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Translation of the original operating manual
sb
11/2017
Rev. 1.7.1 of 08/12/2022
Sigma 4-5KRL;Refrigerated Centrifuge for Robot Use;Sigma 4-5KRL IVD; ;
Refrigerated Centrifuge for Robot Use
Sigma 4-5KRL
Sigma 4-5KRL IVD
Refrigerated Centrifuge
for Robot Use
Operating Manual
from serial no. 165039
part no. 0703302

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Summary of Contents for Sigma 4-5KRL

  • Page 1 Translation of the original operating manual 11/2017 Rev. 1.7.1 of 08/12/2022 Sigma 4-5KRL;Refrigerated Centrifuge for Robot Use;Sigma 4-5KRL IVD; ; Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Sigma 4-5KRL IVD from serial no. 165039 Refrigerated Centrifuge for Robot Use Operating Manual...
  • Page 2 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 2 / 113 Translation of the original operating manual,...
  • Page 3 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD © Copyright by Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode am Harz Germany Tel.: +49 (0) 5522 / 5007-0 Fax: +49 (0) 5522 / 5007-12 Web: www.sigma-zentrifugen.de...
  • Page 4 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 4 / 113 Translation of the original operating manual,...
  • Page 5: Table Of Contents

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Table of contents General information ......................9 Importance of the operating manual .................. 9 Intended use ........................9 Warranty and liability......................9 Copyright ........................10 Standards and regulations ....................
  • Page 6 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Table of contents Storage and transport ....................... 29 Dimensions and weight ....................29 Storage conditions ......................29 Notes on transport ......................29 Packaging ........................30 Transport safety device ....................
  • Page 7 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Table of contents Malfunctions and error correction ..................51 General malfunctions ...................... 51 7.1.1 Emergency lid release ....................52 Table of error codes ......................53 Service contact .......................
  • Page 8 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Table of contents Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 8 / 113 Translation of the original operating manual,...
  • Page 9: General Information

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 1 General information General information Importance of the operating manual A fundamental requirement for the safe and trouble-free operation of the centrifuge is to be familiar with the fundamental safety instructions and all possible hazards.
  • Page 10: Copyright

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 1 General information → Copyright The copyright concerning the operating manual remains with Sigma Laborzentrifugen GmbH. The operating manual is solely intended for the operator and their personnel.
  • Page 11: Layout And Mode Of Operation

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation → Layout and mode of operation → Layout of the centrifuge 2.1.1 Functional and operating elements Centrifuge lid User interface (see chapter 6.3.1 -...
  • Page 12 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation Serial interface (see chapter 2.1.3 - "Serial interface (pin assignment)") Equipotential bonding screw Fuse Mains power input Fig. 3: Detailed view A - connections Version 11/2017, Rev.
  • Page 13: Name Plate

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation 2.1.2 Name plate Manufacturer Power consumption Max. speed Max. kinetic energy Serial number Part number Nominal voltage Type Consult operating...
  • Page 14: Serial Interface (Pin Assignment)

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation 2.1.3 Serial interface (pin assignment) There is a floating, normally closed contact between pin 1 and pin 4. When the centrifuge is started, the contact opens, thereby signalling that the centrifuge is ready for operation.
  • Page 15: Mode Of Operation

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation → Mode of operation → 2.2.1 Centrifugation principle Centrifugation is a process for the separation of heterogeneous mixtures of substances (suspensions, emulsions, or gas mixtures) into their components.
  • Page 16: Speed, Radius, And Relative Centrifugal Force

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 2 Layout and mode of operation → 2.2.2.1 Speed, radius, and relative centrifugal force The acceleration g, which the samples are subject to, can be increased by increasing the radius in the rotor chamber and by increasing the speed.
  • Page 17: Safety

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Safety → Marking of the unit The following symbols are used on this centrifuge: Arrow indicating the direction On (Power) of rotation...
  • Page 18: Explanation Of The Symbols And Notes

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Explanation of the symbols and notes In this operating manual, the following names and symbols to indicate hazards are used: This symbol stands for a direct hazard to the life and health of persons.
  • Page 19: Responsibility Of The Operator

