Table of Contents
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Contents
Introduction ............................................................................................... 5
Pyris Installation ............................................................................................... 6
Safety and Regulatory Information ........................................................... 7
Symbols Used in Online Help ............................................................................. 8
Symbols Used on the Instruments ...................................................................... 8
Electrical Warnings ...........................................................................................12
Electromagnetic Compatibility (EMC) .................................................................14
Electrical Safety ...............................................................................................15
WEEE Instructions for PerkinElmer Products ......................................................16
Prepare the Laboratory ............................................................................ 18
Prepare the Laboratory .....................................................................................19
Electrical Requirements ..............................................................................19
Environmental Requirements ......................................................................19
Purge Gas and Pneumatic Supply ...............................................................20
Space Requirements ..................................................................................20
Install Multiple Analyzers ........................................................................ 23
Install Multiple Analyzers ..................................................................................24
Install a DSC 4000 ................................................................................... 27
Safety Precautions for the DSC 4000 .................................................................28
DSC 4000 Warning Labels .................................................................................32
Warning Labels on the Upper Ring Around the Furnace................................32
Warning Labels on the Back of the DSC 4000 ..............................................34
Install a DSC 4000 ...........................................................................................36
Unpacking the DSC 4000 ..................................................................................37
Set Up the DSC 4000 System Components .........................................................39
Select the Correct Voltage for the DSC 4000 ...............................................39
Connect the Purge Gas Supply to the DSC 4000 ..........................................41
Connect the Cooling Device to the DSC 4000...............................................42
Connect the DSC 4000 System Components ......................................................47
Configure the DSC 4000 ...................................................................................48
Starting the Pyris Manager .........................................................................49
Calibrate the DSC 4000.....................................................................................50
DSC 4000 Hardware ................................................................................. 53
DSC 4000 ........................................................................................................54
Furnace and Sensor Design ........................................................................54
Cooling .....................................................................................................55
Calibration of the DSC 4000 ..............................................................................56
Temperature Calibration ............................................................................56
Perform Indium and Zinc Runs ...................................................................57
Perform a Peak Area with Onset Calculation ................................................57
Performing a Temperature Calibration.........................................................58
Heat Flow Calibration .................................................................................58
Operating Variables and Sample Handling ..........................................................60
Temperature Range ...................................................................................60
Scanning Rate ...........................................................................................60
Subambient Operation of the DSC 4000 .............................................................61
DSC 4000 Maintenance .....................................................................................62
DSC 4000 Part Numbers ...................................................................................63
Miscellaneous Part Numbers .......................................................................64
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