Page 1 Agilent InfinityLab LC Series 1260 Infinity II Binary Pump User Manual InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 2 12.211 (Technical Data) and 12.212 (Computer Software) and, for the Depart- ment of Defense, DFARS 252.227-7015 (Technical Data - Commercial Items) and DFARS 227.7202-3 (Rights in Commer- cial Computer Software or Computer Software Documentation). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 3 In This Guide... This manual covers the Agilent InfinityLab LC Series 1260 Infinity II Binary Pump (G7112B). Introduction This chapter gives an introduction to the module and an instrument overview. Site Requirements and Specifications This chapter provides information about site requirements and specifications for the binary pump.
Page 4 This chapter provides detailed technical information about your binary pump. LAN Configuration This chapter provides information on connecting the module to the Agilent ChemStation PC. Appendix This chapter provides addition information on safety, legal and web. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 5: Table Of Contents
When to Use a Vacuum Degasser When to Use the Active Seal Wash Option When to Use the Low Volume Mixer When to Remove Damper and Mixer How to Optimize the Compressibility Compensation Setting InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 6 What Are Error Messages General Error Messages Module Error Messages Test Functions and Calibration (System) Pressure Test Valve Test Binary Pump Solvent Compressibility Calibration Pump Elasticity Calibration Pump Leak Rate Test InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 7 Exchange the Seal Wash Cartridge Replace Leak Handling System Parts Exchange the Outlet Valve Installation of the Solvent Selection Valve Upgrade Kit Exchange the Solvent Selection Valve Replacing Module Firmware InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 8 Analog Cables Remote Cables CAN/LAN Cables RS-232 Cable Kit Agilent 1200 Module to Printer Hardware Information Firmware Description Electrical Connections Interfaces Setting the 6-bit Configuration Switch Early Maintenance Feedback Instrument Layout InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 9 Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) Manual Configuration Appendix General Safety Information Waste Electrical and Electronic Equipment (WEEE) Directive Radio Interference Sound Emission Agilent Technologies on the Internet InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 10: Introduction
Principle of Operation Product Description Features Overview of the Hydraulic Path Leak and Waste Handling Leak Sensor Waste Concept This chapter gives an introduction to the module and an instrument overview. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 11: Instrument And Operation
(optional) allows to form binary mixtures (isocratic or gradient) from one of two solvents per channel. Active seal wash (optional) is available for use with concentrated buffer solutions. Figure 1 Overview of the binary pump InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 12: Principle Of Operation
Inlet valve Damper Pressure sensor Outlet valve Outlet valve Mixer Pump head A Pump head B Mixing chamber Figure 2 The hydraulic path of the Binary Pump with damper and mixer InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 13 Pump head A Pump head B Mixer Mixing chamber Figure 3 The hydraulic path of the Binary Pump with bypassed damper and mixer For pump specifications, see “Performance Specifications” on page 30. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 14: Product Description
High gradient performance - even at low % B and narrow-bore flow rates. • Integrated 2-channel-degasser. • Fast and precise gradients using LC/MS, as well as UV-only systems. • Fully exploits the speed and separation potential of Poroshell. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 15: Overview Of The Hydraulic Path
The first piston has a stroke volume in the range of 20 µL to 100 µL depending on the flow rate. The microprocessor controls all flow rates in a range InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 16 During the drawing stroke of the first piston, the second piston delivers the drawn volume into the system. For pump specifications, see “Performance Specifications” on page 30. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 17 Solvent compressibility calibrations acquired with a miscalibrated pump will work, but they are not transferable to other pumps. A correct pump elasticity calibration is an essential prerequisite for successful solvent compressibility calibrations. Calibrate the pump elasticity correctly.  InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 18 For compatibility with older methods from G1312A Binary Pumps, the previous one-point compressibility compensation is available, too. However, since the compressibility is a non-linear function, one single compressibility value per solvent will only give good results at one particular pressure. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 19 The stroke volume for the pump is by default set to AUTO mode. This means that the stroke is optimized for the flow rate in use. A change to larger stroke volumes is possible but not recommended. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 20: Leak And Waste Handling
Introduction Leak and Waste Handling Leak and Waste Handling The Agilent InfinityLab LC Series has been designed for safe leak and waste handling. It is important that all security concepts are understood and instructions are carefully followed. The solvent cabinet is designed to store a maximum volume of 8 L solvent. The maximum volume for an individual bottle stored in the solvent cabinet should not exceed 2 L.
Page 21 Introduction Leak and Waste Handling Figure 6 Infinity II Leak Waste Concept (Flex Bench installation) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 22 Introduction Leak and Waste Handling Figure 7 Infinity II Single Stack Leak Waste Concept (bench installation) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 23: Leak Sensor
The solvent DMF (dimethylformamide) leads to corrosion of the leak sensor. The material of the leak sensor, PVDF (polyvinylidene fluoride), is incompatible with DMF.  Do not use DMF as mobile phase. Check the leak sensor regularly for corrosion.  InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 24: Waste Concept
1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports (5043-1221) for optimal and safe waste disposal. If you decide to use your own waste solution, make sure that the tubes don't immerse in the liquid. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 25: Site Requirements And Specifications
Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information about site requirements and specifications for the binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 26: Site Requirements
Make sure the power connector of the instrument can be easily reached  and unplugged. Provide sufficient space behind the power socket of the instrument to  unplug the cable. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 27 Never use a power cord other than the one that Agilent shipped with this  instrument. Never use the power cords that Agilent Technologies supplies with this  instrument for any other equipment. Never use cables other than the ones supplied by Agilent Technologies ...
