Endress+Hauser analytikjena multi N/C UVHS Operating Manual page 4

Toc analyzer
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4 Installation and commissioning ..................................................................................................................................... 34
4.1
Installation conditions ...................................................................................................................................... 34
4.1.1
Ambient conditions .......................................................................................................................................... 34
4.1.2
Device layout and space requirements ............................................................................................................ 34
4.1.3
Power supply..................................................................................................................................................... 35
4.1.4
Gas supply ......................................................................................................................................................... 35
4.2
Unpacking and setting up the device............................................................................................................... 35
4.2.1
Installing and commissioning the analyzer..................................................................................................... 36
4.3
Connecting accessories..................................................................................................................................... 39
4.3.1
The AS 10e and AS 21hp autosamplers ......................................................................................................... 39
4.3.2
AS vario autosampler ...................................................................................................................................... 46
4.3.3
EPA Sampler .................................................................................................................................................... 52
4.3.4
External solids module ..................................................................................................................................... 56
5 Operation ........................................................................................................................................................................ 58
5.1
General notes.................................................................................................................................................... 58
5.2
Switching on the analyzer ................................................................................................................................ 59
5.3
Switching off the analyzer................................................................................................................................ 60
5.4
Carrying out calibration .................................................................................................................................... 61
5.4.1
Preparing and starting calibration................................................................................................................... 61
5.4.2
Displaying the calibration results..................................................................................................................... 63
5.4.3
Editing calibration ............................................................................................................................................ 64
5.4.4
Linking a calibration to a method.................................................................................................................... 65
5.4.5
Managing calibration data............................................................................................................................... 67
5.5
Performing measurements .............................................................................................................................. 67
5.5.1
Measurement with manual sample feed ........................................................................................................ 67
5.5.2
Measurement with autosampler ..................................................................................................................... 68
6 Maintenance and care.................................................................................................................................................... 70
6.1
Maintenance overview ..................................................................................................................................... 70
6.2
Adjustment and setting.................................................................................................................................... 71
6.2.1
General notes for adjusting the autosampler ................................................................................................. 71
6.2.2
Adjusting the AS vario autosampler ................................................................................................................ 71
6.2.3
Adjusting the EPA Sampler .............................................................................................................................. 73
6.2.4
Setting the NPOC purge flow ........................................................................................................................... 76
6.3
Syringe pump maintenance ............................................................................................................................. 77
6.4
Replacing the pump hose................................................................................................................................. 78
6.5
Replacing the hose connections ...................................................................................................................... 79
6.6
Checking the system for leaks.......................................................................................................................... 80
6.7
UV reactor maintenance................................................................................................................................... 81
6.7.1
Checking the illumination of the lamp ............................................................................................................ 81
6.7.2
Cleaning the UV reactor.................................................................................................................................... 81
6.8
Cleaning the TIC condensate vessel................................................................................................................. 82
6.9
Replacing the water traps ................................................................................................................................ 83
6.10
Replacing the halogen trap.............................................................................................................................. 86
7 Troubleshooting.............................................................................................................................................................. 88
7.1
Software error messages.................................................................................................................................. 89
7.2
Status errors...................................................................................................................................................... 93
4
multi N/C UVHS, multi N/C pharma UV

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