Related Manuals for Ametek ta7000R
Summary of Contents for Ametek ta7000R
- Page 1 TRACE ANALYTICAL MODEL ta7000R User Manual Process Instruments Western Research 455 Corporate Boulevard Newark, DE 19702 PN T900-013 Rev. A...
- Page 2 © 2004 AMETEK Process & Analytical Instruments Division This document contains Information for the use of the Model ta7000R Gas Purity Monitor. Data herein has been verified and validated and is believed adequate for the intended use of this instrument. If the instrument or procedures are used for purposes over and above the ca- pabilities specified herein, confirmation of their validity and suitability should be obtained;...
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Page 3: Table Of Contents
Contents About This Document ..................5 Safety Notes ......................5 Grounding ......................6 Important Safety Information ................6 Warning Labels ...................... 7 Electromatic Compatibility (EMC) ..............8 General Safety Considerations ................9 Electric Hazard ..................9 UV Light ....................9 Mercury Vapor .................. - Page 4 Auto Calibration ....................39 Manual Calibration ..................... 40 Non Volatile RAM ....................42 Run ......................42 Blank ......................43 Shut Down ......................44 Description of Internal Components 45 Error Messages ..................46 Dimensional Drawings ................ 48 4 | Model ta7000R Gas Purity Monitor...
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Page 5: About This Document
About This Document This manual is intended as a guide for operation of the ta7000R. This manual is notintended as a service guide and does not contain service information. The ta7000R should only be operated by personnel who have been properly trained in the procedures required for safe operation of the ta7000R. -
Page 6: Grounding
Verify ground continuity of all equipment before applying power. Important Safety Information Before working on the ta7000R, read and understand the following Notes, Warnings, and Cautions, regarding safety and other required information. Additional Notes, Warnings, and Cautions included in individual proce- dures in this manual indicate special conditions to consider during instal- lation, before opening the heater and while working on it. -
Page 7: Warning Labels
Achtung - Heiße Oberfläche Environmental Information (WEEE) This AMETEK product contains materials that can be reclaimed and recycled. In some cases the product may contain materials known to be hazardous to the environment or human health. In order to prevent the release of harmful substances into the environment and to conserve our natural resources, AMETEK recommends that you arrange to recycle this product when it reaches its “end of life.”... -
Page 8: Electromatic Compatibility (Emc)
Heater or the overall system. Examples of electrical events and devices known for the gen- eration of harmful electromagnetic disturbances include motors, capacitor bank switching, storm related transients, RF welding equipment, static, and walkie-talkies. 8 | Model ta7000R Gas Purity Monitor... -
Page 9: General Safety Considerations
General Safety Considerations Components and Functions The following safety items must be observed to avoid personal injury and to prevent damage to the RGD analyzer. All personnel involved in instal- lation, operation or service of the analyzer should be thoroughly familiar with these items. -
Page 10: Warranty And Claims
(90) days from date of shipment. Resale items warranty is limited to the transferable portion of the original equipment manufacturer’s warranty to AMETEK. If you are returning equipment from outside the United State, a statement should appear on the documentation ac- companying the equipment being returned declaring that the goods being returned for repair are American goods, the name of the firm who purchased the goods, and the shipment date. -
Page 11: Overview
OVERVIEW Model ta Gas Purity Monitor Introduction The ta7000R Process Gas Analyzer is a trace level gas chromatograph ca- pable of detecting sub-ppb concentrations of contaminants in sample gas matrices. The system consists of a microprocessor controlled gas chro- matograph utilizing the Unique Reduction Gas Detector (RGD) designed by Trace Analytical. -
Page 12: Reduction Gas Detection
External signal outputs for a data collection system or host computer are located at the rear panel. The microprocessor control system allows complete unattended operation of the ta7000R. This onboard system performs necessary operational and analytical functions such as: •... - Page 13 • · Sampling Frequency • · Data Output • · Alarm Output Data is presented via the front display panel. Alternatively data may be obtained through an RS232 serial computer interface and HP/GL parallel printer interface located on the rear panel. With optional interface kits, two components may be assigned to separate trend channels to provide a continuous signal proportional to the con- centration of the assigned component.