Page 28 If your module was shipped in cold weather, leave it in its box and allow it to  warm slowly to room temperature to avoid condensation. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 29: Physical Specifications
Up to 3000 m (9842 ft) Safety standards: Overvoltage category II, Pollution degree 2 For indoor use only IEC, EN, CSA, UL ISM Classification ISM Group 1 Class B According to CISPR 11 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 30: Performance Specifications
400 µL mixer), dependent on back pressure tracer) Low delay volume configuration:120 µL Composition range Settable: 0 – 100 % Recommended: 1 – 99 % or 5 µL/min per channel, whichever is greater InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 31 Electronic records of maintenance and errors. Housing All materials are recyclable InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 32: Using The Pump
How to Prevent and/or Reduce the Algae Problem Prevent Blocking of Solvent Filters Checking the Solvent Filters Cleaning the Solvent Filters Normal Phase Applications This chapter explains the operational parameters of the Binary Pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 33: Magnets
Using the Pump Magnets Magnets Magnets in doors of pumps, autosamplers, detectors, and fraction collectors. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 34: Turn On/Off
Using the Pump Turn on/off Turn on/off This procedure exemplarily shows an arbitrary LC stack configuration. Power switch: On InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 35 Using the Pump Turn on/off Turn instrument On/Off with the control software. Power switch: Off InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 36: Status Indicators
5. Resident mode (blinking) - for example, during update of main firmware. 6. Bootloader mode (fast blinking). Try to re-boot the module or try a cold-start. Then try a firmware update. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 37: Best Practices
Flush system with water to remove buffer. • Remove all samples from the sampler and store according to good laboratory practice. • Use recommended solvents to store the system. • Power off the system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 38: Prepare The Pump
Label bottles correctly with bottle content, and filling date / expiry date. • Use solvent inlet filters. • Reduce risk of algae growth: use brown bottles for aqueous solvents, avoid direct sunlight. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 39: Leak And Waste Handling
Agilent Information Center or via the Internet. For details on correct installation, see separate installation documentation. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 40: Hints For Successful Use Of The Binary Pump
After changing the piston seals, apply the seal wear-in procedure (see “Seal Wear-in Procedure” on page 133). • Place the aqueous solvent on channel A and the organic solvent on channel B. The default compressibility settings are set accordingly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 41: Setting Up The Pump With The G4208A Instant Pilot
Pilot G4208A User's Guide (G4208-90006). Details about setting up module specific parameters can be found in the Instant Pilot online help. The pump parameters are described in detail in “Overview” on page 42. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 42: Setting Up The Pump With The Instrument Control Interface
Parameters described in following sections are offered by the instrument control interface and can usually be accessed through Agilent instrument control software. For details, please refer to manuals and online help of respective user interfaces. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 43: Setup Of Basic Pump Parameters
Display There are three ways to display the timetable: • in tabular form • as flow/pressure graph • as solvent percentage plot Values can only be changed in tabular view. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 44: Pump Control
C AU T I O N This can result in a rapid and uncontrolled pressure increase.  To prevent harm to the column, open the purge valve until the initialization is finished. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 45: Data Curves
The pressure data curve is generated from the pressure sensor readings, while NOTE %A, %B and flow are calculated from the method settings of the pump. For details, please refer to the online help or manual of your instrument control software. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 46: Bottle Filling
If this option is checked, the pump will turn off before air is aspirated. However, off... the residual solvent volume has been calculated for 1 L solvent bottles and may be too small for large bottles or other vessels. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 47: Solvent Information
Pump head (body) Pistons Sapphire Piston seals/wash seals PTFE, SST (reversed phase) or UHMW-PE, SST (normal phase) Pressure sensor Purge valve SST, gold, PTFE, ceramic Damping unit SST, gold Capillaries/fittings Tubings PTFE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 48 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 49 PEEK capillaries keeps the flow path free of steel and ensures pressure stability up to 600 bar. If in doubt, consult the available literature about the chemical compatibility of PEEK. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 50 It can be corroded by strong bases (e.g. hydroxide solutions > 10 %, diethylamine). It is not recommended for the use with fluoric acid and fluorides. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 51 For example, a 1 % solution of acetic acid in methanol will attack steel. • Solutions containing strong complexing agents (for example, EDTA, ethylene diamine tetra-acetic acid). • Mixtures of carbon tetrachloride with isopropanol or THF. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 52 It can be corroded by complexing cyanides and concentrated acids like aqua regia. Zirconium Oxide (ZrO Zirconium Oxide is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 53 Sapphire, Ruby and Al -based ceramics Sapphire, ruby and ceramics based on aluminum oxide Al are inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 54: Algae Growth In Hplc Systems
Use the amber solvent bottle (Solvent bottle, amber, 1000 mL (9301-6526)) supplied with the instrument for your aqueous mobile phase. • If possible add a few mg/L sodium azide or a few percent organic solvent to the aqueous mobile phase. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 55: Prevent Blocking Of Solvent Filters
• Place a layer of argon on top of your solvent. • Avoid exposure of the solvent bottle to direct sunlight. Never use the system without solvent filter installed. NOTE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 56: Checking The Solvent Filters
Thoroughly flush the filter with HPLC-grade water (remove all nitric acid, some capillary columns can be damaged by nitric acid). • Replace the filter. Never use the system without solvent filter installed. NOTE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 57: Normal Phase Applications
Do not use normal phase valves in applications running with aqueous  solutions. The N-Valves have been tested successfully in using hexane at pressures below 100 bar; heptane can be used as a substitute for neurotoxic hexane. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 58 1290 Infinity Quat Inlet Valve Type N (G4204-60122) Outlet valves Outlet Valve Type N/SFC 1290 Infinity Outlet Valve Type N (G4220-60128) (G1312-60167) Seals PE seals (pack of 2) (0905-1420) Wash Seal PE (0905-1718) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 59: Optimizing Performance
How to Optimize the Compressibility Compensation Setting Solvent Compressibility Calibration Optimization of Legacy Compressibility Settings This chapter gives information on how to optimize the performance of the Binary Pump under special operational conditions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 60: When To Use A Vacuum Degasser
Priming is usually done by pumping at a high flow rate (3 – 5 mL/min). Alternatively, a syringe can be used to draw the solvent through the (empty) degasser if the pump does not aspirate the solvent by itself. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 61: When To Use The Active Seal Wash Option
The operation of the peristaltic pump can be controlled from the data system or the Instant Pilot. For adding a seal-wash option, please contact your local Agilent Technologies service representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 62: When To Use The Low Volume Mixer
The Low volume mixer ( 200 µL) (5067-1565) is designed for use with the Agilent InfinityLab LC Series 1260 Infinity II Binary LC System in low delay volume mode. This configuration is typically used for 2.1 mm i.d., 1.8 µm particle size columns, where emphasis is put on S/N ratio.
