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Thermo Scientific TSQ Quantum XLS Manuals
Manuals and User Guides for Thermo Scientific TSQ Quantum XLS. We have
3
Thermo Scientific TSQ Quantum XLS manuals available for free PDF download: User Manual, Pre-Installation Requirements Manual
Thermo Scientific TSQ Quantum XLS User Manual (190 pages)
TSQ Series
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 6 MB
Table of Contents
FCC Class A, CFR 47 Part
4
Table of Contents
11
Preface
15
Related Documentation
15
Safety and Special Notices
15
Safety Precautions
17
Solvent and Gas Purity Requirements
18
Service Philosophy
18
Level of Repair
18
Contacting Us
19
Chapter 1 Introduction
21
Ionization Modes
23
Electron Ionization Mode
24
Chemical Ionization Mode
24
Ion Polarity Modes
25
Scan Modes
25
Q1MS and Q3MS Scan Modes
27
Product Scan Mode
27
Parent Scan Mode
28
Neutral Loss Scan Modes
29
Data-Dependent Scan Mode
31
Scan Types
32
Full Scan
32
Selected Ion Monitoring (SIM)
32
Selected Reaction Monitoring (SRM)
33
Highly-Selective Reaction Monitoring (H-SRM)
33
Intelligent Selected Reaction Monitoring (Isrm)
33
Quantitation-Enhanced, Data-Dependent MS (QED MS)
34
Autosim
34
Data Types
34
Profile Data Type
34
Centroid Data Type
35
Mass/Charge Range
35
Chapter 2 Functional Description
37
Functional Description
37
Autosampler
38
Direct Sample Probes
39
Gas Chromatograph
39
Transfer Line
40
Mass Spectrometer
41
Controls and Indicators
42
EI CI Ion Source
45
Inlet Valve
49
Ion Optics
50
Mass Analyzer
52
Ion Detection System
59
Vacuum System and Inlet Gasses Hardware
61
Electronic Assemblies
66
Data System
68
Computer Hardware
68
Data System / Mass Spectrometer / GC Interface
68
Data System / Local Area Network Interface
69
Chapter 3 System Shutdown, Startup, and Reset
71
Shutting down the System in an Emergency
71
Placing the System in Standby Mode
72
Shutting down the System Completely
73
Starting up the System after a Complete Shutdown
75
System
75
Starting up the GC
76
Starting up the Data System
76
Starting up the Mass Spectrometer
76
Starting up the Autosampler
78
Setting up Conditions for Operation
78
Resetting the Mass Spectrometer
78
Resetting the Data System
79
Turning off Selected Mass Spectrometer Components
80
Chapter 4 Tuning and Calibrating
83
Displaying the FC-43 Mass Spectrum
84
Running Auto Tune and Calibration
86
Saving the Tune and Calibration Report
89
Chapter 5 Changing Ionization Modes
93
Removing the Ion Volume
93
Installing the Ion Volume
100
Chapter 6 Maintenance
103
Cleaning Ion Source Components
105
Cleaning Ion Volumes
108
Cleaning Lenses of the TSQ Quantum XLS Ion Source
108
Cleaning the Lenses of the TSQ Quantum GC Ion Source
115
Reinstalling the Ion Source
122
Replacing the Filament of the TSQ Quantum XLS Ion Source
122
Replacing the Filament of the TSQ Quantum GC Ion Source
125
Disassembling and Reassembling the TSQ Quantum XLS Ion Source Completely
127
Disassembling and Reassembling the TSQ Quantum GC Ion Source Completely
130
Cleaning Stainless Steel Parts
133
Cleaning Non-Stainless Steel or Hybrid Part
135
Maintaining the Forepump
136
Adding Calibration Compound
137
Replacing the Ball Valve Seal
140
Removing and Installing a GC Capillary Column
142
Removing a GC Capillary Column
142
Installing a GC Capillary Column
144
Maintenance
103
Chapter 7 Diagnostics and Troubleshooting
149
TSQ Quantum XLS System Diagnostics
149
Troubleshooting
151
Communication Issues
151
Contamination Issues
153
Filament and Lens Control Issues
155
Heated Zone Issues
156
High Vacuum Issues
158
Linearity Issues
159
Power Supply Issues
160
Sensitivity Issues
160
Stability Issues
163
Tuning Issues
163
Replacing a Fuse
165
Replacing Pcbs and Power Supplies
166
Appendix 8 Using the Direct Sample Probe
167
Creating an Instrument Method
167
Creating a Sequence
170
Preparing the Probe and Inlet Valve
171
Preparing the Mass Spectrometer
171
Running the Sequence
173
Examining the Raw Data in Qual Browser
177
Removing the Probe
178
Chapter 9 Replaceable Parts and Consumables
181
Accessory Kit
181
Chemicals Kit
182
Index
183
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Thermo Scientific TSQ Quantum XLS User Manual (176 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 12 MB
Table of Contents
Table of Contents
9
Preface
13
Related Documentation
13
Safety and Special Notices
14
Contacting Us
15
Chapter 1 Introduction
17
Ionization Modes