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Responsibility of the operator The operator undertakes to authorise only trained, specialised personnel to work on the centrifuge (see chapter 3.4 - "Requirements concerning the personnel").
  • Page 20: Requirements Concerning The Personnel

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Requirements concerning the personnel Risk of injury if the personnel are not sufficiently qualified If unqualified personnel perform work on the centrifuge or are present in the danger zone of the centrifuge, hazards result that can cause serious injuries and considerable damage to property.
  • Page 21: Informal Safety Instructions

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety The operating personnel must ensure that any serious event which either directly or indirectly had, could have had or could have one of the following...
  • Page 22: Safety Instructions

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Safety instructions 3.6.1 Electrical safety As protection against electric shock, the centrifuge is equipped with an earthed mains power cable and connector. To ensure the effectiveness of this safety feature, the following must be ensured: •...
  • Page 23: Safety Instructions For Robot-Controlled Centrifuges

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety • Do not spin any substances that could damage the material of the rotors and buckets of the centrifuge in any way. Highly corrosive substances, for example, damage the material and affect the mechanical strength of the rotors and buckets.
  • Page 24: Chemical And Biological Safety

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → 3.6.5 Chemical and biological safety If pathogenic, toxic, or radioactive samples are intended to be used in the centrifuge, it is in the responsibility of the user to ensure that all necessary safety regulations, guidelines, precautions, and practices are adhered to accordingly.
  • Page 25: Resistance Of Plastics

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety 3.6.7 Resistance of plastics Chemical influences have a strong effect on the polymeric chains of plastics, and, therefore, on their physical properties. Plastic parts can be damaged if solvents, acids, or alkaline solutions are used.
  • Page 26: Service Life (For Centrifuges According To The Ivd Regulation)

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety 3.6.9 Service life (for centrifuges according to the IVD regulation) Centrifuge The service life of the centrifuge depends on several factors, e.g. the type and frequency of use, the area of application and the performance of service and maintenance tasks.
  • Page 27: Safety Devices

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Safety devices → 3.7.1 Lid lock device The centrifuge can only be started when the lid is properly closed. The electrical lock must be locked. The lid can only be opened when the rotor has stopped.
  • Page 28: Measures In The Event Of Hazards And Accidents

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 3 Safety → Measures in the event of hazards and accidents • If an emergency arises, switch off the centrifuge immediately! • If in doubt, call the emergency doctor! DANGER →...
  • Page 29: Storage And Transport

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 4 Storage and transport → Storage and transport → Dimensions and weight Sigma 4-5KRL, Sigma 4-5KRL IVD Height: 406 mm Height with open lid: 890 mm...
  • Page 30: Packaging

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 4 Storage and transport Packaging The centrifuge is packaged in a wooden crate. • After taking off the lid, remove the side panels. • Remove the packaging material.
  • Page 31: Set-Up And Connection

    CAUTION Sigma centrifuges are units of protection class I. The centrifuges of this model series have a three-wire power cord with an IEC C13 connector. The removable power cord must not be longer than 3 m!
  • Page 32: Customer-Provided Fuses

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 5 Set-up and connection The centrifuges are equipped with a mains power switch with an integrated thermal circuit breaker. • Switch the unit off by actuating the mains power switch.
  • Page 33: Using The Centrifuge

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → Using the centrifuge → Initial start-up • Before the initial start-up, please ensure that your centrifuge is properly set up and installed (see chapter 5 - "Set-up and connection").
  • Page 34: Installation Of Rotors And Accessories

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → 6.2.2 Installation of rotors and accessories → 6.2.2.1 Installation of the rotor • Open the centrifuge lid by pressing the lid key.
  • Page 35 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge Centrifugation with vessels of various sizes Working with vessel of various sizes is possible. In this case, however, it is very important that the rotationally symmetrical inserts are identical (see figure).
  • Page 36: Adapters

