Re-Calibrating With Multiple Groups Of Standards - Agilent Technologies InfinityLab LC Series User Manual

4 Running Multiple-Vial Analyses

Re-calibrating With Multiple Groups of Standards

Re-calibrating With Multiple Groups of Standards

There are two different types of sample, A and B that need to be analyzed. The
analysis for sample type A requires a 5 μl injection and a stoptime of 8 minutes.
The analysis of sample type B requires a 2 μl injection and a stoptime of 5
minutes.
For sample type A:
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For sample type B:
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The samples use METH2 and the calibration standards use METH3. These
methods contain the same analytical parameters and differ only in the analysis
stoptime.
The example assumes that the sequence table is empty. If the sequence table is
not empty, use the Delete button to delete all lines or use File> New.
1 Select the Sequence screen.
2 Move to line 1 and press Insert.
3 Select Method and then move to METH1 and press Load.
G4208A User's Guide
there are 3 calibration standards of different concentrations and 6 samples,
each sample must be analyzed once,
the calibration standards must be analyzed in duplicate and re- analyzed after
every 2 samples,
C1 C2 C3 S7 S8 C1 C2 C3 S9 S10 C1 C2 C3 S11 S12 C1 C2 C3
The calibration standards of type A are in positions 1, 2 and 3 of the
autosampler tray and the 6 sample vials are in positions 7 to 12, and
the samples and the calibration standards use the same method called
METH1.
there are 3 calibration standards of different concentrations and 9 samples,
each sample must be analyzed once,
the calibration standards must be analyzed twice and re- analyzed after every
3 samples,
C1 C2 C3 S13- S15 C1 C2 C3 S16- S18 C1 C2 C3 S19- S21 C1 C2 C3
the calibration standards of type B are in positions 4, 5 and 6 of the
autosampler tray and the 9 sample vials are in positions 13 to 21, and
the samples and calibration standards of type B use different methods.
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