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Contact Us on http://www.thermofisher.com. Technical Assistance For technical support for HPLC products, contact your local Thermo Fisher Scientific support organization. For contact information, go to Contact Us on http://www.thermofisher.com. Refractive Index Detector (VC-D60) Page 3 Operating Manual...
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Contacting Us Page 4 Refractive Index Detector (VC-D60) Operating Manual...
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5.10 Turning On the Device .................. 67 6 Operation................... 69 Introduction to this Chapter ................ 70 Safety Guidelines for Operation................ 71 General Guidelines for Operation................ 72 Control Elements .................... 73 6.4.1 Keypad...................... 73 6.4.2 Status Indicators.................. 74 Page 6 Refractive Index Detector (VC-D60) Operating Manual...
Using this Manual 1 Using this Manual This chapter provides information about this manual, the conventions used throughout the manual, and the reference documentation that is available in addition to this manual. Refractive Index Detector (VC-D60) Page 9 Operating Manual...
The descriptions in this manual assume that the device is installed in the Vanquish system stack. If this is not the case, additional hardware is required and must be ordered separately. The information in this manual applies correspondingly. Page 10 Refractive Index Detector (VC-D60) Operating Manual...
Highlights information necessary to prevent damage to the device or invalid test results. TIP Highlights information of general interest or helpful information that can make a task easier or optimize the performance of the device. Refractive Index Detector (VC-D60) Page 11 Operating Manual...
The electronic version (PDF) of the manual contains numerous links that you can click to go to other locations within the manual. These include: • Table of contents entries • Index entries • Cross-references (in blue text) Page 12 Refractive Index Detector (VC-D60) Operating Manual...
For information about the main elements of the user interface and step-by-step guidance through the most important workflows, refer to the Quick Start Guide. • Reference Card For a concise overview of the most important workflows, refer to the Reference Card. Refractive Index Detector (VC-D60) Page 13 Operating Manual...
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TIP The Chromeleon Help and documents are included in the software shipment. Third-Party Documentation Refer also to the user documentation provided by the manufacturers of third-party components and materials, for example, Safety Data Sheets (SDSs). Page 14 Refractive Index Detector (VC-D60) Operating Manual...
• Safety 2 Safety This chapter provides general and specific safety information and informs about the intended use of the device. Refractive Index Detector (VC-D60) Page 15 Operating Manual...
Always keep the manual near the device for quick reference. • Save this manual and pass it on to any subsequent user. Read, understand, and comply with all safety messages and precautionary statements presented in this manual. Page 16 Refractive Index Detector (VC-D60) Operating Manual...
TIP An additional type label on the leak tray of the device indicates the module name, serial number, part number, and revision number (if any). To facilitate device identification, have the information from this label available when communicating with Thermo Fisher Scientific. Refractive Index Detector (VC-D60) Page 17 Operating Manual...
Regularly running calibration • Establishing shelf life limits and following them for all consumables used with the system • Running the system according to the laboratory's verified and validated 'lab developed test' protocol Page 18 Refractive Index Detector (VC-D60) Operating Manual...
Thermo Fisher Scientific before proceeding. Safety Standard This device is a Safety Class I instrument (provided with terminal for protective grounding). The device has been manufactured and tested according to international safety standards. Refractive Index Detector (VC-D60) Page 19 Operating Manual...
Protective Clothing To protect you from chemical splashes, harmful liquids, or other contamination, put on appropriate protective clothing, such as a lab coat. Page 20 Refractive Index Detector (VC-D60) Operating Manual...
Do not place liquid reservoirs directly upon the device. Liquid might leak into the device and get into contact with electronic components causing a short circuit. Instead, place liquid reservoirs in the solvent rack that is available for the Vanquish system. Refractive Index Detector (VC-D60) Page 21 Operating Manual...
Wear personal protective equipment as required by the hazard and follow good laboratory practice. • Dispose of biohazardous waste in an environmentally safe manner that is consistent with local regulations. Follow a regulated, approved waste disposal program. Page 22 Refractive Index Detector (VC-D60) Operating Manual...
