Shimadzu IonFocus Instruction Manual
  1. Manuals
  2. Brands
  3. Shimadzu Manuals
  4. Laboratory Equipment
  5. IonFocus
  6. Instruction manual
Shimadzu IonFocus Instruction Manual

Shimadzu IonFocus Instruction Manual

Atmospheric pressure ionization interface
Hide thumbs
Table of Contents

Advertisement

Quick Links

Download this manual
225-41675A
Jun. 2022
Atmospheric Pressure Ionization Interface
™
IonFocus
Unit
Instruction Manual
Read this manual thoroughly before you use the product.
Keep this manual for future reference.

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the IonFocus and is the answer not in the manual?

Questions and answers

Related Manuals for Shimadzu IonFocus

Summary of Contents for Shimadzu IonFocus

  • Page 1 225-41675A Jun. 2022 Atmospheric Pressure Ionization Interface ™ IonFocus Unit Instruction Manual Read this manual thoroughly before you use the product. Keep this manual for future reference.
  • Page 2 This page is intentionally left blank.
  • Page 3 • Note that Shimadzu will not be responsible for any damage resulting from operation of the product in accordance with this Instruction Manual. • Note that Shimadzu will not be responsible for the results of operating the product. • Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services, whether or not they are used with trademark symbol “TM”...
  • Page 4 Indicates an action that must be performed. Indicates information provided to improve product performance. Indicates the location of related reference information. Indicates buttons, menu items, settings, screens and windows, icon names, and other text displayed on-screen. 　Example: Click [OK]. ™ IonFocus Unit...
  • Page 5 If solvent gets into the eyes, blindness could result. Should solvent get into the eyes, flush immediately with large amounts of water and get medical attention. Always wear protective gloves when handling any toxic or biologically infectious samples. ™ IonFocus Unit...
  • Page 6 This may cause injury or damage the instrument. The cover does not need to be removed for routine maintenance or inspection. Repairs inside the product must be performed by Shimadzu service personnel. Contact your Shimadzu representative. Do NOT disassemble or modify the product without permission.
  • Page 7 Perform a full inspection before using the product again, and if necessary, contact your Shimadzu representative. Emergency stop procedure Turn OFF the power switches at the mass spectrometer as well as the high performance liquid chromatograph units.
  • Page 8 ↓ Ignition of flammable If any flammable gas of sufficient density is present in the substances vicinity, such gas will ignite. ™ IonFocus Unit...
  • Page 9 If the liquid to be drained into the waste container is virtually non-conductive (10 S/m or less), it will be necessary to add properly conductive, and therefore safe, liquid to the tank. This conductive liquid may be added to the waste container beforehand. ™ IonFocus Unit...
  • Page 10 Use tubing with an inner diameter of at least 2 mm for drain lines with high flow rates. Periodically check the tubing connections for air bubbles. Air bubbles in liquid can multiply the electrostatic charge by a factor of 20, 30 or more. viii ™ IonFocus Unit...
  • Page 11 Use as small a container as possible to minimize damage in the event of fire. This minimizes the damage in the event of fire. <Reference> Anti-static equipment (anti-static clothing, shoes and matting) and charge measurement equipment (electrometer) are sold by specialty manufacturers. ™ IonFocus Unit...
  • Page 12 PEEK resin tubes do not have sufficient strength and should they rupture, solvent may blow out. Black particles may build up on the APCI unit or ESI unit. Because of exposure to corrosive gases, you may need to replace parts at a shorter interval than specified. ™ IonFocus Unit...
  • Page 13 If corrosion on the aluminum surface is observed, wipe the surface clean. If necessary, polish the surface with lapping film. • Discoloration due to corrosion will not affect the performance of the system. ™ IonFocus Unit...
  • Page 14 In order to ensure safety, warning labels are attached in places requiring caution. If a warning label is lost or damaged, obtain a new label through your Shimadzu representative and attach it in the correct position. See "Warning Labels on the Equipment"...
  • Page 15 Safety Instructions xiii ™ IonFocus Unit...
  • Page 16 "List of Residual Risks". n Residual Risk Map The "Mechanical Location" and "No." indicated below are in accordance with those in "List of Residual Risks". For details, see "List of Residual Risks". ™ IonFocus Unit...
  • Page 17 "Warning Reference Labels" Analysis, Operation Category Maintenance Take care because Qualified the tip of the person corona needle is received sharp. Required training to Injury due to the Qualification/ control the corona needle. Education instrument, Service personnel ™ IonFocus Unit...