Page 63: When To Remove Damper And Mixer
For applications that require lowest delay volume (for example, fast gradient methods or gradient applications with low flow rates), damper and mixer can be bypassed. Standard configuration Low delay volume configuration Figure 9 Flow path modifications of the Binary Pump InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 64: Convert The Binary Pump To Low Delay Volume Mode
Disconnect fitting A from outlet 1 of the mixer. Connect fitting A to port 2 of the pressure sensor. Seal port 1 of the mixer with a plastic blank nut. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 65: How To Optimize The Compressibility Compensation Setting
Solvent Compressibility Calibration Unlisted or premixed solvents can be calibrated with the Solvent Compressibility Calibration function. For a detailed description, see “Binary Pump Solvent Compressibility Calibration” on page 100. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 66: Optimization Of Legacy Compressibility Settings
10. The compressibility compensation setting that generates the smallest pressure ripple is the optimum value for your solvent composition. 6 Repeat step 1 through step 5 for the B channel of your binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 67 How to Optimize the Compressibility Compensation Setting Table 8 Solvent Compressibility Solvent (pure) Compressibility (10 /bar) Acetone Acetonitrile Benzene Carbon tetrachloride Chloroform Cyclohexane Ethanol Ethyl acetate Heptane Hexane Isobutanol Isopropanol Methanol 1-Propanol Toluene Water InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 68: Troubleshooting And Diagnostics
Troubleshooting and Diagnostics Overview of the Module’s Indicators and Test Functions User Interfaces Agilent Lab Advisor Software Overview of the troubleshooting and diagnostic features. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 69: Overview Of The Module's Indicators And Test Functions
(i.e. the high pressure flow path between pump and column). After exchanging flow path components (e.g. pump seals or injection seal), use this test to verify the system is pressure tight, see “(System) Pressure Test” page 93. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 70 When a problem with the pump is suspected, use this test to help troubleshoot the pump and its pumping performance, see “Pump Leak Rate Test” on page 104. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 71: User Interfaces
Depending on the user interface, the available tests vary. Some descriptions are only available in the Service Manual. Test Instant Pilot G4208A Agilent Lab Advisor Pressure Test Valve Test Solvent compressibility calibration Pump elasticity calibration InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 72: Agilent Lab Advisor Software
The tests and diagnostic features that are provided by the Agilent Lab Advisor software may differ from the descriptions in this manual. For details, refer to the Agilent Lab Advisor software help files. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 73: Error Information
Degasser: Vacuum cannot be maintained Degasser: limit not reached This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 74: What Are Error Messages
In all cases, error propagation is done via the CAN bus or via an APG/ERI remote cable (see documentation for the APG/ERI interface). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 75: General Error Messages
Check the vacuum degasser for an error The degasser failed to generate sufficient condition. Refer to the Service Manual for the vacuum for solvent degassing. degasser or the pump that has the degasser built-in. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 76: Remote Timeout
Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective mainboard in another module. determine which module or modules are not recognized by the system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 77: Leak
If there are still signs of a leak, exchange the valve, or outlet valve. appropriate seal (purge valve, active inlet valve, outlet valve). Exchange the pump seals. Defective pump seals. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 78: Leak Sensor Open
Leak sensor incorrectly routed, being representative. pinched by a metal component. Please contact your Agilent service Power switch assembly defective representative. Please contact your Agilent service Cable or contact problem. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 79: Compensation Sensor Open
Probable cause Suggested actions Please contact your Agilent service Defective power switch assembly representative. Please contact your Agilent service Loose connection between the power switch representative. board and the mainboard InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 80: Fan Failed
Please contact your Agilent service Defective fan. representative. Please contact your Agilent service Defective mainboard. representative. Please contact your Agilent service Improperly positioned cables or wires representative. obstructing fan blades. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 81: Module Error Messages
(autosampler), column frits and capillaries with small internal diameters (e.g. 50 µm ID). Please contact your Agilent service Defective pressure sensor. representative. Please contact your Agilent service Defective mainboard. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 82: Pressure Below Lower Limit
-120 mV across the pressure sensor. Probable cause Suggested actions Please contact your Agilent service Pressure sensor disconnected representative. Please contact your Agilent service Defective pressure sensor representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 83: Valve Failed
Please contact your Agilent service Connection cable (inside instrument) not representative. connected. Please contact your Agilent service Connection cable (inside instrument) representative. defective. Exchange the solvent selection valve. Solvent selection valve defective. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 84: Electronic Fuse Of Ssv Open
Defective active inlet valve. again, exchange the active inlet valve. Please contact your Agilent service Defective connection cable (front panel to representative. main board). Please contact your Agilent service Defective mainboard. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 85: Motor-Drive Power