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Page 15: Specifications
SPECIFICATIONS Model designation and detection limit specifi cations Sample Gas Model Lower Detection Limit H2 ppb CO ppb Nitrogen ta7000R-N2 < 0.5 < 0.5 Argon ta7000R-Ar < 0.5 < 0.5 Helium ta7000R-He < 0.5 < 0.5 Oxygen ta7000R-O2 < 0.5 <... -
Page 16: Sample Gas Supplies
70 to 90 psig (4.8 to 6.1 bar) Inlet pressure stability + 2%, UHP regulator required Vent pressure Atmospheric pressure vent is opti mal, + 0.5 psig maximum FlowRate 300 cc/min minimum, sample bypass at 50 cc/min 16 | Model ta7000R Gas Purity Monitor... -
Page 17: Gases
7” (18cm) H x 16.8” (43cm) W x 26.5” (67cm) D Weight 35 lb. (15.9 kg) Power 100 - 120 VAC, 50/60 Hz,; 200 - 240 VAC, 50/60 Hz * 1/4-inch face seal x 1/16-inch adapter fi ttings are available from Ametek User Manual | 17... -
Page 18: Outputs
Field 5 Field 6 Field 7 Field 8 EDL / Single Date & Time Analyzer Run / ta7000 Impurity Concentration Analysis of RUN Serial # Maintenance Error Status Name in ppb x 100 18 | Model ta7000R Gas Purity Monitor... -
Page 19: Com Ports
The following defi nes each fi eld: DDDD-DD-DD TT:TT:TT,#,R,S,A,EEEEEEEE,NNNNN,C, … DDDD-DD-DD = Date (2000-03-23) TT:TT:TT = Time (12:23:44) = Analyzer Serial Number = Run or Maintenance (Calibration) Mode = EDL or Single Analysis Mode = N/A EEEEEEEE = Eight digits of error status (0 = Not Error, 1 = Er- ror) General Alarm (MSD) Spare... - Page 20 The printer port follows standard parallel printer protocols. The analyz- ers are compatable with Hewlett Packard printers model numbers HP-6xx, HP-7xx, and HP-8xx. Trace Analytical recommends using one of these suggested models. Parallel Printer Port LPT1 20 | Model ta7000R Gas Purity Monitor...
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Page 21: Analyzer Description
ANALYZER DESCRIPTION Front Panel and User Interface The front panel is where the user interface is found. The user interface is a combinationof the display screen and menu keys. The display screen shows information andoptions for running the analyzer. The Menu Keys correlate to menu labels on thedisplay screen and are used for all input to the operating system. -
Page 22: Display Screen
This could be information about the last analysis run,calibration, or options for future runs. The bottom area is the Menu Bar. The menu bar is where menu labels are displayedfor user input. 22 | Model ta7000R Gas Purity Monitor... - Page 23 Display screen User Manual | 23...
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Page 24: Installation
In- stall the instrument in an area where there are no vibrations to affect the electronics and detectors. There should not be any draft directly on the 24 | Model ta7000R Gas Purity Monitor... -
Page 25: Electrical Preparations And Connections
instrument from air conditioners or extreme temperature fluctuations in the room. Support gases for the instrument should be located near the ana- lyzer. A uniform temperature environment for cylinders and regulators is essential in order to keep constant pressure and flow rate. Always keep gas containers inside the building where temperature fluctuations are at a minimum. -
Page 26: Regulators And Plumbing
Since the ta7000R needs less than 5A of current, the UPS battery pack can be relatively small. Support Gas Utilities Preparations The ta7000R needs a separate actuator gas in order to run properly. Please refer to this section in the Specifications pages for detailed gas specifica- tion. -
Page 27: Damage Prevention
4 each, required for use with VICI-VCR adapters at regulators. Nut and ferrule, 1/8-inch VICI 1 each required for use in connecting the Actuator gas. Gasket, 1/4-inch VCR, Nickel 8 each, required for use with VICI-VCR adapters and purifier connections. Tubing, 1/16-inch OD x 0.03-inch ID, Stainless Steel 4 each approximately 72”... -
Page 28: Installation Instructions
Making Gas Connections Prepare for Gas Connections Remove the red plastic shipping cap from the Hg vapor trap (scrubber). Remove any 1/16” or 1/8” VICI plugs and 1/4” VCR cap from the rear panel. 28 | Model ta7000R Gas Purity Monitor... -
Page 29: View Of Gas And Power Connections
Remove all other shipping caps immediately prior to connection of gas supplies. Connect Sample / Carrier Gas The analyzer uses purified sample gas as a chromatographic carrier and actuator gas. Matching the carrier gas to the sample will prevent upsets caused by the elution of the extraneous balance peak. -
Page 30: Connect Ac Power And Communication Cables
Confirm the instrument power switch is OFF (“O” is Depressed) Connect DIN power cord to instrument Connect DIN power cord to AC voltage source CONNECT COMMUNICATIONS CABLES (if applicable) COM1, COM2, COM3 port, PARALLEL PRINTER port 30 | Model ta7000R Gas Purity Monitor... -
Page 31: Start Up And Operation
START-UP AND OPERATION Power Up NOTE: Do not continue with this section until all prodedures in the previous section have been completed. Adjust incoming gas supply pressures as specified in the Specifications pages 15-21 of this manual. Turn the instrument on by depressing the power DIN switch (1 is de- pressed) on the back panel of the analyzer. -
Page 32: Using The Menu Keys
LCD display. The text labels describe what the keys do. The six keys are called menu keys; the text labels are called menu labels. All operator input to the analyzer occurs through the 6 menu keys. Menu Labels 32 | Model ta7000R Gas Purity Monitor... -
Page 33: Operator State Diagram
Menus Operator State Diagram Power-up Warmup Warmup Edit Edit System Temperatures Page Warm-up Page Page and Status Settings Cool Page Return to Source Calibration Idle Settings Page Edit Blank Calib State Diagram screenm. This chart illustrates how the menus are arranged. Each large circle rep- resents a screen that is displayed on the instrument. - Page 34 Pressing the Run key will take the user to the main screen where the Main menu will be available. Idle Mode 12:34:25 WARM-UP Module Electronics: Pass Detector System: Pass Detector Temperatures: Pass Carrier Pressure: Pass ***** Successful Warm-up ***** Page Cool Warmup Pass Screen 34 | Model ta7000R Gas Purity Monitor...