  • Page 18: Introduction

    Shimadzu may not be able to provide identical replacement products. 3. Limitation of Liability: (1) In no event will Shimadzu be liable for any lost revenue, profit or data, or for special, indirect, consequential, incidental or punitive damages, however caused regardless of the theory of liability, arising out of or related to the use of or inability to use the product, even if Shimadzu has been advised of the possibility of such damage.

  • Page 19: After-Sales Service And Availability Of Replacement Parts

    Thereafter, such parts may cease to be available. If Shimadzu receives notice of the discontinuation of units or parts, the necessary quantity for the above period is immediately calculated and secured. However, such units or parts...

  • Page 20: Table Of Contents

    Preparing for DUIS Analysis ............3.2.1 Mounting the DUIS Focus Unit ASSY ......3.2.2 Removing the DUIS Focus Unit ASSY Configuring the Software ........Troubleshooting Fault Diagnosis and Corrective Actions ............... 4.1.1 Data Acquisition xviii IonFocus ™ Unit...
  • Page 21 Contents Maintenance Periodic Inspections and Maintenance ......... 5.1.1 List of Periodic Inspections and Maintenance Maintenance of the IonFocus ESI Unit ............5.2.1 Replacing the Tubing ........5.2.2 Replacing the PEEK Tube ........5.2.3 Cleaning the Spray Unit ......
  • Page 22 This page is intentionally left blank.

  • Page 23: Outline And Configuration

    Outline and Configuration Outline IonFocus Unit, an ionization unit for NX series, is a heat-assisted ESI unit with ion transport electrodes installed to it. The ion transport electrodes enable efficiently introducing only ions into the mass spectrometer, achieving high sensitivity and high durability simultaneously.

  • Page 24: Component Parts

    Part Name Part No. Q'ty Remarks Ion focus ESI unit ASSY S225-19550-43 Focus unit ASSY S225-41576-41 DUIS focus unit ASSY S225-41576-42 Plug High-voltage socket blank Ground plate S225-41691 Knurled screw, GND S225-41682 Wrench, hex 1.5 Screwdriver, DS-13 ™ IonFocus Unit...

  • Page 25: Part Names And Functions

    Part Names and Functions Names of Parts IonFocus Unit ionizes the sample delivered from the liquid chromatograph at atmospheric pressure. With the ElectroSpray Ionization (ESI) method, the unit performs the ionization effective for ionic/highly polar compounds in the sample. In addition, the focus electrodes enables efficient introduction of ions into the mass spectrometer.
  • Page 26 2 Part Names and Functions ™ IonFocus Unit...
  • Page 27 2.1 Names of Parts Use of the DUIS focus electrodes enables analysis using the dual ion source (DUIS). ™ IonFocus Unit...

  • Page 28: Principle Of Ionization

    The charged droplets are transformed into very fine droplets through repetition of vaporization and disintegration, and ultimately it is thought that sample ions are released in the vapor phase. This state is called ion vaporization. ™ IonFocus Unit...

  • Page 29: Schematics Of Relevant Ionizations

    2.1 Names of Parts 2.1.2 Schematics of Relevant Ionizations n ESI n DUIS ™ IonFocus Unit...
  • Page 30 Part Name Part No. Capillary ASSY S225-14948-91 Heater ASSY S225-19560-46 Heater flange S225-19463-42 DL ASSY3 S225-15718-43 Focus unit ASSY S225-41576-41 DUIS focus unit ASSY S225-41576-42 Focus socket sub-ASSY S225-41578-42 Ground plate S225-41691 ™ IonFocus Unit...