Please contact your Agilent service Defective pump drive assembly. representative. Please contact your Agilent service Defective mainboard. representative. Exchange restriction capillary. Restriction capillary blocked at pre-mixing union. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 86: Encoder Missing
Probable cause Suggested actions Please contact your Agilent service Defective or disconnected pump encoder representative. connector. Please contact your Agilent service Defective pump drive assembly. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 87: Servo Restart Failed
Exchange the (passive or active) inlet valve. Blocked (passive or active) inlet valve. Please contact your Agilent service Defective pump drive assembly. representative. Please contact your Agilent service Defective mainboard. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 88: Pump Head Missing
Irregular or sticking drive movement. pistons, and internal components for signs of wear, contamination or damage. Exchange components as required. Please contact your Agilent service Defective pump drive assembly. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 89: Index Adjustment
Probable cause Suggested actions Please contact your Agilent service Disconnected or defective encoder cable. representative. Please contact your Agilent service Defective pump drive assembly. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 90: Initialization Failed
Measured pressure is higher than 32000 hPa Probable cause Suggested actions Please contact your Agilent service Degasser sensor defect representative. Please contact your Agilent service Degasser sensor not connected to representative. mainboard. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 91: Degasser: Vacuum Cannot Be Maintained
Please contact your Agilent service Liquid in degasser tubing. representative. Please contact your Agilent service Leak in degasser tubing or chamber. representative. Please contact your Agilent service Degasser vacuum pump defect. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 92: Test Functions And Calibration
Pump Leak Rate Test Running the Test Evaluating the Results Potential Causes of Leak Rate Test Failure This chapter explains all test functions that are available for the binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 93: (System) Pressure Test
When the system pressure reaches 600 bar, the pump continues to pump at a flow rate that keeps the pressure constant. The flow that is needed to keep the pressure constant is directly translated into a leak rate. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 94: Positioning The Blank Nut
Pressure Test again. If the test passes, the defective component is located after the blank nut. Confirm the diagnosis by placing the blank nut immediately after the suspected component. The diagnosis is confirmed if the test fails. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 95: Running The System Pressure Test
An error is caused by the abnormal termination during the operation of the test whereas a failure of a test indicates that the test results were not within the specified limits. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 96 Tighten the fitting or exchange the capillary. Damaged pump seals or pistons. Run the valve test to identify the defective component. Loose purge valve. Tighten the purge valve nut (14 mm wrench). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 97 Potential Cause (Column Compartment) Potential Cause (Column Compartment) Corrective Action Loose or leaky fitting. Tighten or exchange the fitting or capillary. Rotor seal (column switching valve). Exchange the rotor seal. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 98: Valve Test
The procedure from step 1 is repeated on pump head B. Step 3 The data from step 1 and 2 are evaluated. In case test failed, a conclusion about the defective part is made. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 99: Running The Valve Test
Make sure to release the pressure by opening the purge valve when the test has NOTE completed. Otherwise the pump may generate an overpressure error. Evaluating the Results Refer to the help file of the Agilent Lab Advisor for further details. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 100: Binary Pump Solvent Compressibility Calibration
The compressibility data set for this solvent is stored in an XML-file on the desktop. It can be shared with other InfinityLab LC Series binary pumps via the controlling data system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 101: Running The Solvent Compressibility Calibration
2 Start the test and follow the instructions. Make sure to release the pressure by opening the purge valve when the test has NOTE completed. Otherwise the pump may generate an overpressure error. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 102: Pump Elasticity Calibration
Solvent compressibility calibrations acquired with a miscalibrated pump will work, but they are not transferable to other pumps. A correct pump elasticity calibration is an essential prerequisite for successful solvent compressibility calibrations.  Calibrate the pump elasticity correctly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 103: Running The Pump Elasticity Calibration
2 Start the test and follow the instructions. Make sure to release the pressure by opening the purge valve when the test has NOTE completed. Otherwise the pump may generate an overpressure error. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 104: Pump Leak Rate Test
1 Select the Pump Leak Rate Test from the Test Selection menu. 2 Start the test and follow the instructions. Make sure to release the pressure by slowly opening the purge valve when the NOTE test has finished. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 105: Evaluating The Results
If any of the leak rates exceeds 3 µL/min, the test will fail. to column Damper Outlet valve Purge valve Inlet valve to waste Seals Pump chamber 2 Pump chamber 1 Piston 1 Piston 2 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 106: Potential Causes Of Leak Rate Test Failure
Tighten or replace blank nut Blank nut not installed tightly Replace outlet valve Outlet valve leaking (read below) Inspect piston, replace piston and/or seal Leak at piston 2 or seal in chamber 2 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 107 Probable cause Suggested actions Replace the part which has failed and re-run the Leak at outlet valve test. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 108: Maintenance
