Sign In
Upload
Manuals
Brands
Thermo Scientific Manuals
Laboratory Equipment
Surveyor MSQ Plus
Thermo Scientific Surveyor MSQ Plus Manuals
Manuals and User Guides for Thermo Scientific Surveyor MSQ Plus. We have
1
Thermo Scientific Surveyor MSQ Plus manual available for free PDF download: Hardware Manual
Thermo Scientific Surveyor MSQ Plus Hardware Manual (148 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 5.52 MB
Table of Contents
Table of Contents
9
About this Guide
13
Preface
13
Related Documentation
13
Safety and Special Notices
13
Safety Precautions
14
Solvent and Gas Purity Requirements
15
Contacting Us
16
Chapter 1 Introduction
17
Ion Polarity Modes
18
Overview
18
Electrospray Ionization (ESI)
19
Ionization Techniques
19
Atmospheric Pressure Chemical Ionization (APCI)
22
Data Types
24
Full Scan
24
Scan Types
24
Selected Ion Monitoring (SIM)
24
Profile Data Type
25
Centroid Data Type
26
MCA Data Type
26
Chapter 2 Functional Description
29
Liquid Chromatograph
31
Reference Inlet System
32
MS Detector
35
Front Panel Status Indicator
35
Rear Panel Controls and Connections
37
Connection between LC and MS Detector
39
API Sources
39
Rf/DC Prefilter
42
Mass Analyzer
42
Ion Detection System
44
Vacuum System
47
Inlet Gas Hardware
49
Cone Wash System
52
Data System
53
Computer Hardware
54
Xcalibur Software
54
Surveyor MSQ Plus Server
55
Tune Window
56
Printer
60
Chapter 3 Daily Operation
61
Things to Do before Operating the MS Detector
61
Checking the Nitrogen Supply
61
Checking the Disk Space
62
Checking the Oil Level in the Oil Mist Filter
62
Things to Do after Operating the MS Detector
63
Flushing the API Probes
64
Placing the System in the off Mode
64
Draining the Oil Mist Filter and Purging the Pump Oil
64
Emptying the Solvent Waste Bottles
65
Chapter 4 Switching Probes
67
Switching from ESI to APCI
67
Switching from APCI to ESI
69
Chapter 5 Routine and Preventive Maintenance
71
Maintenance Schedule
71
Maintaining the ESI Probe
72
Removing the ESI Probe
73
Removing the ESI Capillary
74
Cleaning or Replacing the ESI Capillary
76
Replacing the Ceramic Sleeve of the ESI Probe
77
Installing the ESI Capillary
79
Installing the ESI Probe
82
Maintaining the APCI Probe
83
Removing the APCI Probe
83
Removing the APCI Capillary
84
Installing the APCI Capillary
86
Installing the APCI Probe
88
Maintaining the Probe Heater
89
Removing the Probe Heater
89
Cleaning the Probe Heater
92
Replacing the Detent Screw Insulator
92
Installing the Probe Heater
94
Maintaining the Source Block Assembly
95
Preparing the LC/MS System for Maintenance
96
Clearing Access to the Source Block Assembly
97
Removing the Entrance Cone and the Cone Wash Nozzle
97
Cleaning the Entrance Cone and the Cone Wash Nozzle
99
Removing the Source Block Assembly
101
Cleaning the Rf/DC Prefilter
102
Cleaning the Extraction Cone and the Source Block
104
Assembling the Source Block Assembly
106
Installing the Source Block Assembly
107
Maintaining the Forepump
109
Chapter 6 System Shutdown, Startup, and Reset
111
Shutting down the System in an Emergency
111
Turning off the Nitrogen Gas
112
Placing the System in the off Mode
113
Turning the MS Detector off from Xcalibur
114
Turning the MS Detector off from the Tune Window
115
Shutting the System down for Non-Routine Maintenance
116
Restarting the System Following a Complete Shutdown
117
Checking the System Connections
118
Restarting the Surveyor MSQ Plus System
119
Resetting the MS Detector
120
Chapter 7 Replaceable Parts
123
Consumables
124
Spares
127
General Spares
127
Kits
127
Source Block Assembly
127
ESI Probe Assembly
130
APCI Probe Assembly
131
Probe Heater Assembly
132
Vacuum Spares
133
Gas Flow Spares and Nitrogen Generator
133
Solvent Path and Calibrant Spares
134
Electronic Spares
134
Connection Kits
134
Manuals
134
Appendix A Optimizing the LC Conditions
135
Flow Rates
135
LC Solvents and Mobile Phase Additives
136
LC Solvents
136
Mobile Phase Additives
136
Cone Wash System
139
Flow Splitting
140
PEEK Tubing
140
Index
143
Advertisement
Advertisement
Related Products
Thermo Scientific SUPER-NUOVA+
Thermo Scientific MaxQ SHKE4000-1CE
Thermo Scientific MaxQ SHKE4000-7JPN
Thermo Scientific S3
Thermo Scientific SHKA7000
Thermo Scientific SL4F Plus
Thermo Scientific Solaris 2000
Thermo Scientific Solaris 2000 I
Thermo Scientific Cimarec S194615
Thermo Scientific SpeedVac SPD210
Thermo Scientific Categories
Laboratory Equipment
Measuring Instruments
Accessories
Refrigerator
Freezer
More Thermo Scientific Manuals
Login
Sign In
OR
Sign in with Facebook
Sign in with Google
Upload manual
Upload from disk
Upload from URL