Prevent the generation of static electricity near the chromatography system. 2.3.6 In Case of Emergency WARNING—Safety Hazard In case of emergency, disconnect the device from the power line. Refractive Index Detector (VC-D60) Page 23 Operating Manual...
Thermo Fisher Scientific or one of its authorized representatives. The device has been shipped from the manufacturing site in a safe condition. See also Compliance Information (} page 126) Page 24 Refractive Index Detector (VC-D60) Operating Manual...
• Mobile phases containing ammonium hydroxide: In rare cases, a shortened lifetime of reversed-phase (UHMW-PE) piston seals has been observed with high pH, ammonium hydroxide containing mobile phases and prolonged exposure. Refractive Index Detector (VC-D60) Page 25 Operating Manual...
If a solvent listed below is in use, flush out all the flow path sufficiently with an inert solvent that is compatible with your chromatographic system. Buffers, acids, and other highly ionic aqueous solutions should be flushed out with large amounts of Page 26 Refractive Index Detector (VC-D60) Operating Manual...
• Observe the general guidelines and recommendations on the use of solvents and additives in the chromatography system. Refer to Use of Solvents and Additives in the Vanquish System Operating Manual. Refractive Index Detector (VC-D60) Page 27 Operating Manual...
• Device Overview 3 Device Overview This chapter introduces you to the device and the main components. Refractive Index Detector (VC-D60) Page 29 Operating Manual...
• Stable baselines with a maximum drift of 0.2 µRIU/h or less and with a maximum noise of 2.5 nRIU or less • Flow cell temperature stabilization by active heating for improved baseline signal Page 30 Refractive Index Detector (VC-D60) Operating Manual...
Figure 1: Snell’s Law Character Description index of refraction angle of incidence angle of refraction velocity of light in first medium velocity of light in second medium Refractive Index Detector (VC-D60) Page 31 Operating Manual...
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As long as no difference exists between the refractive indices of the media of the two cells, there is no refraction of the light passing through them. Page 32 Refractive Index Detector (VC-D60) Operating Manual...
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Additional circuitry enables the user to easily correct the signal output to electronic zero. Ns = Nr Ns > Nr Figure 4: Photo sensors Description Photo sensor A Photo sensor B Light beam Refractive Index Detector (VC-D60) Page 33 Operating Manual...
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This difference gives a signal having both amplitude and polarity. Page 34 Refractive Index Detector (VC-D60) Operating Manual...
Keypad with status indicators Flow cell inlet and outlet Capillary clip Leak tray with leak sensor Type label, indicating the module name, serial number, part number, and re- vision number (if any) Leak sensor Refractive Index Detector (VC-D60) Page 35 Operating Manual...
When the leak sensor detects leakage, the status indicators change to red and beeping starts to alert you. Follow the instructions in this manual to find and eliminate the source for the leakage. Page 36 Refractive Index Detector (VC-D60) Operating Manual...
Chromeleon Help. Other data systems may support operation of this device. In this case, installation of additional software may be required. For details, contact the Thermo Fisher Scientific sales organization. Refractive Index Detector (VC-D60) Page 37 Operating Manual...
• Unpacking 4 Unpacking This chapter provides information for unpacking the device and informs you about the scope of delivery. Refractive Index Detector (VC-D60) Page 39 Operating Manual...
2. Remove the ship kit from the shipping container. 3. Remove the device from the shipping container: Grasp the device by the carrying handles. Slowly and carefully, lift the device out of the shipping container. Page 40 Refractive Index Detector (VC-D60) Operating Manual...
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8. Some surfaces including the doors of the device are covered by a protective film during shipment. Remove the protective film from all surfaces as applicable. Refractive Index Detector (VC-D60) Page 41 Operating Manual...
Ship Kit • Operating manual (downloadable from customer manual web site) • Power cord For information on contents of the ship kit or reordering parts, see Accessories, Consumables and Replacement Parts (} page 119). Page 42 Refractive Index Detector (VC-D60) Operating Manual...
Installation 5 Installation This chapter specifies the requirements for the installation site and describes how to set up, install, and configure the device in the Vanquish system and in the chromatography software. Refractive Index Detector (VC-D60) Page 43 Operating Manual...
