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Micromeritics MIC SAS II 5800 Operator's Manual

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MIC SAS II 5800
S
-S
A
S
UB
IEVE
UTO
IZER
O
M
PERATOR
ANUAL
580-42800-01
June 2019
(Rev - )

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Summary of Contents for Micromeritics MIC SAS II 5800

  • Page 1 MIC SAS II 5800 IEVE IZER PERATOR ANUAL 580-42800-01 June 2019 (Rev - )
  • Page 2 RADEMARKS MIC SAS is a registered trademark of Micromeritics Instrument Corporation. Micromeritics is a registered trademark of Micromeritics Instrument Corporation. Copyright The software described in this manual is furnished under a license agreement and may be used or copied only in accordance with the terms of the agreement.
  • Page 3 MICROMERITICS shall not be liable for consequential or other type damages resulting from the use of any of its products other than the liability stated above. This warranty is in lieu of all other warranties, express or implied, including but not limited to, the implied warranties of merchantability or fitness for use.

  • Page 4: Corporate Profile

    This ensures that local, knowledgeable support is available for every customer, in academia or industry. Micromeritics works across a truly diverse range of industries from oil processing, petrochemicals and catalysts, to food and pharmaceuticals, and at the forefront of characterization technology for next generation materials such as graphene, metal-organic-frameworks, nanocatalysts, and zeolites.

  • Page 5: Contact Us

    Phone: 1-770-662-3636 Fax: 1-770-662-3696 www.Micromeritics.com Instrument Service or Repair Phone: 1-770-662-3666 International — contact your local distributor or call 1-770-662-3666 Service.Helpdesk@Micromeritics.com Micromeritics Learning Center Phone: 1-770-662-3607 www.Micro.edu MIC SAS II 5800 Operator Manual 580-42800-01 (Rev - ) — June 2019...

  • Page 6: About This Manual

    WARNING — Warnings contain information to help prevent actions that may cause personal injury. EU D ECLARATION OF ONFORMITY To view the full EU Declaration of Conformity document, visit the Micromeritics web page at https://www.micromeritics.com/About-Us/CE-Declarations-of-Conformity.aspx. Original Instructions (English) Part Number 580-42800-01 (Rev - ) Released June 2019 Copyright 2019...

  • Page 7: Table Of Contents

    3 - 11 4 SOP Menu Selection 4 - 1 5 Instrument Menu Selection 5 - 1 Home Position 5 - 3 6 Maintenance Menu Selection 6 - 1 MIC SAS II 5800 Operator Manual 580-42800-01 (Rev - ) — June 2019...
  • Page 8 Connect a Regulator and a Gas Line to a Gas Cylinder 7 - 6 Power Instrument On and Off 7 - 8 Routine Maintenance 7 - 9 8 Help 8 - 1 Index Index - 1 MIC SAS II 5800 Operator Manual 580-42800-01 (Rev - ) — June 2019...

  • Page 9: About The Mic Sas

    The emergency stop button powers off the stepper motor in case of an emergency. A safety shield is placed around the piston and anvil area during operation. MIC SAS II 5800 Operator Manual 1 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 10 USB port on the back for devices with cords. The USB ports can be used to connect a printer or key- board, export and import data, and update software. MIC SAS II 5800 Operator Manual 1 - 2 580-42800-01 (Rev - ) — June 2019...
  • Page 11 The USB ports can be used to con- nect a printer or keyboard, export and import data, and update software. MIC SAS II 5800 Operator Manual 1 - 3 580-42800-01 (Rev - ) — June 2019...

  • Page 12: Safety Precautions

    Do not use a power cord or power supply other than what was supplied with the instrument. If a replacement is needed, contact your Micromeritics Service Representative. MIC SAS II 5800 Operator Manual 1 - 4 580-42800-01 (Rev - ) — June 2019...

  • Page 13: Menu Selections

    Power Off No analysis is running. Ready Displays at the end of an analysis when the piston is moving Readying towards the disengage position. MIC SAS II 5800 Operator Manual 1 - 5 580-42800-01 (Rev - ) — June 2019...