19
Electron Ionization Mode
20
Chemical Ionization Mode
20
Ion Polarity Modes
21
Scan Modes
21
Q1MS and Q3MS Scan Modes
23
Product Scan Mode
23
Parent Scan Mode
24
Neutral Loss Scan Modes
25
Data-Dependent Scan Mode
27
Scan Types
28
Full Scan
28
Selected Ion Monitoring (SIM)
28
Selected Reaction Monitoring (SRM)
29
Highly-Selective Reaction Monitoring (HSRM)
29
Intelligent Selected Reaction Monitoring (Isrm)
29
Quantitation-Enhanced, Data-Dependent MS (QED MS)
30
Autosim
30
Data Types
30
Profile Data Type
30
Centroid Data Type
31
Mass/Charge Range
31
Chapter 2 Functional Description
33
Autosampler
34
Gas Chromatograph
35
Direct Sample Probes
35
Transfer Line
36
Mass Spectrometer
37
Controls and Indicators
38
EI/CI Ion Source
42
Inlet Valve
44
Ion Optics
45
Mass Analyzer
47
Ion Detection System
54
Vacuum System and Inlet Gasses Hardware
56
Electronic Assemblies
61
Data System
62
Computer Hardware
63
Data System/Mass Spectrometer/Gc Interface
63
Data System/Local Area Network Interface
63
Chapter 3 System Shutdown, Startup, and Reset
65
Shutting down the System in an Emergency
65
Placing the System in Standby Mode
67
Shutting down the System Completely
67
Starting up the System after a Complete Shutdown
69
Restoring Power to the TSQ Quantum XLS Series System
70
Starting up the GC
70
Starting up the Data System
70
Starting up the Mass Spectrometer
70
Starting up the Autosampler
72
Setting up Conditions for Operation
72
Resetting the Mass Spectrometer
73
Resetting the Data System
73
Turning off Selected Mass Spectrometer Components
74
Chapter 4 Tuning and Calibrating
77
Displaying the FC-43 Mass Spectrum
78
Running Auto Tune and Calibration
80
Saving the Tune and Calibration Report
83
Running Maintenance Tune
86
Creating a Quality Control (QC) Tune Report
87
Chapter 5 Changing Ionization Modes
89
Removing the Ion Volume
89
Installing the Ion Volume
96
Maintenance
99
Chapter 6 Maintenance
99
Cleaning Ion Source Components
101
Cleaning Ion Volumes
103
Cleaning the Lenses of the Ion Source
103
Replacing the Filament of the Ion Source
109
Completely Disassembling and Reassembling the Ion Source
111
Complete Disassembly and Reassembly of the Ion Source
112
Cleaning Stainless Steel Parts
114
Cleaning Non-Stainless Steel or Hybrid Parts
116
Maintaining the Forepump
117
Adding Calibration Compound
118
Replacing the Ball Valve Seal
121
Removing and Installing a GC Capillary Column
123
Removing a GC Capillary Column
123
Installing a GC Capillary Column
125
Chapter 7 Diagnostics and Troubleshooting
129
Diagnostics
129
Troubleshooting
130
Communication Issues
130
Contamination Issues
133
Filament and Lens Control Issues
135
Heated Zone Issues
136
High Vacuum Issues
137
Linearity Issues
139
Power Supply Issues
140
Sensitivity Issues
140
Stability Issues
143
Tuning Issues
144
Replacing Fuses
146
Replacing Pcbs and Power Supplies
146
Appendix A Using the Direct Sample Probe
147
Creating an Instrument Method
147
Creating a Sequence
150
Preparing the Probe and Inlet Valve
151
Preparing the Mass Spectrometer
151
Running the Sequence
153
Examining the Raw Data in Qual Browser
157
Removing the Probe
158
Appendix B Replaceable Parts and Consumables
161
EI/CI Ion Source Replaceable Parts
161
Miscellaneous Replaceable Parts and Consumables
163
Accessory Kit
164
Chemicals Kit
165
Index
167
Thermo Scientific TSQ Quantum XLS Pre-Installation Requirements Manual (50 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
11
Preface
13
Related Documentation
13
Safety and Special Notices
14
Contacting Us
14
Chapter 1 Introduction
17
Chapter 2 Site Preparation
19
Entrance
20
Space and Load Requirements
20
Telephone
24
Chapter 3 Operating Environment
25
Temperature
26
Humidity
27
Vibration
27
Lighting
27
Particulate Matter
27
Electrostatic Discharge
28
Chapter 4 Line Power
29
Quality of Power
31
Power Monitoring Devices
32
Power Conditioning Devices
32
Available Outlets
33
Connecting the TSQ Quantum XLS or TSQ Quantum GC Mass Spectrometer, GC, and Other Modules to Wall Outlets
35
Uninterruptible Power Supply
35
Technical Assistance
36
Chapter 5 Waste and Exhaust
37
Exhaust System
37
Solvent Waste
38
Chapter 6 Gas and Plumbing Requirements
39
Gases
40
Plumbing
40
Chapter 7 Installation
41
Preinstallation Survey
42
Installation Kits
43
Installation
44
Preventive Maintenance
44
Chapter 8 Instrument Arrival
45
Index
47
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