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Waters Manuals
Laboratory Equipment
Prep Series
Installation and maintenance manual
Waters Prep Series Installation And Maintenance Manual
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Contents
Table of Contents
Troubleshooting
Bookmarks
Table of Contents
Copyright Notice
Trademarks
Customer Comments
Safety Considerations
Safety Advisories
Operating this Instrument
Audience and Purpose
Intended Use of the Waters Prep Series HPLC System
Calibrating
ISM Classification
ISM Classification: ISM Group 1 Class B
EC Authorized Representative
Table of Contents
1 Overview
Waters Prep Series
Preplc System
Delta-Prep System
Waters Prep Series
Delta-Prep
Waters Prep Series Modules
Inject Start
Waters 746 Integrator
Chassis Ground
Signal Ground
Accessories
Getting Started
Starting the System
Using the Front Panel
Displaying Help
Shutting down the System
Configuring the Controller
2 Installing the System
Setting up and Inspecting
Unpacking and Installing the System
Selecting the Site
Electrical Requirements
Electrical Conditions
Voltage Selections
Assembling the System
Connecting Rheodyne Injectors
Connecting the M-1000 Preppak Module (Optional)
Connecting Additional Devices
Attaching the Interface Cable and Power Cord
Connecting IEEE-488 Interfaces
Connecting to the Waters 746 Data Module
Liquid Line Connections
Connecting a Helium Tank to the Fluid Handling Unit
Helium Specifications
Sparging
Connecting Compression Fittings
Setting up the Plunger Wash
Considerations
Connecting the Plunger Wash Tube
Connecting to the Injection Panel (Preplc System)
Connecting to the Column Rack (Delta-Prep System)
Installing Sample Injection Options
Installing the Small-Scale Sample Injection Valve Option (Preplc System)
Using an Autoinjector
Making Electrical Connections
Connecting Liquid Lines When Using a Waters Autoinjector
Connecting a Fraction Collector
Making the Remote Start Connection
Making Chart Mark Connections
Installing Analytical and Preparative Columns
Preplc System
Delta-Prep System
Making Detector Connections
Preplc or Delta-Prep System
Connecting Detector Semi-Prep Cells
Using the RI Detector with the Flow Splitter Option
3 Troubleshooting, Testing, and Maintenance
Troubleshooting
Troubleshooting Steps
Troubleshooting Flowcharts
Troubleshooting Flowcharts
Baseline Noise
High System Pressure
Troubleshooting Chromatography
Poor Peak Resolution
Chromatography Troubleshooting
Hardware Troubleshooting
Software Troubleshooting
Replace with New Table
Illegal Vial Number
Number out of Range
Program Method Table Saved
Step Does Not Exist
First Vial Greater than Last Vial
Invalid Injection Number
Invalid Vial Number
Performance Tests
Self-Diagnostics
Extended Tests
Maintenance Procedures
Column Rack Tubing Configuration
Fluid Handling Unit Maintenance
Replacing Fuses
Maintaining Rheodyne Manual Injectors
Warning Symbols
A Safety Advisories
Warning Symbols
Task-Specific Hazard Warnings
Specific Warnings
Caution Symbol
Warnings that Apply to All Waters Instruments
Electrical and Handling Symbols
Electrical Symbols
Handling Symbols
B Specifications
C Spare Parts
Gradient
D Solvent Considerations
Clean Solvent
Solvent Miscibility
Viscosity
How to Use Miscibility Numbers (M-Numbers
Buffered Solvents
Solvent Head Height
Solvent Viscosity
Solvent Degassing
Solvent Degassing Methods
Index
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Operating this Instrument
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Waters Prep Series
Installation and Maintenance Guide
71500045204/Revision B
Copyright © Waters Corporation 2010
All rights reserved
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Table of Contents
Troubleshooting
Troubleshooting, Testing, and Maintenance
85
Troubleshooting
86
Troubleshooting flowcharts
87
Troubleshooting flowcharts
89
Troubleshooting chromatography
93
Chromatography troubleshooting
100
Hardware troubleshooting
107
Software troubleshooting
115
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