  • Page 14: Remote Browsers

    27 cm (10.5 in.) Depth 16 kg (34 lbs.) Weight In keeping with a policy of ongoing product improvement, specifications are subject to change without notice. MIC SAS II 5800 Operator Manual 1 - 6 580-42800-01 (Rev - ) — June 2019...

  • Page 15: Mic Sas Menu Selection

    CANCEL. When CANCEL is tapped, the button changes to START. Select an SOP from the drop-down box to display the SOP details. MIC SAS II 5800 Operator Manual 2 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 16 Pause [button] Displays when an analysis is paused. Tap to restart the analysis. Resume [button] Description of the sample used for analysis. Sample name [text box] MIC SAS II 5800 Operator Manual 2 - 2 580-42800-01 (Rev - ) — June 2019...

  • Page 17: Load A Sample

    11. Install the sample tube collar and adjust the collar when the sample tube is in place. 12. Install the safety shield over the anvil, sample tube, and piston assembly. MIC SAS II 5800 Operator Manual 2 - 3 580-42800-01 (Rev - ) — June 2019...

  • Page 18: Remove The Brass Sample Plug

    3. Remove the brass plug from the bottom of sample tube. 4. Pour out the sample, or, if necessary, push the sample out by pushing the remaining plug with the extraction tool. MIC SAS II 5800 Operator Manual 2 - 4 580-42800-01 (Rev - ) — June 2019...

  • Page 19: Records Menu Selection

    Tap to run an analysis with this record's conditions. Tapping it switches to the MIC SAS view and uses the record's conditions as the SOP. MIC SAS II 5800 Operator Manual 3 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 20 Displays the Size Control Chart report or the Surface Area Control Chart for the selected records. There may be mul- tiple selections. MIC SAS II 5800 Operator Manual 3 - 2 580-42800-01 (Rev - ) — June 2019...
  • Page 21 Returns fields to the currently saved values. Revert [button] Description of the sample used for analysis. Sample name [text box] Saves screen changes. Save [button] MIC SAS II 5800 Operator Manual 3 - 3 580-42800-01 (Rev - ) — June 2019...
  • Page 22 3 Records Menu Selection IEW A ECORD Tap a blue link on the Records list to view a record. MIC SAS II 5800 Operator Manual 3 - 4 580-42800-01 (Rev - ) — June 2019...

  • Page 23: Reports

    Temperature offset Pin slope Pin offset Pdiff slope Motor current percent Disengage position Engage position The date and time are shown for each entry. MIC SAS II 5800 Operator Manual 3 - 5 580-42800-01 (Rev - ) — June 2019...

  • Page 24: Fisher Number Map Report

    A Fisher number map is a polynomial that relates SAS particle size to Fisher number for a particular material. The Fisher particle size shown in reports is the Fisher number displayed with units of μm. MIC SAS II 5800 Operator Manual 3 - 6...
  • Page 25 The lower axis limits are zero; the upper limits are autoscaled. The fit is y-axis shown as a smooth curve without points in orange. A legend identifies the two data sets. MIC SAS II 5800 Operator Manual 3 - 7 580-42800-01 (Rev - ) — June 2019...

  • Page 26: Log Report

    Shield placement and removal during analysis Emergency stop and reset Temperature calibration Pressure gauge tare Pressure calibration Motor current set (including number of cycles) MIC SAS II 5800 Operator Manual 3 - 8 580-42800-01 (Rev - ) — June 2019...

  • Page 27: Control Charts

    1. On the Records menu, select one or more records, then tap the Report icon ( 2. Select either Size Control Chart or Surface Area Control Chart. Size Control Chart MIC SAS II 5800 Operator Manual 3 - 9 580-42800-01 (Rev - ) — June 2019...
  • Page 28 3 Records Menu Selection Surface Area Control Chart MIC SAS II 5800 Operator Manual 3 - 10 580-42800-01 (Rev - ) — June 2019...

  • Page 29: Print Or Export Records

    3. Select one or more records to export. 4. Tap the download icon. A success message displays upon successful download: Successfully saved to <USB-location>.zip. Please remove USB. MIC SAS II 5800 Operator Manual 3 - 11 580-42800-01 (Rev - ) — June 2019...

