Thermo Scientific EA IsoLink IRMS System Manuals

Manuals and User Guides for Thermo Scientific EA IsoLink IRMS System. We have 1 Thermo Scientific EA IsoLink IRMS System manual available for free PDF download: Operating Manual

Thermo Scientific EA IsoLink IRMS System Operating Manual (186 pages)

Including the Flash IRMS Elemental Analyzer

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 7.89 MB

Table of Contents
13
Preface
19
About Your System
19
Power Rating
20
Contacting Us
20
Safety Alerts and Important Information
20
Safety Symbols and Signal Words
20
Instrument Markings and Symbols
22
Environmental Conditions
23
Safety Information
23
Use of Gases
23
Safety Cut off Device
23
Gases Precautions
24
Precaution for Helium
24
Precaution for Oxygen
24
Precaution for Hydrogen
24
Precaution for Nitrogen
24
Precaution for Sulfur Dioxide
24
Precaution for Carbon Dioxide
24
Precaution for Carbon Monoxide
25
Hazardous Substances Precautions
25
Venting Toxic Gases
25
Residual Risks
25
High Voltage
25
Hot Parts
25
Hazardous Chemical
26
Maintenance Precaution
26
Personal Protective Equipment
26
Training
27
Getting Familiar with Your EA Isolink IRMS System for CNSOH
29
Technical Features
30
Instrument Configurations
30
Software Requirements
30
Instrument Basics
31
Safety Information
33
Safety Cut off Device
33
Labels Location on the Instrument
34
Use of Gases
35
Gas Supply
35
Gas Purity
35
Maximum Pressure
35
Nominal Pressure
36
Precaution for Carbon Monoxide
36
Precaution for Sulfur Dioxide
36
Using Hydrogen
37
Leak Test
37
Front Panel
39
Back Panel
40
Top Panel
41
Furnaces Compartment
41
Oven Compartment
44
Detection System Description
46
Electrical Compartment
46
Low Voltage Compartment
47
Main Voltage Compartment
48
Connections Panel
49
Interface Area
49
Power Supply Area
50
Gases Supply Area
50
Transformers Compartment
51
Devices for the Furnaces Control
53
Devices Supplying the Furnaces
53
Status Panel
53
Autosamplers
54
MAS Plus Autosampler for Solid Samples
54
AI 1310 /AS 1310 Autosampler for Liquid Samples
55
Ramped GC Oven
56
Analytical Principles
59
About Your System
59
Pneumatic Circuit
60
Pressure Regulators
63
Electronic Flow Controller (EFC-T) Module
64
Automatic Switching Valve Block (ASV)
65
Helium Management
67
Preparation of Reactors and Adsorption Filter
72
NC Configuration
72
H and O Configurations
74
Preparing the Reactors
74
Preparing the Adsorption Filter
77
The Ramped GC Oven
78
Installing Flash IRMS Elemental Analyzer
79
Preliminary Information
79
Who Performs the Installation
79
Standard Outfit
79
Verify Site Preparation
79
Unpacking the Instrument
80
Placing the Instrument
80
Making the Gas Supply Plumbing Connections
81
Building the Gas Lines
81
Purging Gas Lines
81
Connecting the Gas Lines
82
Electrical Connections
82
Mounting Peripheral Devices
82
Power Connections
83
Performing Electrical Connections
83
Installing the Reactors into the Furnaces
84
Setting Pressure and Flow Parameters
91
NCS Determination
91
H-O Determinations
91
Installing Autosampler
92
Isodat Software Suite
92
Installing MAS Plus Autosampler
93
MAS Plus Autosampler Overview
93
MAS Plus Autosampler Installation
95
Installing AI 1310/AS 1310 Autosampler
99
Preliminary Information
99
Who Performs the Installation
99
Electrical Requirement
99
Lift and Carry the Sampling Unit
100
Installing the Direct Injection Device for Flash IRMS Elemental Analyzer
100
Installing the Sampler Support on the Flash IRMS Elemental Analyzer
101
Installing the AI 1310/AS 1310 on the Flash IRMS Elemental Analyzer
104
Installation of the Sampling Unit
105
Installing the Syringe
107
Electrical Connections
109
Starting-Up
110
Using EA Isolink IRMS System for CNSOH
111
Introduction
111
Dual Measurement
112
Procedure
112
Performing a Jump Calibration
113
Creating an Isodat Method for N+C Measurement (Dual Measurement)
116
Creating an EA Method for N+C Measurement
120
Creating an Isodat Method for Single Mode S Measurements
121
High-Temperature Conversion - Analysis of H and O Isotopes
122
Bottom Field Connector
122
Setting up a HO Method
124
Procedure Overview
124
Dual Measurement
125
Creating a New Method for Dual Measurement
125
Creating an EA Method for H+O Measurement
130
Creating a Sequence for Dual Measurement
132
Start Data Acquisition
133
Dual Measurement Results
134
H3-Factor Determination
135
Measuring Sulfur Isotopes
136
Introduction
136
Procedure
136
Sulfur Measurement Kits
137
Preparing the System for a Sulfur Measurement
137
Before Starting a Sulfur Measurement
138
Setting for Flash Elemental Analyzer
139
Create a Gas Configuration for a Sulfur Measurement
139
Starting a Sulfur Measurement
142
EA Isolink Setting
142
Defining an Isodat Method
143
Events During Acquisition
144
Maintenance
147
Post-Analysis Operations
148
Putting the Instrument in Standby Mode
148
Maintaining the Instrument
150
Current Maintenance Program
150
Replacing Reactors and Adsorption Filters
150
Replacing the Filling Materials
151
Ashes Removal and Crucible Cleaning
152
Maintaining the Reactor of the Pyrolysis Unit
153
Replacing the Gas Chromatographic Column
155
Maintaining the MAS Plus Autosampler
157
Upgrading EA for 25 MM OD Macro Reactor
161
Cleaning the Instrument
163
Troubleshooting
165
Analytical Troubleshooting
165
Safety Cutoff
166
EFC-T Module
168
Eagersmart Software Installation
169
Running the Flash IRMS as Stand-Alone Instrument
170
Eagersmart Main Menu
171
Configuring the Analyzer
171
Performing a Leak Test
175
Adjusting the Detector Signal Level
176
View Sample Being Acquired
177
Configuring Eagersmart Data Handling Software
178

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Thermo Scientific EA IsoLink IRMS System Manuals

Thermo Scientific EA IsoLink IRMS System Operating Manual (186 pages)

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