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- Page 1 206-97457 Aug. 2011 ISR-2600 for UV-2600/2700 ISR-2600Plus for UV-2600 Integrating Sphere Attachment INSTRUCTION MANUAL Read the instruction manual thoroughly before you use the product. Keep this instruction manual for future reference.
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- Page 3 • Copyright of this manual is owned by Shimadzu Corporation. Reproduction or duplication of its content, in whole or part, without permission of the copyright holder is strictly prohibited.
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Page 4: Notations Used In This Manual
Emphasizes additional information that is provided to ensure the proper use of this product. The following pictorial symbol is used in this manual: Notation Description Indicates the location of related information in the instruction manuals. ii ISR-2600/2600Plus... -
Page 5: Safety Instructions
Doing so may cause injury or product malfunction. The cover does not need to be removed for routine maintenance, inspection, and adjustment. Before attempting repairs that require the cover to be removed, contact your Shimadzu representative. Procedures in Emergency or Power Failure Situations There are no procedures specifically required for this product. -
Page 6: Warranty
Shimadzu may not be able to provide identical replacement products. 3. Limitation of 1. In no event will Shimadzu be liable for any lost revenue, profit or data, or for special, indirect, consequential, incidental or punitive damages, however caused Liability:... -
Page 7: After-Sales Service And Replacement Parts Availability
Note, however, that the availability of units or parts not manufactured by Shimadzu shall be determined by the relevant manufacturers. If Shimadzu receives notice of the discontinuation of units or parts, the necessary quantity for the above period is immediately calculated and secured. -
Page 8: Disposal Precautions
WEEE Mark With your co-operation we are aiming to reduce contamination from waste electronic and electrical equipment and preserve natural resource through re-use and recycling. Do not hesitate to ask Shimadzu service representative, if you require further information. vi ISR-2600/2600Plus... -
Page 9: Table Of Contents
3.7 Using (Optical Beam) Masks ................13 3.8 Using the Powder Sample Holder ..............14 Inspection and Maintenance ..........15 4.1 Inspection and Maintenance................15 4.2 Sample Compartment Inspection ..............15 4.3 Cleaning the Exterior ..................16 4.4 Maintenance Parts ..................16 Troubleshooting..............17 5.1 Symptoms and Remedial Actions..............17 ISR-2600/2600Plus... - Page 10 Contents References................19 6.1 Specifications....................19 6.2 Optional Accessories ..................20 6.3 Cells....................... 20 viii ISR-2600/2600Plus...
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Page 11: Overview
UVProbe, which is control software for spectrophotometers. • Measurement can be performed on liquid samples contained in a cell and solid samples. • The ISR-2600 can be mounted to the UV-2600/2700, and the ISR-2600Plus to the UV-2600. 1.2 Parts List This instrument contains the following parts. - Page 12 (Filled with barium sulfate powder) Square cell holder for transmission 204-52472-01 measurement Film holder 204-03878-03 Mask (2 x 5) 206-61585-03 Mask (5 x 5) 206-61585-02 Knurled screw 202-31975-01 Glass rod 201-99041 Barium sulfate powder, 500 g 017-41646-01 Instruction Manual (this manual) 206-97457 2 ISR-2600/2600Plus...
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Page 13: Mounting
Refer to "5.2 Remove/Install the Sample Compartment U nit (Standard)" in "Shimadzu UV-Visible Spectrophotometer UV-2600/2700 INSTRUCT ION MANUAL". Fit this instrument into the s ample compartment section. - Page 14 [I/O 1] connector for the external detector on the left side of the spectrophotometer. When c orrectly oriented, the hinges at both ends of the connector will fit into place with a click. Connector for ISR unit Fig 1.4 Connector for the External Detector of the Spectrophotometer 4 ISR-2600/2600Plus...
- Page 15 During normal m easurement, nothing is set in the mask holders (Fig 1.5). "3.7 Using (Optical Beam) Masks". Close the sample compartment cover. Turn on the power switch of the spectrophotometer. ISR-2600/2600Plus 5...
