
Displaying the Method Window
41
Setting Measurement Mode
41
Setting Analyte Element
41
Instrument Setup
43
Setting Analytical Conditions
47
Setting Standards Table
50
Setting Sample Table
54
Setting QC Conditions
61
Setting Report Format
62
Check of Analytical Conditions
62
Verification of Measurement Condition
64
Monitoring of Measurement Process
65
Wavelength Adjustment
69
Check of Optical Axis of Atomizer
71
Supply of Cooling Water
71
Ignition of Flame
72
Start of Measurement
75
Preparation for Measurement
76
Start of Measurement
77
Change of Monitor Graph Display
79
Trace
79
Grid
79
Signals/Change Scale
80
Y-Axis Auto-Scale
82
Reset Scale
82
Print Graph
82
Copy Graph
82
Clearing of Monitor Graph
83
Changing the Display of a Profile Graph
83
Display Mode
83
Auto Scale
83
Other Menus
83
Changing the Display of a Working Curve Graph
84
Termination of Measurement
85
Checking the Result
88
Data Table
89
Error Marks
91
Correction of Operator, Analysis Name, and Comment
92
Profile Graph
92
Working Curve Graph
97
Displaying Details of Working Curve
98
Saving and Printout of Result
101
Saving the Data
101
Printout of Result
103
Printing Format of Profile
106
Analysis and Recalculation of Data
109
Deleting and Restoring Data
109
Exchanging Data
110
Changing Calculation Mode
110
Changing the Concentration Correction Factor
110
Changing Sample Name
110
Changing Sample Unit
111
Changing Digits below Decimal Point
111
Editing Reagent Name
111
Restoring the Recalculated Results
111
Detailed Display of Profile Graph
111
Specifying a Sample Blank
111
Use of the Data in Other Applications
113
Output in Text Format or Excel Format
113
Customize by MS Excel
113
Customizing the Template
114
Using Various Functions
117
Various Measurement Methods
117
Absorbance Mode
118
Standard Addition Method
119
Simple Standard Addition Method
122
Correction of Working Curve Drift (Reslope Function)
125
Measurement under the same Conditions (Copy Method)
127
Using an Existing Working Curve
128
Insertion and Remeasurment of Sample
130
Remeasurement
131
Auto-Start
132
Auto-Flame off
134
Emission Measurement
135
Using Monitor Measuring Function
138
Setting Automatic Start
141
Power/Water Saving by Eco Mode
143
Canceling Eco Status
144
Restoring Data Lost Due to a Power Failure
147
Using the Qc Functions
148
Using Correlation Coefficient of Working Curve (Check Working Curve)
150
Contents to be Printed on the Report
151
Using the Working Curve Range and RSD (Check Sample)
152
Setting Procedure
154
Using the QC Sample (Check QC Sample)
154
Changing the Analyte Element for Continuous Measurement
158
Terminating Measurement
159
Closing AAS Program
160
Closing Operations
162
Turning off Power Supply of PC and Instrument
162
Final Steps
162
Instrument Diagnosis
163
Items to be Prepared by the User
164
Diagnostic Items
165
Operation
166
Preparation
166
Setting of Conditions
166
Start of Measurement
171
Check of Instrument
199
Mounting Hollow Cathode Lamp
200
Supply of Gases
202
Graphite Cuvette Installation
203
Selection of Graphite Cuvette
203
Mounting of Graphite Cuvette
205
Power-On
208
Power-On Exhaust Duct
209
Basic Operation Flow
210
Startup of Software
211
Startup of Atomic Absorption Spectrophotometer Program
211
Setting the Instrument Online
212
When
212
Fundamental Operation of Software Windows
215
Clicking and Double-Clicking
215
Names and Functions of Window Elements
215
How to Input Measurement Conditions
217
Opening Files
219
Saving Files
221
Asking for Help
222
Measurement with Conditions Input
225
Generation of Measurement Conditions
225
Displaying the Method Window
226
Setting Measurement Mode
226
Setting Analyte Element
226
Instrument Setup
228
Setting Sample Table
245
Setting QC Conditions
265
Setting Report Format
265
Check of Analytical Conditions
266
Verification of Measurement Condition
268
Monitoring of Measurement Process
271
Wavelength Adjustment
277
Preparation for Autosampler
279
Supply of Rinse Water
279
Flowing Rinse Water
279
Nozzle Adjustment
279
Flowing of Cooling Water
285
Cleaning of Graphite Cuvette
286
Memorizing Optical Temperature Control Equation
287
Start of Measurement
288
Interrupting a Measurement
290
Change of Monitor Graph Display
291
Trace
292
Grid
292
Signal/Change Scale
292
Y-Axis Auto-Scale
294
Reset Scale
294
Print Graph
294
Copy Graph
294
Clearing the Monitor Graph
295
Changing the Display of a Profile Graph
295
Display Mode
295
Auto Scale
295
Other Menus
295
Changing the Display of a Working Curve Graph
296
Menus
296
Termination of Measurement
