Agilent Technologies 1290 Infinity LC System System Manual And Quick Reference page 99

4 Right-click the Thermostatted Column Compartment (TCC) area, and select
5 Right-click the Diode-Array Detector area, and select Method... in the
6 All the required module parameters have now been entered. Select Method >
7 Allow the system to equilibrate for at least 10 min, and check that the
Agilent 1290 Infinity LC System Manual and Quick Reference
b Other parameters can remain at default settings. Click OK to exit the
window.
The changes are sent to the autosampler module.
Method... in the context menu.
a In the Method page for the 1290 Infinity TCC, enter the following
parameters:
•
Left Temperature 40 °C
•
Right Temperature Combined
b Other parameters can remain at default settings. Click OK to exit the
window.
The changes are sent to the TCC module.
context menu.
a In the Method page for the 1290 Infinity DAD , enter the following
parameters:
• Use Signal: Turn all signals except Signal A off by clearing the check
boxes.
•
Signal A: 250 nm, bw 100 nm, ref 360 nm, bw 100 nm
•
Peak width: 0.012 min (0.25 s Response, 20 Hz)
b In the Advanced section, set Spectrum Store to All.
c Other parameters can remain at default settings. Click OK to exit the
window.
The changes are sent to the DAD module.
Save Method As... to save the method with a new name.
The ChemStation will not allow the method to be saved as DEF_LC.M, so that
the default method template is not altered.
baseline in the Online Plot is stable before starting the analysis.
Data Acquisition in Method and Run Control View
5
Quick Start Guide
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