  • Page 31: Mounting The Ground Plate

    Be sure to adjust the projection length of the ESI capillary to 0 mm or less. If the ESI capillary projects at all, the tip of the capillary may stick into your fingers during the work. Contact with fingers may also reduce sensitivity. Loosen the knurled screw 1. ™ IonFocus Unit...
  • Page 32 Hold the knob 2 of the ground plate and then put the hook on the shank of the knurled screw. Put the hook from the lower left of the knurled screw. Check that the upper side of the groove in the ground plate is in contact with the pin. ™ IonFocus Unit...

  • Page 33: Removing The Ground Plate

    Be sure to adjust the projection length of the ESI capillary to 0 mm or less. If the ESI capillary projects at all, the tip of the capillary may stick into your fingers during the work. Contact with fingers may also reduce sensitivity. ™ IonFocus Unit...
  • Page 34 3 Preparation To prevent the ground plate from falling, loosen the knurled screw 1 while holding the knob 2. Lift the ground plate to the upper left. Lower the ground plate and then pull it out toward you. ™ IonFocus Unit...

  • Page 35: Mounting The Focus Unit Assy

    If the ESI capillary projects at all, the tip of the capillary may stick into your fingers during the work. Contact with fingers may also reduce sensitivity. Remove the ground plate. "3.1.2 Removing the Ground Plate" P.11 ™ IonFocus Unit...
  • Page 36 Align the pin of the focus unit ASSY with the notch, and insert the ASSY as far as it will go. Visually check that the tip of the capillary is aligned with the center of the electrodes of the focus unit ASSY. Mount the ground plate. "3.1.1 Mounting the Ground Plate" P.9 ™ IonFocus Unit...

  • Page 37: Removing The Focus Unit Assy

    If the ESI capillary projects at all, the tip of the capillary may stick into your fingers during the work. Contact with fingers may also reduce sensitivity. Remove the ground plate. "3.1.2 Removing the Ground Plate" P.11 ™ IonFocus Unit...
  • Page 38 It is possible to perform analysis without mounting the focus unit ASSY. When not using the focus unit ASSY, be sure to attach the plug in order to prevent contamination of the parts where high voltage is applied. Mount the ground plate. "3.1.1 Mounting the Ground Plate" P.9 ™ IonFocus Unit...

  • Page 39: Mounting The Ionization Unit

    Check also that no dirt or dust is adhered to the tip of the capillary. "5.2.1 Replacing the Tubing" P.39 Do NOT knock the tip of the capillary tube against anything or contaminate it. This may reduce sensitivity. ™ IonFocus Unit...
  • Page 40 3 Preparation Insert the ionization unit in its hinges. Close the ionization unit and lock it by sliding the knob to the right. ™ IonFocus Unit...
  • Page 41 On the other hand, moving the probe closer may improve intensity. Analysis Method Flow Rate Spray Position 0.2 mL/min to 0.5 mL/min +1.5 mm to +3 mm ESI, DUIS 1 mL/min +3 mm or greater Auto tuning +1.5 mm ™ IonFocus Unit...
  • Page 42 3 Preparation Connect the tubing from the LC. ™ IonFocus Unit...

  • Page 43: Removing The Ionization Unit

    Turn the LC pump OFF and disconnect the tubing from the LC. Turn the gas OFF from LabSolutions. “LCMS Instruction Manual”, “Gas ON/OFF Status and Flow Rate Monitor” Unlock the ionization unit by sliding the knob to the left, and open the ionization unit. ™ IonFocus Unit...
  • Page 44 Lift the ionization unit upward to remove it. When removing the ionization unit, hold the parts shown in the following figure. Do NOT knock the tip of the capillary tube against anything or contaminate it. This may reduce sensitivity. ™ IonFocus Unit...
  • Page 45 3.1 Preparation for Analysis ™ IonFocus Unit...