Setting Up the Flow Connections (} page 58) ↓ Set up the device in the software Setting Up the Device in the Software (} page 65) ↓ Turn on the device Turning On the Device (} page 67) ↓ Page 44 Refractive Index Detector (VC-D60) Operating Manual...
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Recommended: Perform Instrument Installation Qualification On the Chromeleon 7 Console, click Tools > Instrument Qualification > Installation Qualification. ↓ Recommended: Perform Operational Qualification On the Chromeleon 7 Console, click Tools > Instrument Qualification > Operational Qualification. Refractive Index Detector (VC-D60) Page 45 Operating Manual...
Always unplug the power cord before starting repair work inside the device. • If you were instructed to remove any housing covers or panels, do not connect the power cord to the device while the cover or panels are removed. Page 46 Refractive Index Detector (VC-D60) Operating Manual...
The end of the power cords that plugs into the power socket on the device is identical for all power cords. The end of the power cords that plugs into the wall socket is different. Refractive Index Detector (VC-D60) Page 47 Operating Manual...
If you suspect that condensation is present, allow the device to warm up to room temperature. This may take several hours. Wait until the condensation is gone completely before connecting the device to the power line. Page 48 Refractive Index Detector (VC-D60) Operating Manual...
To access the interior components in the device, open the front doors. To allow easy access from the front, the flow connections of the device are located directly behind the doors. Figure 8: Opening the front doors Refractive Index Detector (VC-D60) Page 49 Operating Manual...
UV/VIS detector. For instructions on how to set up the system stack, refer to the Vanquish System Operating Manual. Page 50 Refractive Index Detector (VC-D60) Operating Manual...
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• Installation System with Single Detector Figure 9: Vanquish system, standard configuration (example) Description Solvent rack Refractive index detector Autosampler Pump System base Column compartment Refractive Index Detector (VC-D60) Page 51 Operating Manual...
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• Installation System with Refractive Index Detector as Second Detector Figure 10: Vanquish system, configuration with two detectors (example) Description Solvent rack Refractive index detector UV/VIS detector Autosampler Pump System base Column compartment Page 52 Refractive Index Detector (VC-D60) Operating Manual...
2. Loosen the 2 screws by 2 turns each. Do not fully remove them. Figure 11: Loosening the locking screws 3. Install the slide-in module (see Installing the Slide-In Module (} page 103)). Refractive Index Detector (VC-D60) Page 53 Operating Manual...
USB (Universal Serial Bus) port ("B"-type connector): Allows connection to the computer on which the data management system is installed, such as the Chromeleon software. System interlink port: Allows power on/off control for the detector from the system base. Page 54 Refractive Index Detector (VC-D60) Operating Manual...
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Vanquish system. For instructions, see Connecting Cables in a One- Detector-Configuration (} page 56) Connecting Cables in a Two- Detector Configuration (} page 56). 2. Connect the power cord (see Connecting the Power Cord (} page 57)). Refractive Index Detector (VC-D60) Page 55 Operating Manual...
2. Connect a system interlink cable from the free System Interlink port on the diode array detector to the refractive index detector. 3. Connect a system interlink cable from the free System Interlink port on the refractive index detector to the column compartment. Page 56 Refractive Index Detector (VC-D60) Operating Manual...
1. Verify that the power switch on the device is set to OFF. 2. Connect the power cord to the power inlet connector on the device. 3. Connect the free end of the power cord to an appropriate power source. Refractive Index Detector (VC-D60) Page 57 Operating Manual...
Connect the waste line to the flow cell only as described in the manual. • Do not discharge waste from the flow cell through the open leakage drain system of the Vanquish system. Page 58 Refractive Index Detector (VC-D60) Operating Manual...
Connecting Viper Capillaries This section describes how to connect Viper™ capillaries. All Viper flow connections in the Vanquish system are designed to be finger-tight. To connect Viper capillaries with knurls, follow these steps: Refractive Index Detector (VC-D60) Page 59 Operating Manual...