  • Page 31: Sop Menu Selection

    Tap a blue link in the SOP list to view or edit SOP details. Tap the plus icon on the toolbar to create a new SOP. MIC SAS II 5800 Operator Manual 4 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 32 Analysis Type [button] Organics — mainly pharmaceuticals Inorganics — mainly for heavy metal powders such as tungsten Name of the analysis batch. Batch name [text box] MIC SAS II 5800 Operator Manual 4 - 2 580-42800-01 (Rev - ) — June 2019...
  • Page 33 Step Size [Inorganics]. Analysis terminates after: Termination threshold [button] Low. 3 decreasing particle sizes or 25 cycles High. 5 decreasing particle sizes or 40 cycles MIC SAS II 5800 Operator Manual 4 - 3 580-42800-01 (Rev - ) — June 2019...
  • Page 34 Deletes the selected SOPs from the list. Tap the box to the left of the record to select it, then tap the Delete icon to delete the selected SOPs. Tap to create a new SOP. MIC SAS II 5800 Operator Manual 4 - 4 580-42800-01 (Rev - ) — June 2019...

  • Page 35: Instrument Menu Selection

    Use for manual operation and monitoring the state of the instrument. Additional controls are present when Allow calibration is selected in the Maintenance > Advanced view. Changing calibrations can affect the performance of the instrument. Make changes only under the direction of a Micromeritics Service Representative. Instrument Schematic Description Component Anvil with O-ring inside sample tube.
  • Page 36 Up arrow. Tap to move the piston up in increments. Stop button. Tap to stop the piston movement. Down arrow. Tap to move the piston down in increments. MIC SAS II 5800 Operator Manual 5 - 2 580-42800-01 (Rev - ) — June 2019...

  • Page 37: Home Position

    The Home position is where there is no gap between the plugs. ETURN THE PISTON TO THE HOME POSITION 1. Tap Instrument on the menu. 2. Tap Home. The piston lowers to the home position. MIC SAS II 5800 Operator Manual 5 - 3 580-42800-01 (Rev - ) — June 2019...

  • Page 39: Maintenance Menu Selection

    Shows setup information about the instrument. Maintenance Description Field or Button Administrator level configuration options — enabled only when the Advanced [button] instrument is in the Idle state. MIC SAS II 5800 Operator Manual 6 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 40 Allow calibration [check box]. Enable to allow users to calibrate the instrument. These settings affect the instrument operation. Make changes only under the direction of a Micromeritics Service Rep- resentative. Disk usage .* Displays the percentage of disk space used .
  • Page 41 Installation on page 6 - Returns fields to the currently saved values. Revert [button] Saves screen changes. Save [button] Serial number of the instrument. Serial Number ** MIC SAS II 5800 Operator Manual 6 - 3 580-42800-01 (Rev - ) — June 2019...
  • Page 42 [drop-down box] * Applicable to Static networks only. ** Field cannot be edited. *** Field can be edited on the Advanced view only. MIC SAS II 5800 Operator Manual 6 - 4 580-42800-01 (Rev - ) — June 2019...

  • Page 43: Remote Computer Configuration

    To access the instrument from the remote computer, enter the IP address of the instrument in a web browser on the remote computer. Firefox and Chrome are the recommended browsers. MIC SAS II 5800 Operator Manual 6 - 5 580-42800-01 (Rev - ) — June 2019...

  • Page 44: Printer Installation

    1. Tap the Maintenance tab. 2. Tap Printers at the bottom of the window. 3. On the Administration tab, select the attached printer, then tap Continue. MIC SAS II 5800 Operator Manual 6 - 6 580-42800-01 (Rev - ) — June 2019...
  • Page 45 Share This Printer option. Tap Continue when done. 5. Select the printer model from the Model drop-down list then tap Printer. MIC SAS II 5800 Operator Manual 6 - 7 580-42800-01 (Rev - ) — June 2019...
  • Page 46 7. Tap the Printers tab. The installed printer displays. 8. Tap the Administration drop-down list and tap Set as default printer. 9. To specify additional printer options, tap the Administration drop-down list. MIC SAS II 5800 Operator Manual 6 - 8 580-42800-01 (Rev - ) — June 2019...
  • Page 47 Printer Installation 10. Tap MIC SAS to return to the application. MIC SAS II 5800 Operator Manual 6 - 9 580-42800-01 (Rev - ) — June 2019...