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Page 35: Main Menu Screens
Main Menu After warm-up has completed successfully the main menu will be dis- played. The main menu is a set of primary choices leading to other menu options. The following table shows the choices available from the main menu. 12:34:25 Idle Mode CO = Cool... -
Page 36: Page Screens
An Edit menu label appears if there are fields that allow the user to enter information Screen What Information is available Page 1 System Settings. Page 2 Temperatures and Page 3 Status Page Screens 36 | Model ta7000R Gas Purity Monitor... -
Page 37: Setting The Clock
System Settings Page The first Page Screen is for general configuration settings. The following list shows the function of each option for this screen Idle Mode 12:34:25 System Settings Ver. 2.70 Clock: 10-Jan-03 12:34:25 Print Chromatograms: EDL mode: -------------------- System Errors -------------------- Edit Print Page... -
Page 38: Temperatures
RGD Window = 79 # RGD Lamp = On RGD Vout = 36187 RGD Vsig = 1978.4 ------------------------- Pressure -------------------------- Carrier = 60.3 Calib. = 75.2 Page Image of Temperatures and Status Screen 38 | Model ta7000R Gas Purity Monitor... -
Page 39: Calibration
Calibration Page Pressing the Page key three times will display the calibration informa- tion page. The calibration screen shows information about the most recent calibra- tion run. Name. is the gas species to be measured. Conc is the cylinder concentration (or blend) of the calibration gas connected to the instrument. -
Page 40: Manual Calibration
Changes into non-volatile Ram section of this manual. Manual Calibration From the main menu, pressing the Calib key will begin a manual calibra- tion run of the ta7000R. The analyzer does not need zero calibration. An 40 | Model ta7000R Gas Purity Monitor... - Page 41 In calibration mode the instrument first checks for calibration gas pres- sure. Next the instrument purges the calibration gas line for a user-preset amount of time. Finally the ta7000R performs three calibration runs. The first of these three calibrations is discarded. The second and third runs are used to generate the calibration response factor.
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Page 42: Non Volatile Ram
To continue running the instrument after the Idle key has been pressed, simply press the Idle key again and the Pound will disappear and the instrument will continue to automatically run samples. 42 | Model ta7000R Gas Purity Monitor... -
Page 43: Blank
# indicates cycle run will end Run Mode# 235 12:55:30 Cycle Run = 16.1 CO = 12.7 Idle Page Run Mode Screens Blank Pressing the “Blank Key” will begin a “blank” run. This is a system diagnostic run which tests the internal gas inside the instrument. No ex- ternal sample will be introduced into the systems during this run. -
Page 44: Shut Down
From the main menu press the Idle key to stop analysis. Press the Cool key and allow the analyzer to cool down for two to three hours. Switch the analyzer and all other components off. Shut off the carrier/sample gas. 44 | Model ta7000R Gas Purity Monitor... -
Page 45: Description Of Internal Components
DESCRIPTION OF INTERNAL COMPONENTS Main Front Panel Processor Display Module Chassis Lamp Control Module Detector Controller Detector Power Supply Chrom Module Light Power Guide Supply Carrier / Sample Stream Blender Regulator Selector Rear Panel Front and Rear Panels User Manual | 45... -
Page 46: Error Messages
If the RGD lamp is not within operating range this error will be displayed. Carrier Pressure Out of Range External carrier pressure is not within specified limits. Verify external car- rier pressure supply. 46 | Model ta7000R Gas Purity Monitor... - Page 47 Analog Signal Zeroing Error The instrument has failed to zero the detectors analog signal. Vsig Minimum Voltage Limit This fault will occur if the RGD detector does not have the minimum Vsig (1000mv) for proper analysis. Typical Values are 1750-2250. Vsig cannot be above 2500.
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Page 48: Dimensional Drawings
Dimensional Drawings ta7oooR 3-D View 48 | Model ta7000R Gas Purity Monitor... - Page 49 ta7oooR Side View User Manual | 49...
- Page 50 Top View 50 | Model ta7000R Gas Purity Monitor...