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2. If leakage continues, remove the capillary. 3. Clean the capillary ends carefully by using a lint-free tissue wetted with isopropanol. 4. Reinstall the capillary. 5. If the connection continues to leak, install a new Viper capillary. Page 60 Refractive Index Detector (VC-D60) Operating Manual...
(i.e. peak broadening effects due to extra dispersion volume). 2. Connect the capillary to the flow cell inlet (IN). Refractive Index Detector (VC-D60) Page 61 Operating Manual...
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UV/VIS detector. Refer to the instructions in the Operating Manual for the UV/VIS detector. 2. Route the connecting capillary from the flow cell outlet of the UV/ VIS detector upward to the refractive index detector. Page 62 Refractive Index Detector (VC-D60) Operating Manual...
(refer to the Vanquish System Operating Manual). 2. Remove the plug from the flow cell outlet. Refractive Index Detector (VC-D60) Page 63 Operating Manual...
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(refer to the Vanquish System Operating Manual). TIP The waste line should go straight to the system base and to waste. Make sure that the line is positioned straight in the tubing guides. Page 64 Refractive Index Detector (VC-D60) Operating Manual...
1. Start the Chromeleon 7 Instrument Configuration Manager. 2. Select the instrument and click Add Module. 3. On the Manufacturers list, select Thermo Scientific HPLC: Vanquish, and on the Modules list, select Vanquish Refractive Index Detector. 4. On the General page, in the COM Port box, select the new virtual COM port (usually the COM port with the highest number).
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COM port. Try a different COM port and test the connection again. 6. Save the installation and close the Instrument Configuration Manager. Page 66 Refractive Index Detector (VC-D60) Operating Manual...
Turn off the device with the main power switch, when instructed to do so, for example, during maintenance. Pressing the system power button will not be sufficient to turn off the power to the device completely. See also Power On/Off Control (} page 76) Refractive Index Detector (VC-D60) Page 67 Operating Manual...
• Operation 6 Operation This chapter describes the elements for device control, provides information for routine operation and for shutdown. Refractive Index Detector (VC-D60) Page 69 Operating Manual...
Operating Manual. Details on control and operation of the device are available in the Chromeleon Help. Software descriptions in this manual refer to Chromeleon 7. Terminology may be different to that of other software versions. Page 70 Refractive Index Detector (VC-D60) Operating Manual...
Never expose the fluidic components of the detector to excessive backpressure. Observe the specified pressure rating for the detector (see Performance Specifications (} page 116)). • Avoid clogging of the flow cell or waste line. Refractive Index Detector (VC-D60) Page 71 Operating Manual...
Stable backpressure and correct waste line setup ¨ TIP During measurements, avoid touching the module’s front (close the doors) or the electrical connectors as this may impair the measurement signal. Page 72 Refractive Index Detector (VC-D60) Operating Manual...
To turn off the beep for the current alarm, press this button. Eliminate the source for the alarm within 10 minutes. Otherwise, beeping starts again. If the device detects a different problem, beeping alerts you again immediately. Refractive Index Detector (VC-D60) Page 73 Operating Manual...
An injection, sequence or validation procedure (such as span validation) is running. A problem or error has occurred. For the related message, check the Instrument Audit Trail. For remedial action, see Troubleshooting (} page 107). Page 74 Refractive Index Detector (VC-D60) Operating Manual...
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A problem or error has occurred. For the related message, check the Instrument Audit Trail. For remedial action, see Troubleshooting (} page 107). For information about the LED that is present next to the PURGE button on the keypad, see Keypad (} page 73). Refractive Index Detector (VC-D60) Page 75 Operating Manual...
To turn off a device completely, you have to turn it off with the main power switch on the device. Pressing the system power button will not be sufficient to turn off the power to the device completely. Page 76 Refractive Index Detector (VC-D60) Operating Manual...
3. Perform an Autozero. This may take up to 40 seconds. TIP The chromatography data system supports procedures for automatically starting a chromatography system, including stabilizing the noise and drift signal (Smart Startup). For details, refer to the Chromeleon Help. Refractive Index Detector (VC-D60) Page 77 Operating Manual...
