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Vion IMS QTof
Waters Vion IMS QTof Manuals
Manuals and User Guides for Waters Vion IMS QTof. We have
2
Waters Vion IMS QTof manuals available for free PDF download: Overview And Maintenance Manual, Quick Start Manual
Waters Vion IMS QTof Overview And Maintenance Manual (200 pages)
Brand:
Waters
| Category:
Laboratory Equipment
| Size: 7.89 MB
Table of Contents
General Information
2
Trademarks
2
Customer Comments
3
Contacting Waters
3
Safety Considerations
4
Considerations Specific to the Device
4
Electrical Power Safety Notice
7
Safety Hazard Symbol Notice
7
Equipment Misuse Notice
7
Safety Advisories
8
Operating the Device
8
Applicable Symbols
8
Intended Use of the Vion IMS Qtof
9
Calibrating
9
Quality Control
10
EMC Considerations
10
FCC Radiation Emissions Notice
10
Canada Spectrum Management Emissions Notice
10
ISM Classification: ISM Group 1 Class a
10
Table of Contents
11
Waters Vion IMS Qtof Overview
17
Waters Vion IMS Qtof
17
Automated Setup and Calibration Check
17
ACQUITY Vion IMS Qtof UPLC/MS Systems
18
Software and Data System
19
Lockspray Source and Ionization Modes
20
Electrospray Ionization (ESI)
21
Atmospheric Pressure Chemical Ionization (APCI)
21
Nanolockspray Source and Ionization Modes
22
Apgc
23
Fluidics System
23
Physical Layout of the Fluidics System
24
System Operation
25
Ion Optics
25
Leak Sensors
27
Vacuum System
27
Preparing the Mass Spectrometer for Operation
29
Starting the Mass Spectrometer
29
Verifying the Instrument's State of Readiness
30
Automated Setup
31
Flow Rates for the Vion IMS Qtof System
31
Preparing the Fluidics System
31
Installing the Reservoir Bottles
32
Installing the Low-Volume Vials
33
Purging the Fluidics
33
Rebooting the Mass Spectrometer
33
Leaving the Mass Spectrometer in Standby Mode
34
Emergency Shutdown
35
Configuring the Lockspray Source
36
Configuring for ESI Mode
36
Installing the ESI Probe
36
Removing the ESI Probe
40
Configuring for APCI Mode
40
Installing the Ionsabre II Probe
41
Removing the Ionsabre II Probe
43
Configuring the Nanolockspray Source
44
Overview of the Nanolockspray Source
44
Sample Sprayer
46
Lockspray Sprayer
46
Nanoflow Gas Supply
46
Purge Gas
46
Sprayer Platform Adjuster Assembly
46
Selecting and Configuring the Nanolockspray Source
47
Deploying the Sprayer Platform Adjuster Assembly
47
Moving the Sprayer Platform out of the Source
47
Moving the Sprayer Platform into the Source
48
Setting up the Camera
48
Adjusting the Sprayer Tip Position
49
Optional Glass Capillary Sprayer
50
Maintenance Procedures
51
Maintenance Schedule
51
Spare Parts
52
Safety and Handling
52
Preparing the Instrument for Working on the Source
53
Using UNIFI Software to Prepare the Instrument for Working on the Source
54
Removing and Refitting the Source Enclosure
54
Removing the Source Enclosure from the Instrument
54
Fitting the Source Enclosure to the Instrument
56
Installing and Removing the Corona Pin
57
Installing the Corona Pin in the Source
57
Removing the Corona Pin from the Source
59
Operating the Source Isolation Valve
60
Closing the Source Isolation Valve
61
Opening the Source Isolation Valve
62
Removing O-Rings and Seals
62
O-Ring Removal Kit
62
Cleaning the Instrument Case
63
Emptying the Nitrogen Exhaust Trap Bottle
63
Maintaining the Roughing Pump
65
Cleaning the Source Components
65
Cleaning the Sampling Cone Assembly
66
Removing the Sampling Cone Assembly from the Source
66
Disassembling the Sampling Cone Assembly
67