Replace Leak Handling System Parts Exchange the Outlet Valve Installation of the Solvent Selection Valve Upgrade Kit Exchange the Solvent Selection Valve Replacing Module Firmware This chapter describes the maintenance of the module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 109: Introduction To Maintenance
These procedures are described in “Overview of Maintenance and Simple Repairs” on page 113. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 110: Cautions And Warnings
The volume of substances should be reduced to the minimum required  for the analysis. Do not operate the instrument in an explosive atmosphere.  InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 111 If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 112: Cleaning The Module
Drain all solvent lines before opening any connections in the flow path.  A solution of 70 % isopropanol and 30 % water might be used if the surface of the NOTE module needs to be disinfected. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 113: Overview Of Maintenance And Simple Repairs
“Exchange the Active Inlet Valve (AIV) or its Cartridge” on page 134 Pump head, see “Maintenance of a Pump Head with Seal Wash” on page 127 Solvent selection valve, see “Exchange the Solvent Selection Valve” on page 145 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 114: Maintenance Procedures
Pressure ripple unstable, run Pump Leak Rate Test for verification “Exchange the Solvent Selection Valve” If internally leaking Cross port flow page 145 If solenoid is defective Error message “Valve Failed” InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 115: Remove And Install Doors
The figures shown in this procedure exemplarily show the Infinity II Multisampler NOTE module. The principle of how to remove and/or install doors works in the same way for all Infinity II modules. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 116 Press the release buttons and pull the front door out. For the Installation of the front door. Insert the hinges into their guides and move the door in until the release buttons click into their final position. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 117: Exchange The Purge Valve Frit Or The Purge Valve
Using the 14 mm wrench, unscrew the purge valve and capillary from the purge valve. Disconnect the waste remove it from the purge valve holder. tube. Beware of leaking solvents due to hydrostatic pressure. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 118 (slit in frit points to the front). NOTE Seal cap Before reinstallation always check the gold seal in the seal cap. A deformed seal cap should be exchanged. Frit InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 119 The rubber o-ring might break.  Anticipate the correct position of the connections before tightening the valve. Tighten the purge valve and reconnect outlet capillary and waste tubing. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 120: Replace The O-Ring On The Purge Valve
Use an optional solvent shutoff valve or lift up solvent filters in solvent reservoirs for avoiding leakages. • Remove the purge valve from the pump head. Disassemble the purge valve. Remove the old o-ring from the purge valve. Clean the purge valve parts. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 121 Reinstall the seal cap including the gold seal. pump. The o-ring will take damage. NOTE Before reinstallation always check the gold seal in the seal cap. A deformed seal cap should be exchanged. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 122: Remove The Pump Head Assembly
A is fitted with the purge valve. The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 123 Using a 4 mm hexagonal key stepwise loosen and Unplug the active inlet valve cable from the connector. remove the two pump head screws. Remove the pump head assembly from the module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 124: Maintenance Of A Pump Head Without Seal Wash
A is fitted with the purge valve. The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 125 Using the steel side of the insert tool, carefully remove layers: clean the piston surface with abrasive paper and the seal from the pump housing. rinse with 2-propanol. Replace piston if scratched. Piston Surface InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 126 10 Insert the pistons and carefully press them into the seals. 11 Tighten the lock screw. 12 Install the pump head, see “Reinstall the Pump Head Assembly” on page 131. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 127: Maintenance Of A Pump Head With Seal Wash
A is fitted with the purge valve. The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 128 Lift the housing away from the pistons. Check the piston surface and remove any deposits or layers: clean the piston surface with abrasive paper and rinse with 2-propanol. Replace piston if scratched. Piston Surface InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 129 12 Place the support rings on the piston housing. Note the ring. Use a matching orientation of gasket and support correct position of the pins on the support ring. ring. Put the seal holder on top of the gasket. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 130 14 Insert the pistons and carefully press them into the housing. seals. 15 Tighten the lock screw. 16 Install the pump head, see “Reinstall the Pump Head Assembly” on page 131. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 131: Reinstall The Pump Head Assembly
Slide the pump head assembly onto the pump drive. Using a 4 mm hexagonal key, tighten the pump head Reconnect the active inlet valve cable to the connector. screws stepwise with increasing torque. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 132 Maintenance Reinstall the Pump Head Assembly Reconnect all tubings and capillaries. Close the doors. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 133: Seal Wear-In Procedure
Reconnect the intake tubing to the solvent selection valve and the connecting tube from the solvent selection valve (if installed) to the AIV. 7 Purge your system with the solvent used for your next application. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 134: Exchange The Active Inlet Valve (Aiv) Or Its Cartridge
C AU T I O N Overtightening will destroy the active inlet valve cartridge. Tighten the active inlet valve properly.  Open the doors. Unplug the active inlet valve cable from the connector. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 135 Screw the new valve into the pump head. With the Position the valve so that the solvent inlet tube 14 mm wrench, turn the nut until it is hand tight. connection points towards the front. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 136 After an exchange of the valve it may be required to pump several mL of the NOTE solvent used in the current application before the flow stabilizes at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 137: Exchange The Seal Wash Cartridge