20 minutes from the above step. 5. Press or deactivate PURGE again to turn off the valve. Mobile phase solvent flows to the sample cell. 6. Wait until the baseline is stabilized. Page 78 Refractive Index Detector (VC-D60) Operating Manual...
• If you select a lower temperature setting than was set before, the stabilization time will take longer compared to setting a higher temperature. Refractive Index Detector (VC-D60) Page 79 Operating Manual...
THF as the solvent. Organohalocarbons, such as methylene Keep a small amount of flow to keep chloride and chloroform down the amount of corrosive chloride impurities in the cell. Page 80 Refractive Index Detector (VC-D60) Operating Manual...
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If the detector is to be exposed to sub-freezing temperatures, an antifreeze flush, such as methanol must be used. Ideally, you are suggested to expel residual solution out of the detector and to fill the sample and reference cells with isopropanol. Refractive Index Detector (VC-D60) Page 81 Operating Manual...
• Maintenance and Service 7 Maintenance and Service This chapter describes the routine maintenance and the service procedures that the user may perform. Refractive Index Detector (VC-D60) Page 83 Operating Manual...
However, it is possible to remove a door if this should ever be required for a specific reason or procedure. If you need to remove a door, follow the related steps in Replacing the Doors (} page 93). Page 84 Refractive Index Detector (VC-D60) Operating Manual...
Solvents can spray when under high pressure. • Stop the pump flow prior to opening the flow path. • Wait until the system pressure is down to zero. • When opening the flow path, wear appropriate protective equipment. Refractive Index Detector (VC-D60) Page 85 Operating Manual...
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Always unplug the power cord before starting repair work inside the device. • If you were instructed to remove any housing covers or panels, do not connect the power cord to the device while the cover or panels are removed. Page 86 Refractive Index Detector (VC-D60) Operating Manual...
Decontamination is required, for example, when leakage or spillage has occurred, or before service or transport of the device. Use a suitable cleaning detergent or disinfectant to ensure that the treatment renders the device safe to handle. Refractive Index Detector (VC-D60) Page 87 Operating Manual...
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If necessary, slightly dampen the cloth or wipe with a solution of lukewarm water and a suitable cleaning detergent. 2. Allow the cleaning detergent to react as recommended by the manufacturer. Page 88 Refractive Index Detector (VC-D60) Operating Manual...
If span validation was successful, the validation date is updated. If span validation fails, contact Thermo Fisher Scientific Technical Support for assistance. Refractive Index Detector (VC-D60) Page 89 Operating Manual...
Never put hydrochloric acid in the flow cell. Use diluted (10-20%) or concentrated nitric acid as a cleaning solution instead. • The sample and reference cells should be filled with water or air (blown dry) before proceeding. Page 90 Refractive Index Detector (VC-D60) Operating Manual...
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Make sure to flush the flow path with deionized water before and after. Apply the nitric acid solution using a syringe and make sure the solution does not stay more than 5 minutes. Refractive Index Detector (VC-D60) Page 91 Operating Manual...
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(1) miscible with your mobile phase, (2) a good solvent for the predicted contaminant, and (3) generally of greater polarity than your mobile phase. Page 92 Refractive Index Detector (VC-D60) Operating Manual...
You can remove the door only when the hinges are in the grooves. Figure 21: Unhinging a door Description Hinge on the housing Reception groove on the door Refractive Index Detector (VC-D60) Page 93 Operating Manual...
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5. Insert the hinges in the groove, by pushing up and slightly turning the door. 6. Push the door downward to lock it in place. You can close the door only when it is properly installed. Page 94 Refractive Index Detector (VC-D60) Operating Manual...
Do not use repaired fuses and do not short-circuit the fuse holders. Follow these steps The fuse holder is located next to the main power switch. Figure 22: Fuse holder Description Main power switch (on/off control) Fuse holder Power-inlet connector Refractive Index Detector (VC-D60) Page 95 Operating Manual...
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Always replace both fuses. 3. Reinstall the fuse holder. 4. Reconnect the power cord to the power source and to the device. 5. Turn on the device with the main power switch. Page 96 Refractive Index Detector (VC-D60) Operating Manual...