  • Page 48: Clean The Instrument

    2. Remove the keyboard before the browser refresh process completes. When the browser com- pletes the refresh process, the virtual keyboard can be used. MIC SAS II 5800 Operator Manual 6 - 10 580-42800-01 (Rev - ) — June 2019...

  • Page 49: Upload Logo

    2. Tap the Maintenance menu, then tap Advanced. 3. Tap Upload Logo. 4. On the Confirm Action window, tap to restart the application immediately or tap to can- cel the operation. MIC SAS II 5800 Operator Manual 6 - 11 580-42800-01 (Rev - ) — June 2019...
  • Page 50 3. Select the file in the list, then click Upload. 4. On the Confirm Action window, click to restart the application immediately or click cancel the operation. MIC SAS II 5800 Operator Manual 6 - 12 580-42800-01 (Rev - ) — June 2019...

  • Page 51: Troubleshooting And Maintenance

    Action: The loss of a very small amount of sample may not require any action. A second filter paper on the top brass plug may reduce the amount of sample lost. MIC SAS II 5800 Operator Manual 7 - 1...
  • Page 52 Be sure to enter the actual mass and density. A warning that mass and density differ by more than 5% is shown, but the analysis can still be started. MIC SAS II 5800 Operator Manual 7 - 2 580-42800-01 (Rev - ) — June 2019...

  • Page 53: Gas Connections

    Ensure the gas cylinder is closed before connecting to the analyzer. MIC SAS II 5800 Operator Manual 7 - 3 580-42800-01 (Rev - ) — June 2019...

  • Page 54: Replace A Gas Cylinder

    7. Replace the protective cap on the depleted cylinder. Disconnect the retaining strap and move the cylinder to an appropriate location. MIC SAS II 5800 Operator Manual 7 - 4 580-42800-01 (Rev - ) — June 2019...
  • Page 55 15-20 psig (103-138 kPag) MIC SAS II 15-18 psig (103 - 124 kPag) TriStar Exceeding the maximum recommended air pressure could cause personal injury or dam- age the instrument. MIC SAS II 5800 Operator Manual 7 - 5 580-42800-01 (Rev - ) — June 2019...

  • Page 56: Connect A Regulator And A Gas Line To A Gas Cylinder

    If pressure drops, repair the leak. 6. Connect the gas line to the regulator. a. Connect the gas line to the regulator connector. MIC SAS II 5800 Operator Manual 7 - 6 580-42800-01 (Rev - ) — June 2019...
  • Page 57 Open the gas cylinder shutoff valve and flow gas for 10 to 30 seconds. c. Close the gas cylinder shutoff valve and allow regulator pressure to go to zero. MIC SAS II 5800 Operator Manual 7 - 7 580-42800-01 (Rev - ) — June 2019...

  • Page 58: Power Instrument On And Off

    Power OFF the equipment in the following order: 1. Ensure the instrument status is Idle. 2. Disconnect the power plug from the instrument. (There is no ON/OFF power switch.) MIC SAS II 5800 Operator Manual 7 - 8 580-42800-01 (Rev - ) — June 2019...

  • Page 59: Routine Maintenance

    UPPLY Check that the cylinder has adequate pressure. Replace the cylinder when it is low. See Replace a Gas Cylinder on page 7 - 4 MIC SAS II 5800 Operator Manual 7 - 9 580-42800-01 (Rev - ) — June 2019...

  • Page 61: Help

    Internet connection is required for online help. If internet connection is not available on the instrument, go to http://bit.ly/2PCKB7B on a device with internet access, or scan the QR code. MIC SAS II 5800 Operator Manual 8 - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 63 7 - 3 gas line, connect to gas cylinder 7 - 6 power analyzer on and off 7 - 8 print records 3 - 11 MIC SAS II 5800 Operator Manual Index - 1 580-42800-01 (Rev - ) — June 2019...
  • Page 64 2 - 4 SOP menu selection 4 - 1 specifications 1 - 6 status instrument 1 - 5 troubleshooting 7 - 1 warranty i MIC SAS II 5800 Operator Manual Index - 2 580-42800-01 (Rev - ) — June 2019...

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