296
Checking the Result
299
Data Table
301
Error Marks
302
Correction of Operator, Analysis Name and Comment
303
Profile Graph
304
Working Curve Graph
310
Displaying Details of Working Curve
311
Saving and Printout of Result
314
Saving the Data
314
Printout of Result
316
Printing Format of Profile
319
Analysis and Recalculation of Data
322
Deleting and Restoring Data
322
Exchanging Data
323
Changing Calculation Mode
323
Changing the Concentration Correction Factor
323
Changing Sample Name
323
Changing Sample Unit
324
Changing Digits below Decimal Point
324
Editing Reagent Name
324
Restoring the Recalculated Results
324
Detailed Display of Profile Graph
324
Specifying a Sample Blank
324
Use of the Data in Other Applications
326
Customize by MS Excel
326
Customizing the Template
327
Using Various Functions
330
Various Measurement Methods
330
Absorbance Mode
332
Standard Addition Method (Ex-Furnace Addition)
337
Simple Standard Addition Method (In-Furnace Addition)
341
Simple Standard Addition Method (Ex-Furnace Addition)
345
Using Stock Standard Solutions
349
Addition of Matrix Modifier
351
Drying of Matrix Modifier
352
Sequential Injection of Samples
353
Twin Injection
355
Cleaning Cuvette
358
Sample Bumping Detection
361
Correction of Working Curve Drift (Reslope Function)
362
Concentrating Sample
364
Diluting Sample
365
Heating Injection of Sample
367
Measurement under the same Conditions (Copy Method)
368
Using an Existing Working Curve
369
Insertion and Remeasurement of Sample
371
Remeasurement
374
Setting Automatic Start
375
Power/Water Saving by Eco Mode
377
Restoring Data Lost Due to a Power Failure
380
Using the Qc Functions
381
Using Correlation Coefficient of Working Curve (Check Working Curve)
383
Setting Procedure
384
Setting Procedure
385
Using the Working Curve Range and RSD (Check Sample)
385
Using Sensitivity Variations of Standard Solution (Check STD)
388
Setting Procedure
390
Using the QC Sample (Check QC Sample)
390
Contents to be Printed on the Report
393
Using Spike Recovery (Check Recovery)
393
Setting Procedure
393
Contents to be Printed on the Report
396
Displaying QC Message
397
Terminating or Continuing Measurement
398
Continuing Measurement with Element Change
398
Terminating Measurement
399
Closing AAS Program
400
Closing Operations
402
Instrument
402
Final Steps
402
Measurement in Manual Mode
403
Setting of Conditions
403
Preparation for Measurement
404
Flowing of Cooling Water
405
Cleaning of Graphite Cuvette
406
Memorizing Optical Temperature Control Equation
407
Start of Measurement
408
Starting Measurement
409
Interrupting a Measurement
410
Terminating or Continuing Measurement
412
Change
412
Terminating Measurement
412
Stopping the Cooling Water
412
Instrument Diagnosis
413
Items to be Prepared by User
414
Diagnosis Items
415
Operation
416
Preparation
416
Setting of Conditions
416
Start of Measurement
421
Check and Saving of Diagnostic Result
421
Output of Diagnostic Result
424
Temperature Program Development Function
426
Setting of Temperature Program Test Conditions
427
Start of Measurement
443
Heating Temperature Graph
444
Judgment Standards for Automatic Generation of Temperature Program
445
Reflecting on Analysis Conditions
447
Troubleshooting
450
Installation (for Customer's Reference)
477
Location
477
Installation Table and Layout
477
Site Requirements
477
Required Equipment
478
Power Supply
478
Gases
478
Check of Standard Parts
479
Items to be Prepared by User
479
Assembly
479
Setting of Three-Liquid Flow Channel
480
Installation of Separator
482
Setting of Four-Liquid Flow Channel
484
Installation of Atomizer
488
Piping
490
Power Distribution and Grounding
492
Function
493
Name and Function for each Part
493
Front Panel
493
Pump Unit
494
Rear Panel
494
Principle
495
Specifications
496
Operation
497
Reagents
497
Sample
498
Setting of Reagents
500
Setting of Conditions
500
Setting of Absorption Cell
501
Startup of HFS-4
505
Measurement
507
Closing Operations
508
Measurement with Autosampler
509
Principle
510
Sample
510
Measurement Using Four Liquids
510
Preparation for Measurement Using Four Liquids
513
Operation of Measurement Using Four Liquids
515
Maintenance
517
Replacement of Pump Tube
517
Replacement of Fuse
518
Troubleshooting
519
Replacement Parts
521
Consumables
521
Parts to be Replaced Periodically
521
Maintenance Parts
522

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Hitachi ZA3000 Series Instruction Manual (522 pages)

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