2. Turn off the device with its main power switch and disconnect the power cord. 3. Remove all cables and flow connections to other devices. 4. Tighten the locking screws (see Tightening the Locking Screws (} page 98)). Refractive Index Detector (VC-D60) Page 97 Operating Manual...
(} page 101)). Follow these steps 1. Place the slide-in module on an even and clean surface with the bottom side facing up. 2. Gently tighten the 2 screws. Figure 23: Tightening the locking screws Page 98 Refractive Index Detector (VC-D60) Operating Manual...
• Fill in and sign the Health and Safety Form. Thermo Fisher Scientific refuses to accept devices for repair if the Health and Safety Form is missing, incompletely filled in, or unsigned. Refractive Index Detector (VC-D60) Page 99 Operating Manual...
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Thermo Fisher Scientific support organization for the appropriate procedure. Restarting the Device after Shipping To install the device after shipping, follow the instructions on mounting the system stack in the Vanquish System Operating Manual. Page 100 Refractive Index Detector (VC-D60) Operating Manual...
Transporting or Shipping the Detector (} page 97). Follow these steps 1. Loosen the four captive screws on the front left and front right of the device. Figure 24: Captive screws on the slide-in module Refractive Index Detector (VC-D60) Page 101 Operating Manual...
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Place the slide-in module on a clean and stable surface. 5. If the module is transported over a longer distance or if it is shipped: Fasten the locking screws (see Tightening the Locking Screws (} page 98)). Page 102 Refractive Index Detector (VC-D60) Operating Manual...
Physical handling of the device, including lifting or moving, requires a team effort of two persons. • A team effort is in particular required when lifting the device into the system stack or when removing it. Tools required Screwdriver, Torx T20 Refractive Index Detector (VC-D60) Page 103 Operating Manual...
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Figure 26: Inserting the slide-in module 4. To facilitate tightening the slide-in module in the enclosure, pull out the module a few millimeters (approximately 2 to 5 mm). Page 104 Refractive Index Detector (VC-D60) Operating Manual...
Refer to the Operating Manuals for the modules. 3. Before starting an analysis, let the chromatography system equilibrate and be sure that it is ready for operation. 4. In the Chromeleon software, run the device-specific Performance Qualification (PQ) tests. Refractive Index Detector (VC-D60) Page 105 Operating Manual...
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• Maintenance and Service Page 106 Refractive Index Detector (VC-D60) Operating Manual...
• Troubleshooting 8 Troubleshooting This chapter is a guide to troubleshooting issues that may arise during operation of the device. Refractive Index Detector (VC-D60) Page 107 Operating Manual...
The Instrument Audit Trails can be found on the ePanel Set (Audit ePanel). In addition, Audit Trails for each instrument are available in the Chromeleon 7 Console Data view, in the folder of the Instrument. Page 108 Refractive Index Detector (VC-D60) Operating Manual...
An error occurred during span validation. Verify that the sucrose span value could not be confirmed. solution was prepared as described in Performing Span Validation Please check the used sucrose solution (} page 89). and try again. Refractive Index Detector (VC-D60) Page 109 Operating Manual...
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V. Please ensure a stable environment and try again. Unstable Temperature The flow cell temperature has not met the preset temperature. For hints regarding temperature setting, see Flow Cell Temperature Setting (} page 79). Page 110 Refractive Index Detector (VC-D60) Operating Manual...
This section provides additional issues that may arise during operation of the device. Locate the table for the type of symptom you have, find the possible cause, and use the description of the solution to help you solve your problem quickly. Refractive Index Detector (VC-D60) Page 111 Operating Manual...
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Cyclic noise Waste line is too • Verify that you have installed the correct waste line at the matching the narrow outlet port. pump stroke • Check the waste line for crimps. frequency Page 112 Refractive Index Detector (VC-D60) Operating Manual...
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Intensity alarm Flow cell dirty Clean the reference and sample cells. See Cleaning the Flow Cell (} page 90). Lamp burned out Contact Technical Support. Flow cell empty Fill the flow cell with eluent. Refractive Index Detector (VC-D60) Page 113 Operating Manual...