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge 6.2.2.3 Adapters In order to ensure easy handling, even if vessels of various sizes are used, carrier systems were developed. •...
  • Page 37: Control System "Spincontrol L

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → Control system "Spincontrol L" → 6.3.1 User interface The centrifuge is operated via three buttons with integrated light-emitting diodes and one function knob. The display is divided into several different fields.
  • Page 38: Manual Mode

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → 6.3.2 Manual mode → 6.3.2.1 Starting a centrifugation run The centrifuge is ready for operation when the start key is illuminated.
  • Page 39: Speed / Relative Centrifugal Force (Rcf)

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → 6.3.2.5 Speed / relative centrifugal force (RCF) The set speed of the centrifuge is displayed in the upper area of the Speed/RCF field.
  • Page 40 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge Runtime as of the set speed If the runtime is to be counted as of the moment when the set speed is...
  • Page 41: Temperature

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge Short run A short run can be started if no run is active. • Keep the start key pressed during the short run.
  • Page 42 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge Program "Rapid Temp" The centrifuge has a special "Rapid Temp" program that precools the centrifuge rapidly under defined conditions. • Select the program with the aid of the menu item "run Prog" (see chapter 6.3.3.2 - "Loading a program").
  • Page 43: Rotor Selection

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → → 6.3.2.8 Rotor selection This field shows the rotor that is currently being used. The rotor selection can only be changed when the centrifuge is at a standstill.
  • Page 44: Acceleration And Deceleration Curves

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → 6.3.2.9 Acceleration and deceleration curves Acceleration This function is used to select an acceleration curve. The system offers 10 fixed, programmed acceleration curves (curves 0-9).
  • Page 45: Cycle Display ("Cycles")

    WARNING The cycle display will be reset after the rotor and buckets have been replaced by the service department of Sigma Laborzentrifugen GmbH (see chapter 7.3 - "Service contact"). Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb...
  • Page 46: 6.3.2.12 Input Lock

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge 6.3.2.12 Input lock In order to prevent the centrifuge from being manipulated by unauthorised persons, inputs can be disabled via the menu. Inputs via the keypad, i.e. for starting or stopping a centrifugation run or for opening the lid, are enabled.
  • Page 47: Saving A Program

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → → 6.3.3.1 Saving a program This function is only available if the centrifuge is at a standstill. NOTE • Enter the parameters that are to be included in the program.
  • Page 48: Use As A Robot-Controlled Centrifuge

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge Use as a robot-controlled centrifuge In addition to manual operation, the centrifuge is also suitable for being loaded by a robot. A separate computer is used for the control.
  • Page 49: Input

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge 6.4.3 Input The centrifuge can be controlled with several input commands. The input commands are divided into several categories: • Check commands, these commands trigger an immediate action •...
  • Page 50: Switching The Centrifuge Off

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 6 Using the centrifuge → Switching the centrifuge off • Open the centrifuge when it is not in use so moisture can evaporate. • Switch the centrifuge off by pressing the mains power switch.
  • Page 51: Malfunctions And Error Correction

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 7 Malfunctions and error correction → Malfunctions and error correction → General malfunctions Error messages are displayed as "Error" followed by a code number. If the acoustic signal is activated, it sounds when the error message is displayed.
  • Page 52: Emergency Lid Release

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 7 Malfunctions and error correction 7.1.1 Emergency lid release In the event of a power failure, it is possible to manually open the centrifuge lid.
  • Page 53: Table Of Error Codes

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 7 Malfunctions and error correction → Table of error codes Error no. Kind of error Measures Note • System error Allow to slow down All these errors stop the centrifuge or cause it to •...
  • Page 54: Service Contact

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 7 Malfunctions and error correction → Service contact In the event of queries, malfunctions, or spare part enquiries: From Germany: Contact Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode (Germany) Tel.
  • Page 55: Maintenance And Service

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → Maintenance and service The centrifuge, rotor, and accessories are subject to high mechanical stress. Thorough maintenance performed by the user extends the service life and prevents premature failure.
  • Page 56: Condenser (Only Refrigerated Centrifuges With An Air-Cooled Refrigeration System)

