Analysis Equipment And Supplies; Application Related Issues; Gases For Instrument Test; Degas Unit - Micromeritics TriStar II Plus Pre-Installation Manual

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Application Related Issues

Analysis Equipment and Supplies

Since the analysis results are expressed in units of surface area per gram of sample, the true mass of the
sample must be known. This requires an analytical balance with the capacity of 100 grams measure-
ment and 1 mg readability.
In order to obtain accurate analysis results, the sample tubes must be clean. The following items are
suggested for cleaning sample tubes:
• Sink
• Small plastic tub for detergent solution
• Alconox or similar laboratory detergent
• Drying oven
• Ultrasonic bath
• Isopropyl Alcohol
Application Related Issues
To ensure a thorough installation, it will be helpful for Micromeritics to know which types of samples
you will be testing. If possible, please list those types in the section
13.
Please advise us if your samples require any pretreatment. If required, do you have the proper equip-
ment, such as a vacuum oven or furnace, to pretreat your samples?
Micromeritics offers application assistance through our materials analysis laboratory (Micromeritics
Analytical Services at 770-662-3630).

Gases for Instrument Test

To verify proper instrument operation and to train your instrument users, Micromeritics representatives
will analyze the reference material provided in the instrument accessories.
The gases listed below are required in order to analyze the reference materials. If these gases are not
available, Micromeritics representatives will only be able to perform a limited number of instrument
tests during installation and operator training.
(CGA 580) N
2
(CGA 580) He

Degas Unit

It is highly recommended that a degas unit be used to ensure that proper degassing of all sample types
can be performed. Using a degas unit avoids moisture in the analyzer.
8
TriStar II Plus Preinstallation Instructions and Checklist
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Application Related
Issues, page
303-42870-01 (Rev B) - Mar 2015

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