  • Page 46: Preparing For Duis Analysis

    Turn the heater OFF from the LabSolutions before starting this work. If you proceed with the work while the temperature is still high, you may sustain burns. “LCMS Instruction Manual”, “Heater ON/OFF Status and Temperature Monitor” Remove the ground plate. "3.1.2 Removing the Ground Plate" P.11 ™ IonFocus Unit...
  • Page 47 3.2 Preparing for DUIS Analysis Remove the focus unit ASSY. ™ IonFocus Unit...
  • Page 48 Check that the tip of the corona needle is in the notch of the focus electrode 1 of the DUIS focus unit ASSY. If the tip of the corona needle does not enter the notch of the focus electrode 1, replace the corona needle. "5.2.5 Maintenance of the DUIS Focus Electrodes" P.58 ™ IonFocus Unit...
  • Page 49 "3.1.1 Mounting the Ground Plate" P.9 Close the ionization unit and lock it by sliding the knob to the right. "3.1.5 Mounting the Ionization Unit " P.17 Check the spray position. "3.1.5 Mounting the Ionization Unit " P.17 ™ IonFocus Unit...

  • Page 50: Removing The Duis Focus Unit Assy

    Take care because the tip of the needle unit is sharp. Remove the ionization unit. "3.1.6 Removing the Ionization Unit" P.21 Remove the ground plate. "3.1.2 Removing the Ground Plate" P.11 Remove the DUIS focus unit ASSY. ™ IonFocus Unit...
  • Page 51 ASSY. Mount the ground plate. "3.1.1 Mounting the Ground Plate" P.9 Close the ionization unit and lock it by sliding the knob to the right. "3.1.5 Mounting the Ionization Unit " P.17 ™ IonFocus Unit...

  • Page 52: Configuring The Software

    3 Preparation Configuring the Software Click (System Configuration). Select the instrument in the [System Configuration] window and then click [Properties]. ™ IonFocus Unit...
  • Page 53 3.3 Configuring the Software Check [Corona Needle] if necessary. Uncheck the box when performing analysis with the focus unit ASSY mounted to the ionization unit. ™ IonFocus Unit...
  • Page 54 3 Preparation Check the box when performing analysis with the DUIS focus unit ASSY mounted to the ionization unit. ™ IonFocus Unit...

  • Page 55: Troubleshooting

    For information on problems with the LCMS main unit, refer to “Troubleshooting” of “LCMS Instruction Manual”. If the problem is not resolved after taking the corrective action described here, or if the fault is considered to be one not described here, contact your Shimadzu representative. 4.1.1 Data Acquisition Problem...
  • Page 56 Focus Electrodes" P.58 The probe has not been Check the analysis method heated properly. parameters and the tuning file. Contact your Shimadzu representative if the situation does not improve. The interface current and Decrease the interface voltage and focus current are large.

  • Page 57: Periodic Inspections And Maintenance

    In order to use this product safely, make sure to carry out periodic inspections. Conduct everyday maintenance and management of performance as appropriate. For details on maintenance inspection contracts, consult your Shimadzu representative. Before starting inspection or maintenance, turn the power to the product OFF.

  • Page 58: List Of Periodic Inspections And Maintenance

    P.58 ✓ DUIS focus unit ASSY S225-41576-42 ✓ Corona needle S225-41587-41 Interface P.46 ✓* Holder S225-41572 ✓* Guide S225-41573 M6 PEEK washer for ✓ S023-65106-01 heater flange O-ring for the ✓* O-ring, 4D P95 S036-11267 ionization unit ™ IonFocus Unit...
  • Page 59 Wipe. Ultrasonically ✓ Guide clean if the soiling is severe Wipe. Ultrasonically ✓ Drain mesh clean if the soiling is severe The cleaning frequency may differ depending on the operating conditions at your site. ™ IonFocus Unit...

  • Page 60: Maintenance Of The Ionfocus Esi Unit

    5 Maintenance Maintenance of the IonFocus ESI Unit Before performing maintenance work, turn the high voltage OFF from the LabSolutions software. If you do not turn the high voltage OFF, there will be a danger of electric shock. “LCMS Instruction Manual”, “Turning the High Voltage ON/OFF”...