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → 8.1.1.1 Condenser (only refrigerated centrifuges with an air-cooled refrigeration system) In order to cool the refrigerant that is compressed by the refrigeration unit, centrifuges with an air-cooled refrigeration system use a lamellar condenser.
  • Page 57: Plastic Accessories

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service 8.1.2.1 Plastic accessories The chemical resistance of plastic decreases with rising temperatures (see chapter 11.5 - "Resistance data"). • If solvents, acids, or alkaline solutions have been used, clean the plastic accessories thoroughly.
  • Page 58: Load Bearing Bolts

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → 8.1.4 Load bearing bolts Only greased load-bearing bolts ensure a uniform swing-out of the buckets and, therefore, the smooth operation of the centrifuge. Load-bearing bolts that are insufficiently greased may cause the centrifuge to stop due to an imbalance.
  • Page 59: Glass Breakage

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → 8.1.5 Glass breakage In the case of glass breakage, immediately remove all glass particles (e.g. with a vacuum cleaner). Replace the rubber cushions since even thorough cleaning will not remove all glass particles.
  • Page 60: 8.2.1 Autoclaving

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → 8.2.1 Autoclaving The service life of the accessories essentially depends on the frequency of autoclaving and use. • Replace the accessories immediately when the parts show changes in colour or structure or in the occurrence of leaks etc.
  • Page 61: Service

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → Service In the event of service work that requires the removal of the panels, there is a risk of electric shock or mechanical injury.
  • Page 62: Return Of Defective Centrifuges Or Parts

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service → Return of defective centrifuges or parts Although we exercise great care during the production of our products, it may be necessary to return a unit or accessory to the manufacturer.
  • Page 63 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 8 Maintenance and service The defective part/unit must be packaged in a transport-safe manner. Please use the original packaging for the unit, if at all possible.
  • Page 64: Disposal

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 9 Disposal → Disposal → Disposal of the centrifuge In accordance with the directive 2012/19/EU, SIGMA centrifuges are marked with the symbol shown to the left. This symbol means that it is not permissible to dispose of the unit among household waste.
  • Page 65: 10 Technical Data

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 10 Technical data → 10 Technical data Manufacturer Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode (Germany) Type: 4-5KRL 4-5KRL IVD Part no.:...
  • Page 66: Ambient Conditions

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 10 Technical data → 10.1 Ambient conditions • The figures are valid for an ambient temperature of +23°C and a nominal voltage  10 %. The minimum temperature is ≤ +4°C and depends on the rotor type, speed, and ambient temperature.
  • Page 67: 11 Appendix

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix → 11 Appendix 11.1 Suitable accessories For use in a robot-controlled centrifuge, special equipment is required. Please contact our sales department: SIGMA Laborzentrifugen GmbH An der Unteren Söse 50...
  • Page 68: Speed-Gravitational-Field-Diagram

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix → 11.2 Speed-gravitational-field-diagram Fig. 34: Speed-gravitational-field-diagram Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 68 / 113 Translation of the original operating manual,...
  • Page 69: Acceleration And Deceleration Curves

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix → 11.3 Acceleration and deceleration curves Linear curves are numbered in the direction of increasing acceleration (from right to left). The deceleration curves are inverted images of the acceleration curves and are assigned the same numbers.
  • Page 70: Table Of The Service Life Of Rotors And Accessories

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix → 11.4 Table of the service life of rotors and accessories • The rotors and accessories must be put out of service after 10 years. Any use after this period may be permissible in individual cases after an inspection performed by the manufacturer.
  • Page 71: Resistance Data

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix → 11.5 Resistance data The data refer to resistance at 20°C. NOTE - no data 1 resistant 2 practically resistant 3 partially resistant...
  • Page 72 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Chromic acid Chromic potassium KCr(SO saturated sulphate...
  • Page 73 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Isopropyl alcohol Lactic acid Magnesium chloride MgCl...
  • Page 74 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Sodium bisulphite NaHSO Sodium carbonate Sodium chloride...
  • Page 75: Serial Control Interface Specification