Remove the wash solvent tubings from the support ring Unclip the peristaltic pump cartridge from the module outlet and from the adapter leading to the waste bottle. housing and remove it. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 138 Connect the peristaltic pump tubes to the support rings the pump motor and push the plastic clips into the outlet and to the adapter leading to the waste bottle. module housing. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 139: Replace Leak Handling System Parts
(2.). Install the Leak Adapter by pressing it into the Main Insert the Tubing (approximately 85 mm required for Cover. replacement) between Leak Adapter outlet and Leak Panel. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 140 Maintenance Replace Leak Handling System Parts Close the doors. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 141: Exchange The Outlet Valve
Unscrew the valve with the 14 mm wrench and remove capillary from the outlet valve. it from the pump body. NOTE Do not disassemble the outlet valve, as this can damage the valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 142 Maintenance Exchange the Outlet Valve Reinstall the outlet valve and tighten it using a torque Reconnect the capillary. wrench (approx.12 Nm). approx. 12 Nm InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 143: Installation Of The Solvent Selection Valve Upgrade Kit
Guide the SSV cable through the slots in the distance connection socket inside (behind the pump front metal sheet and route it through the slot in the pump front panel). metal panel to the internal connection socket. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 144 Before using of the system with a new installed valve it may be required to pump NOTE several mL of solvent to get the flow stabilized at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 145: Exchange The Solvent Selection Valve
Place the bottles back into the solvent cabinet. Using a screwdriver, loosen the holding screws of the Carefully pull the valve holder out. valve holder. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 146 Bend the cable at the connector of the new valve. Guide the cable and connector into the hole and push the connector into the socket. Exchange the defective solvent selection valve. 10 Tighten the screws of the valve holder. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 147 After an exchange of the valve it may be required to pump several mL of solvent NOTE before the flow stabilizes at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 148: Replacing Module Firmware
Agilent web. http://www.agilent.com/en-us/firmwareDownload?whid=69761 2 For loading the firmware into the module follow the instructions in the documentation. Module Specific Information There is no specific information for this module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 149: Parts And Materials For Maintenance
HPLC System Tool Kit Active Seal Wash Option Solvent Cabinet Bottle Head Assembly Accessory Kit Cover Parts This chapter lists all parts and tools that are required for maintenance and simple repairs. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 150: Hydraulic Path With Solvent Selection Valve
Capillary, ST, 0.17 mm x 900 mm SI/SX 5064-5444 Peristaltic pump cartridge, silicone tubing 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m for seal wash option 5062-2461 Waste tube, 5 m (reorder pack) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 151 Parts and Materials for Maintenance Hydraulic Path with Solvent Selection Valve Figure 11 Hydraulic Path with Solvent Selection Valve InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 152: Hydraulic Path Without Solvent Selection Valve
Capillary, ST, 0.17 mm x 900 mm SI/SX 5065-4445 Peristaltic pump with PharMed tubing 5062-2461 Waste tube, 5 m (reorder pack) 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m for seal wash option InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 153 Parts and Materials for Maintenance Hydraulic Path without Solvent Selection Valve Figure 12 Hydraulic Path without Solvent Selection Valve, with Active Seal Wash InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 154: Pump Head Assembly Without Seal Wash
Lock screw 12 a G1312-60025 Active inlet valve body, without cartridge 12 b G1312-60020 Cartridge for active inlet valve 600 bar G1312-23201 Adapter 0515-2118 Pump head screw (M5, 60 mm) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 155 Parts and Materials for Maintenance Pump Head Assembly Without Seal Wash 12 a,b Figure 13 Pump Head Assembly Without Seal Wash InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 156: Pump Head Assembly With Seal Wash Option
Lock screw G1311-25200 Pump chamber housing G1312-60025 Active inlet valve body, without cartridge G1312-60020 Cartridge for active inlet valve 600 bar G1312-23201 Adapter 0515-2118 Pump head screw (M5, 60 mm) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 157 Parts and Materials for Maintenance Pump Head Assembly with Seal Wash Option 16 a,b Figure 14 Pump Head Assembly with Seal Wash Option InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 158: Outlet Valve
Parts and Materials for Maintenance Outlet Valve Outlet Valve Item Description G1312-60067 Outlet valve (standard) OR 2 G1312-60167 Outlet valve (type N/SFC) Figure 15 Outlet valve InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 159: Purge Valve Assembly
Purge Valve Assembly Purge Valve Assembly Item Description G7111-60061 Purge valve 01018-22707 PTFE frits (pack of 5) 5067-4728 Seal cap 5067-6595 1260 PV O-ring FKM 5/pack Figure 16 Purge Valve Assembly InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 160: Active Inlet Valve Assembly
Active Inlet Valve Assembly Active Inlet Valve Assembly Item Description G1312-60025 Active inlet valve body, without cartridge G1312-60020 Cartridge for active inlet valve 600 bar Figure 17 Active Inlet Valve Assembly InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 161: Hplc System Tool Kit
0100-1710 (Mounting tool for flangeless nut) 0100-1681 (Adapter luer/barb) 5023-2499 (Hex Key Set) 01018-23702 (Seal Insert tool) 5043-1361 5067-6127 (Blank Nut V) (Hex Key Set Driver) 5023-2653 (Hex Key 3/32“) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 162: Active Seal Wash Option