  • Page 61: Replacing The Tubing

    5.2 Maintenance of the IonFocus ESI Unit 5.2.1 Replacing the Tubing A high voltage (up to 5 kV) is applied to the sample solution sprayed from the tip of the capillary ASSY in order to ionize the sample. If the fine capillary ASSY tubing becomes blocked due to very small particles of contamination that get into the mobile phase or the sample, it may lead to a rise in the pump pressure.
  • Page 62 Loosen the male nut 2 by hand and remove it. Loosen the ESI coupling 3 with a wrench. Remove the knurled screw 4. Completely loosen the ESI coupling 5, and remove it in the direction indicated by the arrow. ™ IonFocus Unit...
  • Page 63 5.2 Maintenance of the IonFocus ESI Unit Replace the capillary ASSY. Remove the capillary ASSY 2 from the ESI coupling 1. Mount the new capillary ASSY 3 on the ESI coupling 1. Tighten it firmly by hand. Make sure that the tip of the ESI tubing is not either projecting too far or too recessed.
  • Page 64 "7.3.1 Ionization Unit" P.71 Tighten the ESI coupling 1 by hand and then turn it with a wrench to adjust the projection of the tip. Make the tip of the capillary ASSY project about 0.5 to 1 mm. ™ IonFocus Unit...
  • Page 65 5.2 Maintenance of the IonFocus ESI Unit Secure the ESI coupling in place. Tighten the knurled screw 1 by hand to fix the position of the ESI coupling . Tighten the male nut 2 by hand to secure the PEEK tube .

  • Page 66: Replacing The Peek Tube

    In addition, the sensitivity may decrease due to the contamination or clogging in the tube. Parts used Part Name Part No. PEEK tube, φ1.6 x φ0.13, red, 3 m Turn the LC pump OFF and disconnect the tubing from the LC. ™ IonFocus Unit...
  • Page 67 5.2 Maintenance of the IonFocus ESI Unit Replace the PEEK tube. Remove the male nuts 1 at both ends and remove the PEEK tube 2. Replace the PEEK tube with a new one. The standard tube length is 420 mm.

  • Page 68: Cleaning The Spray Unit

    Failure to observe this instruction may result in burn injury. Remove the ground plate and the focus unit ASSY or the DUIS focus unit ASSY. "3.1.4 Removing the Focus Unit ASSY" P.15 "3.2.2 Removing the DUIS Focus Unit ASSY" P.28 ™ IonFocus Unit...
  • Page 69 5.2 Maintenance of the IonFocus ESI Unit n Routine inspection Wipe off soiling. Moisten gauze with a solvent that can remove soiling (such as water/methanol) and wipe any soiling off with the gauze. Clean the locations indicated below. • Holder •...
  • Page 70 Do not clean the tip of the DL because cleaning it may cause the tubing to clog. If the tip of the DL is badly soiled, replace the DL. For replacement of the DL, refer to “LCMS Instruction Manual”. ™ IonFocus Unit...
  • Page 71 5.2 Maintenance of the IonFocus ESI Unit n If the soiling is severe Remove the heater flange. Loosen the two screws 1 with the included hexagon wrench. Insert the included drawing tool 2 under the heat block 3 and remove the heater flange 4.
  • Page 72 Moisten gauze with a solvent that can remove soiling (such as water/methanol) and wipe any soiling off with the gauze. If the heat block is soiled, scrub it with a nylon brush and then wipe it clean with gauze. ™ IonFocus Unit...
  • Page 73 5.2 Maintenance of the IonFocus ESI Unit Remove the drain mesh. Lift the drain mesh up with tweezers. Subject the holder, guide, screws and drain mesh to ultrasonic cleaning in a methanol solution. If the holder, screws, and drain mesh are badly soiled, polish the parts with about 4-micron lapping film.