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix 11.6 Serial Control Interface Specification Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 75 / 113 Translation of the original operating manual,...
  • Page 76 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 76 / 113 Translation of the original operating manual,...
  • Page 77 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 77 / 113 Translation of the original operating manual,...
  • Page 78 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 78 / 113 Translation of the original operating manual,...
  • Page 79 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 79 / 113 Translation of the original operating manual,...
  • Page 80 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 80 / 113 Translation of the original operating manual,...
  • Page 81 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 81 / 113 Translation of the original operating manual,...
  • Page 82 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 82 / 113 Translation of the original operating manual,...
  • Page 83 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 83 / 113 Translation of the original operating manual,...
  • Page 84 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 84 / 113 Translation of the original operating manual,...
  • Page 85 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 85 / 113 Translation of the original operating manual,...
  • Page 86 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 86 / 113 Translation of the original operating manual,...
  • Page 87 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 87 / 113 Translation of the original operating manual,...
  • Page 88 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 88 / 113 Translation of the original operating manual,...
  • Page 89 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 89 / 113 Translation of the original operating manual,...
  • Page 90 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 90 / 113 Translation of the original operating manual,...
  • Page 91 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 91 / 113 Translation of the original operating manual,...
  • Page 92 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 92 / 113 Translation of the original operating manual,...
  • Page 93 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 93 / 113 Translation of the original operating manual,...
  • Page 94 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 94 / 113 Translation of the original operating manual,...
  • Page 95 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 95 / 113 Translation of the original operating manual,...
  • Page 96 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 96 / 113 Translation of the original operating manual,...
  • Page 97 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 97 / 113 Translation of the original operating manual,...
  • Page 98 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 98 / 113 Translation of the original operating manual,...
  • Page 99 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 99 / 113 Translation of the original operating manual,...
  • Page 100 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 100 / 113 Translation of the original operating manual,...
  • Page 101: Ec Declaration Of Conformity

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Lars 11.7 EC declaration of conformity Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 101 / 113 Translation of the original operating manual,...
  • Page 102 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 102 / 113 Translation of the original operating manual,...
  • Page 103 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 103 / 113 Translation of the original operating manual,...
  • Page 104 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 104 / 113 Translation of the original operating manual,...
  • Page 105: Declaration Of Conformity - China Rohs 2

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Declaration of conformity – China RoHS 2 11.8 Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 105 / 113 Translation of the original operating manual,...
  • Page 106 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 106 / 113 Translation of the original operating manual,...
  • Page 107: Ukca Declaration Of Conformity

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix 11.9 UKCA declaration of conformity Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 107 / 113 Translation of the original operating manual,...
  • Page 108 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD 11 Appendix Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 108 / 113 Translation of the original operating manual,...
  • Page 109: 12 Index

    Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Index 12 Index Changes in structure ........60 Check commands ........49 Acceleration ..........44 Chemical and biological safety ....24 Acceleration curves ......44, 69 Chemical resistance of plastic ....
  • Page 110 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Index Dimensions ..........29 Highly corrosive substances ...... 23 Direct hazard to the life and health ..... 18 Directive 2002/96/EC ......... 64 Imbalance ..........34, 36 Disinfectants ..........
  • Page 111 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Index Mains switch ..........11 Power supply ..........31 Mains voltage ..........22 Preselection of a curve....... 44 Maintenance ..........55 Pressure (refrigerant) ......... 65 Malfunctions and error correction ....
  • Page 112 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Index Rotors, cleaning and care ......57 Stopping of the centrifuge due to an imbalance ..........58 RS232 cable ..........10 Storage and transport ........ 29 Runtime .............
  • Page 113 Refrigerated Centrifuge for Robot Use Sigma 4-5KRL Refrigerated Centrifuge for Robot Use Sigma 4-5KRL IVD Index Wear ............61 Weight ............29 Warranty and liability ........9 Version 11/2017, Rev. 1.7.1 of 08/12/2022 • sb 113 / 113 Translation of the original operating manual,...

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