1520-0260 Shock mount 1540-0455 Edge protector 5041-2120 Folding box 5065-4445 Peristaltic pump with PharMed tubing 5042-6422 Tubing Connector, PP 5065-9943 Stepper Motor for the Peristaltic Pump G3010-01203 RFI Strip 10×30 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 163: Solvent Cabinet
Parts and Materials for Maintenance Solvent Cabinet Solvent Cabinet Description 5067-6871 Solvent Cabinet Kit For details refer to: Usage Guideline for the Solvent Cabinet (01200-90150) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 164: Bottle Head Assembly
5063-6599 Tube screw (10/Pk) Wire marker 5062-2483 Tube PTFE 1.5 mm x 5 m, 3 mm od 5062-8517 Inlet filter adapter (4/Pk) 5041-2168 Solvent inlet filter, 20 µm pore size InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 165: Accessory Kit
5500-1169 Y Tube Connector ID 6.4 5500-1155 Tube Connector, 90 degree, ID 6.4 5043-1372 Tubing Connector Leak 3-1 5043-1373 Tubing Connector Leak Cap 0890-1195 Flexible sleeving 1.45 mm/2.5 mm, PTFE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 166: Cover Parts
Door Assembly Infinity 180 Left 5043-1354 Name Plate 1290 Infinity 2 G7104-68713 Cabinet Kit 180 Infinity II (includes sides, bottom, top, leak adapter top and status indicator insert) Figure 18 Cover Parts InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 167: Identifying Cables
Cable Overview Analog Cables Remote Cables CAN/LAN Cables RS-232 Cable Kit Agilent 1200 Module to Printer This chapter provides information on cables used with the Agilent InfinityLab LC Series modules. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 168: Cable Overview
Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure NOTE proper functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent 35900A A/D converter 01046-60105 Analog cable (BNC to general purpose, spade lugs)
Page 169 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m USB cables Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 170: Analog Cables
The other end depends on the instrument to which connection is being made. Agilent Module to 35900 A/D converters p/n 35900-60750 35900 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 171 Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 172: Remote Cables
NOT USED pink SHUT DOWN blue START PREPARE black 1wire DATA violet DGND grey-pink +5V ERI out red-blue PGND white-green PGND brown-green +24V ERI out white-yellow +24V ERI out yellow-brown InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 173 5188-8045 ERI to APG (Connector D_Subminiature 15 pin (ERI), Connector D_Subminiature 9 pin (APG)) p/n 5188-8045 Pin (ERI) Signal Pin (APG) Active (TTL) Start Request Stop Ready High Power on High Future Shut Down Start Prepare Ground Cable Shielding InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 174 Ground Cable Shielding One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 175 Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink Not connected Yellow Power on High Ready High Green Stop Black Start request InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 176: Can/Lan Cables
CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 177: Rs-232 Cable Kit
It is also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 178: Agilent 1200 Module To Printer
To connect a USB Flash Drive use a USB OTG cable with Mini-B plug and A socket. Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 179: Hardware Information
ERI (Enhanced Remote Interface) USB (Universal Serial Bus) Setting the 6-bit Configuration Switch Special Settings Early Maintenance Feedback Instrument Layout This chapter provides detailed technical information about your binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 180: Firmware Description
APG/ERI remote, • error handling, • diagnostic functions, • or module specific functions like • internal events such as lamp control, filter movements, • raw data collection and conversion to absorbance. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 181 Main and resident firmware must be from the same set. Main FW update Main System Resident System Resident FW Update Figure 19 Firmware Update Mechanism InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 182 All this specific information is described in the documentation provided with the firmware update tools. The firmware update tools, firmware and documentation are available from the Agilent web. • http://www.agilent.com/en-us/firmwareDownload?whid=69761 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 183: Electrical Connections
There are no externally accessible fuses because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure NOTE proper functionality and compliance with safety or EMC regulations.
Page 184: Serial Number Information (All)
00000 Serial number Rear view of the module Configuration switch USB-Mini-Port Power socket Figure 20 Rear view of the pump – electrical connections and label InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 185: Interfaces
Hardware Information Interfaces Interfaces The Agilent InfinityLab LC Series modules provide the following interfaces: Table 14 Agilent InfinityLab LC Series Interfaces Module RS-232 Analog APG (A) Special (on-board) / ERI (E) Pumps G7104A/C G7110B G7111A/B, G5654A G7112B G7120A, G7132A G7161A/B...
Page 186 RS-232C as interface to a computer • USB (Universal Series Bus) as interface to a computer • REMOTE connector as interface to other Agilent products • Analog output connector(s) for signal output InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 187: Overview Interfaces
“USB (Universal Serial Bus)” on page 192. Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s mainboard. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 188 Remote (ERI) The ERI (Enhanced Remote Interface) connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. It allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
Page 189 PREPARE (L) Request to prepare for analysis (for example, calibration, detector lamp on). Receiver is any module performing pre-analysis activities. Special Interfaces There is no special interface for this module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 190: Eri (Enhanced Remote Interface)
ERI replaces the AGP Remote Interface that is used in the HP 1090/1040/1050/1100 HPLC systems and Agilent 1100/1200/1200 Infinity HPLC modules. All new InfinityLab LC Series products using the FUSION core electronics use ERI. This interface is already used in the Agilent Universal...