  • Page 74: Maintenance Of The Focus Electrodes

    If you do not turn the high voltage OFF, there will be a danger of electric shock. “LCMS Instruction Manual”, “Turning the High Voltage ON/OFF” Parts used Part Name Part No. Ground plate S225-41691 Focus unit ASSY S225-41576-41 Focus electrode 1 S225-41561 Focus electrode 2 S225-41574 ™ IonFocus Unit...
  • Page 75 5.2 Maintenance of the IonFocus ESI Unit Remove the ionization unit. "3.1.6 Removing the Ionization Unit" P.21 The inside of the ionization unit reaches a high temperature. Wait until the temperature decreases sufficiently before handling or servicing the area. The inside of the ionization unit and the area around the DL and heat block reach high temperatures.
  • Page 76 Remove the focus electrode 1 and focus electrode 2 from the focus unit ASSY. Loosen the knurled nut 2 1. Remove the focus electrode 2 2. Loosen the knurled nut 1 3. Remove the focus electrode 1 4. ™ IonFocus Unit...
  • Page 77 5.2 Maintenance of the IonFocus ESI Unit Immerse the ground plate, focus electrode 1, and focus electrode 2 in methanol solution, then subject them to ultrasonic cleaning. Be sure to remove the focus electrode 1 and focus electrode 2 from the focus unit ASSY before ultrasonic cleaning.
  • Page 78 2 4. Fix it with the knurled nut 1 3. Align the pin of the focus unit ASSY with the notch and then attach the focus electrode 1 2. Fix it with the knurled nut 2 1. ™ IonFocus Unit...
  • Page 79 5.2 Maintenance of the IonFocus ESI Unit Mount the focus unit ASSY. "3.1.3 Mounting the Focus Unit ASSY" P.13 Align the pin of the focus unit ASSY with the notch, and insert the ASSY as far as it will go.

  • Page 80: Maintenance Of The Duis Focus Electrodes

    If you do not turn the high voltage OFF, there will be a danger of electric shock. “LCMS Instruction Manual”, “Turning the High Voltage ON/OFF” Parts used Part Name Part No. Ground plate S225-41691 DUIS focus unit ASSY S225-41576-42 Corona needle S225-41587-41 Focus electrode 1 S225-41561 ™ IonFocus Unit...
  • Page 81 5.2 Maintenance of the IonFocus ESI Unit Part Name Part No. Focus electrode 2 S225-41574 Remove the ionization unit. "3.1.6 Removing the Ionization Unit" P.21 The inside of the ionization unit reaches a high temperature. Wait until the temperature decreases sufficiently before handling or servicing the area.
  • Page 82 Remove the corona needle by loosening it with a screwdriver. Polish the tip of the corona needle. Polish the tip of the corona needle using about 4-micron lapping film. Take care not to round off the tip. ™ IonFocus Unit...
  • Page 83 5.2 Maintenance of the IonFocus ESI Unit Remove the focus electrode 1 and focus electrode 2 from the focus unit ASSY. Loosen the knurled nut 2 1. Remove the focus electrode 2 2. Loosen the knurled nut 1 3. Remove the focus electrode 1 4.
  • Page 84 If the parts are badly soiled, polish them with about 4-micron lapping film. If ultrasonic cleaning and polishing with the lapping film cannot remove the soiling, it is recommended to replace the focus electrode 1, focus electrode 2, or focus unit ASSY. ™ IonFocus Unit...
  • Page 85 5.2 Maintenance of the IonFocus ESI Unit Attach the focus electrode 1 and focus electrode 2 to the DUIS focus unit ASSY. Align the pin of the DUIS focus unit ASSY with the notch and then attach the focus electrode 1 4.
  • Page 86 Align the pin of the focus unit ASSY with the notch, and insert the ASSY as far as it will go. Visually check that the tip of the capillary is aligned with the center of the electrodes of the focus unit ASSY. Mount the ground plate. "3.1.1 Mounting the Ground Plate" P.9 ™ IonFocus Unit...
  • Page 87 5.2 Maintenance of the IonFocus ESI Unit Mount the ionization unit. "3.1.5 Mounting the Ionization Unit " P.17 ™ IonFocus Unit...

  • Page 88: Specifications

    Required gas Supply pressure: 500 to 800 kPa Purity: 99.99 % or greater Flow rate during use: Approx. 10 mL/min Dry air Supply pressure: 690 to 800 kPa Purity: Water-free, Oil-free Max. flow rate 25 L/min during use: ™ IonFocus Unit...

  • Page 89: Maintenance Parts 7.1 Consumables

    "5.2.1 Replacing the Tubing" P.39 　 PEEK TUBE 5999 S228-32999-01 "5.2.2 Replacing the PEEK Tube" P.44 DUIS 　 CORONA NEEDLE S225-41587-41 For IonFocus ESI unit Interface ASSY GUIDE S225-41573 　 WASHER PEEK S023-65106-01 Seal for fixed part of heater flange ™...