• Specifications 9 Specifications This chapter provides the physical and performance specifications, including information about the materials used in the flow path of the device. Refractive Index Detector (VC-D60) Page 115 Operating Manual...
All system parameters are logged in the Chromeleon Audit Trail. features Biocompatible 1-13 For details, refer to Allowed pH Ranges (} page 25). Buffer concentration ≤ 1mol/L Chloride concentration ≤ 0.1 mol/L NP compatibility Page 116 Refractive Index Detector (VC-D60) Operating Manual...
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Materials in the flow path Stainless steel, PTFE, quartz glass Linearity < 5.0% RSD Noise ≤ 2.5 nRIU at retention time 3 s, data collection rate 50 Hz Drift ≤ 200 nRIU/hour at retention time 3 s, data collection rate 50 Hz Refractive Index Detector (VC-D60) Page 117 Operating Manual...
100 – 240 V AC, ± 10 %; 50/60 Hz; max. 250 W / 560 VA Overvoltage category Emission sound pressure level None Dimensions 16 x 42 x 62 cm (height x width x depth) Weight 16.5 kg Page 118 Refractive Index Detector (VC-D60) Operating Manual...
This chapter describes the standard accessories that are shipped with the device and the accessories that are available as an option. This chapter also provides information for reordering consumables and replacement parts. Refractive Index Detector (VC-D60) Page 119 Operating Manual...
Accessories, consumables, and replacement parts are always maintained at the latest technical standard. Therefore, part numbers are subject to change. If not otherwise stated, updated parts will be compatible with the parts they replace. Page 120 Refractive Index Detector (VC-D60) Operating Manual...
Tubing bracket USB cable, USB 2.0, high-speed, type A to B, 1m Viper capillary, 350 mm length, stainless steel, I.D. 0.18 mm Waste line For reordering information, see Consumables and Replacement Parts (} page 123). Refractive Index Detector (VC-D60) Page 121 Operating Manual...
Accessories, Consumables and Replacement Parts 10.3 Optional Accessories Item Part No. Flushing and injection kit for flow cells, including syringe 6078.4200 Analog I/O cable, 6 pin, for Vanquish Refractive Index Detectors 6060.0006 Page 122 Refractive Index Detector (VC-D60) Operating Manual...
Power cord, Denmark 6000.1070 Power cord, EU 6000.1000 Power cord, India, SA 6000.1090 Power cord, Italy 6000.1040 Power cord, Japan 6000.1050 Power cord, UK 6000.1020 Power cord, USA 6000.1001 Power cord, Switzerland 6000.1030 Refractive Index Detector (VC-D60) Page 123 Operating Manual...
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• Accessories, Consumables and Replacement Parts Page 124 Refractive Index Detector (VC-D60) Operating Manual...
• Appendix 11 Appendix This chapter provides additional information about compliance and the I/O pin assignment. Refractive Index Detector (VC-D60) Page 125 Operating Manual...
For more information, go to http://www.thermofisher.com/us/en/ home/technical-resources/rohs-certificates.html UKCA Declaration of Conformity The device has satisfied the requirements for the UKCA mark and is compliant with the applicable requirements. Page 126 Refractive Index Detector (VC-D60) Operating Manual...
Operation of this equipment in a residential area is likely to cause harmful interference, in which case the user will be required to correct the interference at his expense. Refractive Index Detector (VC-D60) Page 127 Operating Manual...
• Appendix 11.1.4 Manual Release History Revision Covering VC-D60-A-01 The instructions were prepared in English (original instructions). Other language versions are translations based on the English original instructions. Page 128 Refractive Index Detector (VC-D60) Operating Manual...
Figure 28: I/O port pin assignment Signal Name Wire Content color Integrator white Analog output: Sig(+) Range 500 µRIU: 500 µRIU/V Integrator black Range 125 µRIU: 125 µRIU/V Sig(-) Frame clear ground (FG) A_Zero Not used Purge Not used Not used Refractive Index Detector (VC-D60) Page 129 Operating Manual...
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