Page 191 This serial line can be used to read out an EPROM or write into an EPROM of a connected ERI-device. The firmware can detect the connected type of device automatically and update information in the device (if required). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 192: Usb (Universal Serial Bus)
Short circuit will be detected through hardware. USB (Universal Serial Bus) USB (Universal Serial Bus) - replaces RS232, supports: • a PC with control software (for example Agilent Lab Advisor) • USB Flash Disk InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 193: Setting The 6-Bit Configuration Switch
For specific LAN modes switches 4-5 must be set as required. • For boot resident/cold start modes switches 1+2 or 6 must be UP. Configuration switch Figure 22 Location of Configuration switch (example shows a G7114A/B VWD) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 194 When selecting mode COM, settings are stored to non-volatile memory. When selecting mode TEST, COM settings are taken from non-volatile memory. not assigned - Always keep these switches on position ‘0’ (off) Default IP Address is 192.168.254.11 Host Name will be the MAC address. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 195: Special Settings
Save your methods and data before executing a forced cold start.  If you use the following switch settings and power the instrument up again, it will start as described above. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 196 Boot Main System / Keep Data Boot Resident System / Keep Data Boot Main System / Revert to Default Data Boot Resident System / Revert to Default Data Note: The setting '0' (down) is essential. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 197: Early Maintenance Feedback
EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 198: Instrument Layout
• the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 199: Lan Configuration
Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) Setup (DHCP) Manual Configuration With Telnet This chapter provides information on connecting the module to the Agilent ChemStation PC. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 200: What You Have To Do First
PC network card using a crossover network cable (point-to-point) or • a hub or switch using a standard LAN cable. LAN interface MAC label Figure 24 Location of LAN interfaces and MAC label InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 201: Tcp/Ip Parameter Configuration
TCP/IP parameters after power-on. The parameters may be derived non-volatile memory or initialized with known default values. The initialization mode is selected by the configuration switch, see Table 18 on page 203. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 202: Configuration Switches
Location of Configuration switch (example shows a G7114A/B VWD) The module is shipped with all switches set to OFF, as shown above. To perform any LAN configuration, SW1 and SW2 must be set to OFF. NOTE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 203: Initialization Mode Selection
The TCP/IP connection will be established using these parameters. The parameters were configured previously by one of the described methods. Non-Volatile Active Parameter Stored Parameter Figure 26 Using Stored (Principle) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 204 In the Using Default mode, the parameters stored in the memory of the module NOTE are not cleared automatically. If not changed by the user, they are still available, when switching back to the mode Using Stored. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 205: Dynamic Host Configuration Protocol (Dhcp)
2 It may be necessary to fully qualify the hostname with the DNS suffix, e.g. 0030d3177321.country.company.com. 3 The DHCP server may reject the hostname proposed by the card and assign a name following local naming conventions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 206 0030d3177321. On the Local Controller the MAC address can be found under Details in the LAN section. Figure 29 LAN Setting on Instant Pilot InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 207 Advisor, Firmware Update Tool) and use MAC address as host name, e.g. 0030d3177321. The LC system should become visible in the control software (see Note in section “General Information (DHCP)” on page 205). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 208: Manual Configuration
TELNET Session Non-Volatile Stored Parameter Control Module Figure 30 Manual Configuration (Principle) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 209: With Telnet
When the connection was established successfully, the module responds with the following: Figure 32 A connection to the module is made 3 Type ? and press enter to see the available commands. Figure 33 Telnet Commands InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 210 TCP/IP settings TCP/IP status - here ready connected to PC with controller software (e.g. Agilent Figure 34 Telnet - Current settings in "Using Stored" mode ChemStation), here not connected InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 211 If the Initialization Mode Switch is changed now to “Using Stored” mode, the NOTE instrument will take the stored settings when the module is re-booted. In the example above it would be 192.168.254.12. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 212: Appendix
In Case of Damage Solvents Safety Symbols Waste Electrical and Electronic Equipment (WEEE) Directive Radio Interference Sound Emission Agilent Technologies on the Internet This chapter provides addition information on safety, legal and web. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 213: General Safety Information
Do not use this product in any manner not specified by the manufacturer. The protective features of this product may be impaired if it is used in a manner not specified in the operation instructions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 214: Before Applying Power
Verify that the voltage range and frequency of your power distribution  matches to the power specification of the individual instrument. Never use cables other than the ones supplied by Agilent Technologies  to ensure proper functionality and compliance with safety or EMC regulations.
Page 215: Do Not Operate In An Explosive Atmosphere
Personal injury (for example electrical shock, intoxication) Instruments that appear damaged or defective should be made  inoperative and secured against unintended operation until they can be repaired by qualified service personnel. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 216: Solvents
For details, see the usage guideline for the solvent cabinet. A printed copy of the NOTE guideline has been shipped with the solvent cabinet, electronic copies are available in the Agilent Information Center or via the Internet. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 217: Safety Symbols
A pacemaker could switch into test mode and cause illness. A heart defibrillator may stop working. If you wear these devices keep at least 55 mm distance to magnets. Warn others who wear these devices from getting too close to magnets. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 218 Do not proceed beyond a caution until you have fully understood and met  the indicated conditions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 219: Waste Electrical And Electronic Equipment (Weee) Directive
The affixed label indicates that you must not discard this electrical/electronic product in domestic household waste. Do not dispose of in domestic household waste NOTE To return unwanted products, contact your local Agilent office, or see http://www.agilent.com for more information. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 220: Radio Interference
If test and measurement equipment is operated with unscreened cables, or used for measurements on open set-ups, the user has to assure that under operating conditions the radio interference limits are still met within the premises. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 221: Sound Emission
Appendix Sound Emission Sound Emission Sound pressure Sound pressure Lp <70 db(A) according to DIN EN ISO 7779 Schalldruckpegel Schalldruckpegel Lp <70 db(A) nach DIN EN ISO 7779 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 222: Agilent Technologies On The Internet
Appendix Agilent Technologies on the Internet Agilent Technologies on the Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
Page 223 • using the binary pump, • optimizing performance, • troubleshooting and diagnostics, • maintenance, • parts and materials for maintenance, • identifying cables, • hardware information, • appendix. www.agilent.com  Agilent Technologies Inc. 2016-2021 Edition: 10/2021 Document No: SD-29000214 Rev. C...

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Agilent Technologies InfinityLab LC Series User Manual

Table of Contents

3 Using the Pump

4 Optimizing Performance

6 Error Information

7 Test Functions and Calibration

8 Maintenance

9 Parts and Materials for Maintenance

10 Identifying Cables

11 Hardware Information

12 LAN Configuration

13 Appendix

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Summary of Contents for Agilent Technologies InfinityLab LC Series