  • Page 90: Spare Parts

    　 O-RING, 4D P95 S036-11267 　 O-RING, 4D S18 S036-19004-14 　 O-RING, 4D P30 S036-11233 ESI unit 　 ION FOCUS ESI UNIT ASSY S225-19550-43 ESI unit body HEATER ASSY, NX S225-19560-46 HEATER,SUPPORT PLATE S225-42245-41 ASSY ,PM ESI HEATER 2 S225-34722 ™ IonFocus Unit...
  • Page 91 LOW HEAD SCREW M3×5, S225-14287-44 For securing the SUPPORT PLATE NICKEL PLATED WASHER, UUW-0309-10H S023-66210-03 HEATER CABLE ASSY, NX S225-19494-45 FOCUS UNIT ASSY FOCUS ELECTRODE 1 S225-41561 FOCUS ELECTRODE 2 S225-41574 KNURLED NUT 1 S225-41563 KNURLED NUT 2 S225-41558 ™ IonFocus Unit...

  • Page 92: Unit Configurations

    PCB-ASSY, IFHV-DIV S225-41610-41 focus Unit Configurations Part Name Part No. Remarks IONIZATION UNIT S225-19550-43 FOCUS UNIT ASSY S225-41576-41 DUIS FOCUS UNIT ASSY S225-41576-42 IF BLOCK ASSY HEATER FLANGE ASSY S225-19463-42 FOCUS SOCKET ASSY HEATER ASSY, NX S225-19560-46 ™ IonFocus Unit...

  • Page 93: Ionization Unit

    FOCUS SOCKET CABLE ASSY S225-19473-42 HV cable for ion focus HEATER CABLE ASSY, NX S225-19494-45 GND CABLE ASSY S225-41592-41 GND cable for ion focus Includes No.10, 14, 16, 17, HEATER,SUPPORT PLATE ASSY ,PM S225-42245-41 18, 19, 20 ™ IonFocus Unit...
  • Page 94 7 Maintenance Parts ™ IonFocus Unit...

  • Page 95: Heater Assy, Nx

    MESH, NX, 4 S225-41672 MESH KIT S225-42246-41 Includes No.4, 5, 6, 7 7.3.3 Focus Unit ASSY Part Name Part No. Remarks FOCUS ELECTRODE 1 S225-41561 FOCUS ELECTRODE 2 S225-41574 KNURLED SCREW 1 S225-41563 KNURLED SCREW 2 S225-41558 ™ IonFocus Unit...

  • Page 96: Duis Focus Unit Assy

    FOCUS ELECTRODE 2 S225-41574 KNURLED SCREW 1 S225-41563 KNURLED SCREW 2 S225-41558 NEEDLE ASSY D S225-41587-41 7.3.5 Focus Socket ASSY Part Name Part No. Remarks FOCUS SOCKET SUB-ASSY S225-41578-42 Voltage divider board for PCB-ASSY, IFHV-DIV S225-41610-41 ion focus ™ IonFocus Unit...

  • Page 97: If Block Assy

    7.3 Unit Configurations 7.3.6 IF Block ASSY Part Name Part No. Remarks HEATER FLANGE ASSY S225-19463-42 ™ IonFocus Unit...
  • Page 98 S225-41573 BLOCK, HEATER S225-15488 INSULATOR BLOCK S225-15489 HEATER ASSY S225-15716-41 INSULATOR, FLANGE S225-15491 BUSH, HEATER S225-15498 O-RING, 4D-S18 S036-19004-14 O-RING, 4D S14 S036-19004-11 O-RING, 4D-S10 S036-19004-07 LOW HEAD,M3X5,ADD,NICKEL PLT S225-14287-46 BOLT M6X16 S225-19636 WASHER S023-65106-01 HOLDER S225-41572 ™ IonFocus Unit...

  • Page 99: Index

    17, 39 DUIS Analysis DUIS Focus Electrodes DUIS Focus Unit ASSY 24, 26, 59 ESI coupling Focus Electrodes Focus Unit ASSY 13, 15, 25, 53 Ground Plate 9, 11 hexafluoroisopropanol IonFocus ESI PEEK Tube IonFocus ™ Unit...
  • Page 100 This page is intentionally left blank.

Table of Contents