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Page 16: Removal
• Handle this instrument with care so that you do not drop it or bang it against surrounding objects. Strong impact brought to this instrument may damage the barium sulfate coating on the inner surface of the integrating sphere, leading to possible performance degradation. 6 ISR-2600/2600Plus... -
Page 17: Structure
8-degree specular reflectance in the reflectance measurement position on the reference side. "3.1 Setting the Conditions". Mirror M3 Mask Reference light Mirror M2 8 degrees 90 degrees Mask φ60 integrating sphere Sample light Mirror M1 Fig 2.1 Optical System Diagram ISR-2600/2600Plus 7... -
Page 18: Components
Sample holder (S side) This bar keeps the sample on the sample side in close contact. Sample holder (R side) This bar keeps the sample on the reference side in close contact. Signal cable This cable connects to the spectrophotometer and helps send measurement signals. 8 ISR-2600/2600Plus... -
Page 19: Basic Operation
Detector Unit When using this instrument, switch the setting for the detector unit. • [Direct]: Use the detector mounted on the spectrophotometer. • [External(1Detector)]: Use the integrating sphere attachment ISR-2600. • [External(2Detector)]: Use the integrating sphere attachment ISR-2600Plus. Light Source Change... -
Page 20: Basic Operation
Remove the standard white plate on the sample side of the integrating sphere and then set a target sample in its place for measurement. Knurled screw Integrating sphere Powder sample holder Fig 3.2 Mounting a Powder Sample Holder 10 ISR-2600/2600Plus... -
Page 21: Measuring Diffuse Reflectance
An aluminum mirror is usually employed as a reference mirror. Reference mirrors are not supplied as standard accessories. If you do not have any appropriate mirrors, procure them separately. ISR-2600/2600Plus 11... -
Page 22: Measuring Transmittance Of A Liquid Sample
10-mm square cell. Put the sample in the square cell an d ca rry out the measurement. Square cell holder Blank sample or measurement sample Standard white plate Fig 3.5 Measurement of Transmittance of a Liquid Sample 12 ISR-2600/2600Plus... -
Page 23: Measuring Transmittance Of A Film Sample
The use of masks reduces the beam angle with respect to the center line of the sample light beam (to less than 5 degrees with 5 x 5 masks), providing an irradiation beam that is closer to parallel light as compared to that obtained without masks. ISR-2600/2600Plus 13... -
Page 24: Using The Powder Sample Holder
Compacting using chemical wrapping paper inserted between the glass rod and barium sulfate or the powder sample makes filling of the powder sample holder easier.This technique is an effective way out when the filling is not easy due to the powder sticking to the glass rod. 14 ISR-2600/2600Plus... -
Page 25: Inspection And Maintenance
• Do not remove the covers of this instrument under any circumstances. Doing so may cause an electric shock, injury, or instrument malfunction. Repairs that require any covers to be removed must be performed by a Shimadzu representative. If you require such repairs to be carried out, contact your Shimadzu representative. -
Page 26: Cleaning The Exterior
"Fig 3.8 Filling the Powder Sample Holder"). Should the interior of the integrating sphere have become discolored, it cannot be re-coated with barium sulfate. In this case, contact your Shimadzu representative to have the integrating sphere assembly replaced. 4.4 Maintenance Parts... -
Page 27: Troubleshooting
Check whether the problem exhibits the following symptoms before requesting repairs. Contact your Shimadzu representative if the error cannot be resolved through the remedial action described below, or if any symptom occurs that is not listed below. Symptom... - Page 28 Are you using an optional Depending on an optional accessory? accessory you use, the performance specifications for the baseline, etc., of the spectrophotometer may not be satisfied. 18 ISR-2600/2600Plus...
- Page 29 Slit width: 5 nm Slit width: 5 nm UV-2600: Max. 0.1%T RMS at a UV-2600: Max. 0.1%T RMS at a wavelength of wavelength of 500 nm 500 nm UV-2700: Max. 0.3%T RMS at a wavelength of 500 nm ISR-2600/2600Plus 19...
- Page 30 200-34655 200-34662-11 length cell length cell is required. l = 5 mm 200-34449 200-34449-01 For 1 mm 204-21473-03 Spacer for short Not required. For 2 mm 204-21473-01 optical length cell For 5 mm 204-21473-02 Fig 6.1 Cell Appearances 20 ISR-2600/2600Plus...
- Page 31 Record of Revision Date Revision Changed Page Description...
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