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Summary of Contents for Shimadzu LCMS-8050
- Page 1 ZEBV-5073B Shimadzu High-Performance Liquid Chromatograph Mass Spectrometer LCMS-8050 LCMS-8045 Pre-Installation Requirements (Installation Preparations/Confirmation)
- Page 2 Notice (1) All rights are reserved, including those to reproduce this manual or parts thereof in any form without permission in writing from Shimadzu Corporation. Copyright 2018 Shimadzu Corporation (2) Information in this manual is subject to change without notice and does not represent a commitment on the part of the vendor.
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Page 3: Table Of Contents
Contents Contents 1. INTRODUCTION ..............3 2. INSTALLATION CONDITIONS ..........5 2.1 Corrosive Gas and Dust ...............5 2.2 Ventilation and Open Flame Precautions ........5 2.3 Electromagnetic Noise ..............5 2.4 Installation Space .................5 2.5 Other Installation Conditions ............5 2.6 System Size (Dimensions and Weight) ........6 2.7 System Installation Example ............6 2.7.1 Connecting to the Rotary Pump .............. - Page 4 Contents This page is intentionally left blank. LCMS-8045/8050 Pre-Installation Requirements...
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Page 5: Introduction
These Pre-Installation Requirements describe prior preparation required at the customer's site in order to facilitate installation of the LCMS-8045 and LCMS-8050. Please make sure that the content of this document is carefully observed to ensure that the instrument functions stably, providing data acquisition with a high degree of reliability. - Page 6 1 Introduction This page is intentionally left blank. LCMS-8045/8050 Pre-Installation Requirements...
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Page 7: Installation Conditions
2 Installation Conditions 2. Installation Conditions Be sure to read the installation precautions described below to ensure correct and safe use of the instrument. Also, follow the precautions given in the Safety Precautions of the instruction manual that came with the instrument. 2.1 Corrosive Gas and Dust To prolong the service life and performance of the instrument, avoid installing the instrument in dusty locations or locations subject to corrosive gases. -
Page 8: System Size (Dimensions And Weight)
2 Installation Conditions 2.6 System Size (Dimensions and Weight) Dimensions (mm) Weight (kg) LCMS-8050 / 8045 1180 Rotary pump E2M28 Rotary pump (with Oil mist filter) 2.7 System Installation Example Unit: mm E2M28 Power cable (With oil mist filter) 2500 Evacuation hose (length: 1.2 m from the back of the MS unit) -
Page 9: Connecting To The Rotary Pump
SI Cover LC-Mikros 2.7.1 Connecting to the Rotary Pump Use the rotary pump specified by Shimadzu. Using a different pump may impair the intended performance of the instrument. It may also cause an accident L: 1200 mm, OD: 41mm Evacuation hose Impossible to extend. -
Page 10: Connecting To A Pc
2 Installation Conditions 2.7.2 Connecting to a PC Connect to the PC using the USB cable. Limit the length of the USB cable to (USB cable is standard accessory of LCMS) (Standard LCMS-8045/8050 System) USB cable Max. length 3 m (Micro ESI 8060 / LCMS-8045/8050 System) Caution) USB port for... -
Page 11: Required Power Supply
2 Installation Conditions 2.8 Required Power Supply Unit Voltage Current LCMS-8050, 8045 230 VAC, single-phase (50/60 Hz) 15(A) (including E2M28 rotary pump) LC system * See the LC Pre-Installation Requirements. PC, Monitor, Printer * See the respective instruction manual. Nitrogen gas generator * See the Pre-Installation Requirements of Nitrogen generator. -
Page 12: Gas
(*4) LCMS-8045: 230 (kPa) Argon 500 to 800 CID gas 99.99 % or more LCMS-8050: 270 (kPa) (kPa) 450 (kPa) See * 2.9.2 *1 Organic-free nitrogen gas *2 Use of a hydrocarbon trap is recommended. *3 When using a gas cylinder for synthetic air, 690〜800(kpa) is required for the supply pressure where an atmospheric composition needs CO:less than 1ppm, CO2:less than 1ppm, HC:less than 1ppm, H2O:-50℃(dew point). -
Page 13: Nebulizer Gas Drying Gas And Heating Gas
2 Installation Conditions 2.9.1 Nebulizer Gas Drying Gas and Heating Gas Prepare resin tubing of O.D. 6 mm (I.D. 4 mm) for connecting these gases. This tube need not be prepared for the nitrogen gas generator (GENIUS1051) since O.D. 6 mm tube is provided as standard. When using other nitrogen gas generators or centralized piping, for example, replace the tubes seeing 2.9.1.2 to 2.9.1.4, and prepare O.D. -
Page 14: Using Gas Generated From Centralized Piping (Liquid Nitrogen)
Gas piping adapter kit 1 pc Pressure regulator S221-35999-01 Model: PPR-N2 Piping between gas cylinder and LCMS The following gas supply pipes are available from Shimadzu. Please order them in advance. Part Number Part Name S201-48067 Gas supply pipe Length: 2.5 m... -
Page 15: When The Customer Already Has A Nitrogen Gas Generator
CID gas Argon gas For carrier gas supply pipe (M type) Piping between argon gas cylinder and LCMS The following gas supply pipes are available from Shimadzu. Please order them in advance. Part Number Part Name S221-35999-01 (1) Pressure Regurator... - Page 16 2 Installation Conditions LCMS-8050 47L (7m ) Cylinder In case of setting CID gas flow rate to standard (270kPa) Reference operating time: 7,000 (L) / 0.012(L/min) / 60 (min) / 24(h) = approx. 405(days) In case of setting CID gas flow rate to maximum (450kPa) Reference operating time: 7,000 (L) / 0.020 (L/min) / 60 (min) / 24(h) = approx.
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Page 17: Evacuation System
2 Installation Conditions 2.10 Evacuation System To keep the room clean, the evacuation gases from the rotary pump and the vapors from solvents used for mobile phases must be vented to evacuation equipment such as a draft chamber or exhaust facilities. The system comes with 5-meter evacuation hoses respectively for venting the rotary pump and the drain containers. -
Page 18: Reagents And Mobile Phase
2 Installation Conditions 2.11 Reagents and Mobile Phase Prepare the following required items beforehand. Standard samples for adjusting instrument (S225-14122-01) PEG (polyethylene glycol) + PPG (polypropylene glycol) + Raffinose 200 mL Samples for checking sensitivity (S225-06613-14) (for ESI/APCI) 1 mL ampule × 2 Reserpine (1 ng/uL) Sample for checking sensitivity (S225-06613-13) -
Page 19: Import (Packing Box Size)
2 Installation Conditions 2.13 Import (Packing box size) The instrument comes in the packing box of following size and excessive tilting is not allowed. Please prepare for it by checking the following points: Availability/non-availability of an elevator Carry-in route Carry-in equipments (forklift) if necessary, etc. Size : 1400 (W) x 900 (D) x 820 (H) Weight... -
Page 21: Preliminary Check List
3. Preliminary Check List Address: The following page summarizes each of the installation conditions described so far as a check list. The customer should fill in this sheet himself and hand it over to the Shimadzu representative. Customer: Address: TEL:... - Page 22 (for ESI/APC/Micro ESII) installation ▪ Acetophenone (for DUIS) ▪ Drain bottle ▪ Reservoir bottle (mobile phase) 6.Other Check with the Shimadzu representative as necessary. ▪ (Maintenance parts, consumables) An elevator must be available when installing the instrument on 7.Carry-in Carry-in route and the second or higher floor above the ground.
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