Micromeritics AccuPyc 1330 Operator's Manual page 5

Table of Contents
Entering Commands . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5
Performing an Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-6
Reviewing and Editing Data . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7
Printing Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-10
Transmitting Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-14
Calibrating the Pycnometer . . . . . . . . . . . . . . . . . . . . . . . . . . 4-15
Zeroing the Pressure Transducer . . . . . . . . . . . . . . . . . . . . . . . 4-16
Manually Controlling the Valves . . . . . . . . . . . . . . . . . . . . . . . 4-17
Editing the Setup Parameters . . . . . . . . . . . . . . . . . . . . . . . . . 4-18
5. TROUBLESHOOTING AND MAINTENANCE
Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-1
Error and Status Messages . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-5
Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-14
Recovering from a Power Failure . . . . . . . . . . . . . . . . . . . . . . . 5-21
6. ORDERING INFORMATION
APPENDICES
Appendix A: Changing the Analysis Module
Appendix B: Analysis Theory
Appendix C: Calibration Theory
Appendix D: Format of Transmitted Data
Appendix E: Printer Character Set
INDEX
ii
Reviewing and Editing Analysis Results and Parameters . . . . . . . 4-7
Reviewing and Editing Calibration Results and Parameters
Analysis or Calibration Parameters . . . . . . . . . . . . . . . . . . . 4-19
Report Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-22
Calibration Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-24
Data Transmission . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-26
Unit Types, Operating Language, Date, and Time . . . . . . . . . . . 4-27
Queued Messages . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-5
Messages Displayed During an Automatic Operation . . . . . . . . . 5-12
Replacing the Chamber Cap O-Ring . . . . . . . . . . . . . . . . . . 5-15
Checking the Cell and Expansion Chambers for Leaks . . . . . . . . 5-16
Replacing the Gas Inlet Filters . . . . . . . . . . . . . . . . . . . . . 5-18
Cleaning the Pycnometer . . . . . . . . . . . . . . . . . . . . . . . . 5-21
AccuPyc 1330
. . . . . 4-9
September 1996