Cleaning the Sample Cone and Cone Gas Nozzle
69
Assembling the Sampling Cone Assembly
71
Fitting the Sampling Cone Assembly to the Source
72
Cleaning the Ion Block Assembly
73
Removing the Ion Block Assembly from the Source Assembly
73
Disassembling the Source Ion Block Assembly
74
Cleaning the Ion Block Components
79
Assembling the Source Ion Block Assembly
80
Fitting the Ion Block Assembly to the Source Assembly
81
Cleaning the Stepwave Ion Guide Assembly
82
Handling the Stepwave Ion Guide Assembly
82
Removing the Ion Block Support from the Source Assembly
82
Removing the Stepwave Assembly from the Source Assembly
83
Cleaning the Stepwave Ion Guide Assembly
85
Fitting the Stepwave Assembly to the Source Assembly
87
Fitting the Ion Block Support to the Source
89
Maintaining the ESI Probe
90
Replacing the ESI Probe Tip and Gasket
90
Replacing the ESI Probe Capillary
93
Maintaining the Ionsabre II Probe
111
Cleaning the Ionsabre II Probe Tip
111
Replacing the Ionsabre II Probe Sample Capillary
111
Cleaning or Replacing the Corona Pin
117
Replacing the Lockspray Reference Probe Capillary
118
Removing the Existing Capillary
118
Installing the New Capillary
120
Replacing the Lockspray II Reference Probe
123
Removing the Existing One-Piece Reference Probe
125
Installing the New Reference Probe
129
Replacing the Nanolockspray Reference Probe Tapertip Emitter or Capillary
133
Removing the Nanolockspray Reference Probe
133
Installing the New Tapertip Emitter and Capillary
135
Replacing the Ionsabre II Probe Heater
137
Removing the Ionsabre II Probe Heater
137
Fitting the New Ionsabre II Probe Heater
139
Replacing the Ion Block Source Heater
140
Replacing the Lockspray Source's Assembly Seals
143
Removing the Probe Adjuster Assembly Probe and Source Enclosure Seals
144
Fitting the New Source Enclosure and Probe Adjuster Assembly Probe Seals
145
Replacing the Fluidics Tubing
147
Replacing Fluidics Tubing (Standard Configuration)
147
Removing the Fluidics Tubing
148
Plumbing the Fluidics Lockspray System
149
Plumbing the Fluidics Sample Delivery System
155
Plumbing the Fluidics Sample Delivery System for Nanolockspray Operation
161
Replacing the Instrument's Fuses
167
A Safety Advisories
169
Warning Symbols
169
Notices
170
Bottles Prohibited Symbol
170
Required Protection
171
Warnings that Apply to All Waters Instruments and Devices
171
Warnings that Address the Replacement of Fuses
175
Electrical Symbols
176
Handling Symbols
177
B External Connections
179
Mass Spectrometer: External Wiring and Vacuum Connections
179
Connecting the Ebara Oil-Free Roughing Pump
181
Connecting to the Nitrogen Gas Supply
185
Connecting to the Collision Cell Gas Supply
186
Connecting the Nitrogen Exhaust Line
186
Connecting Liquid Waste Lines
188
Connecting the Workstation (Systems with no ACQUITY LC)
190
Connecting to the Workstation
190
Connecting the Workstation to the Power Source
191
Connecting Ethernet Cables (Systems with ACQUITY LC)
191
Input/Output Signal Connectors
192
Signal Connections
194
Connecting the Contact-Closure Cable to an ACQUITY LC
196
Connecting to the Electricity Source
198
C Materials of Construction and Compatible Solvents
199
Preventing Contamination
199
Items Exposed to Solvent
199
Solvents Used to Prepare Mobile Phases
200
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Waters Vion IMS QTof Quick Start Manual (2 pages)
No flow from fluidics
Brand:
Waters
| Category:
Laboratory Equipment
| Size: 0.04 MB
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