Gas Purity; Traps; Purity Requirements - Thermo Scientific FOCUS GC Site Preparation And Installation Manual

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Gas and Plumbing Requirements

Gas Purity

If possible, you should use only instrument or chromatographic purity grade gases
in your FOCUS GC.

Traps

UHP (Ultra-High Purity) gases should not contain impurities above 1 ppm.
Impurities below 1 ppm generally do not require purification. Gases with higher
impurity levels may require oxygen and hydrocarbon traps. A number of GC
supply and accessory companies carry a variety of traps for gases.
See Figure 4-2,
sequence. For more information on gas purification, contact your local Thermo
Fisher Scientific CSE.
Moisture Traps
Water in the carrier or fuel gas may damage the gas chromatograph column and
contaminate the FOCUS GC system. Water content should be less than 1 ppm in
all cases. If you are using multiple traps, install the moisture trap closest the gas
supply, before the hydrocarbon and the oxygen trap.
Hydrocarbon Traps
Hydrocarbon traps remove organic materials from gases. If you are using multiple
traps, install the hydrocarbon trap after the moisture trap, but before the oxygen
trap.
Oxygen Traps
Oxygen content in the carrier and gas lines should be less than 1 ppm. To achieve
a level of oxygen of less than 1 ppm, install an oxygen-removing trap in the
carrier gas line between the gas tank and the GC. If you are using multiple traps,
the oxygen trap should be the last trap in the series.

Purity Requirements

The following sections describe the minimum requirements for gases used in your
gas chromatograph system. Always consider using UHP 99.999% pure gases
when available.
Site Preparation and Installation Manual
Gas Trap
Order, on page 57, for the correct trap installation
Chapter 1
Laboratory Preparation
33

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