3
Chromatographic Symptoms
Negative Peaks Seen with TCD
86
• Verify that the correct gas type is being used.
• Check for a leak in the system, especially at the detector
column fitting. (See
• Consider thermal conductivity of analytes relative to carrier.
• Check the flow settings, then measure the actual detector
flows. (See
"To Measure a Detector
"Checking for
Leaks".)
Flow".)
Agilent 7890 Series Troubleshooting