Sigma 4-16KHS Operating Manual
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Sigma 4-16KHS Operating Manual

Refrigerated centrifuge with heating system
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Translation of the original operating manual
sb
10/2012
Rev. 1.22 of 08/05/2020
Sigma 4-16KHS; ;
part no. 0701802
Sigma 4-16KHS
Refrigerated Centrifuge
with Heating System
Operating Manual
Please retain for later use!
from serial no. 147161

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  • Page 1 Translation of the original operating manual 10/2012 Rev. 1.22 of 08/05/2020 Sigma 4-16KHS; ; part no. 0701802 Sigma 4-16KHS from serial no. 147161 Refrigerated Centrifuge with Heating System Operating Manual Please retain for later use!
  • Page 2 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 2 / 91 Translation of the original operating manual, part no. 0701802...
  • Page 3 Refrigerated Centrifuge with Heating System Sigma 4-16KHS © Copyright by Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode am Harz Germany Tel.: +49 (0) 5522 / 5007-0 Fax: +49 (0) 5522 / 5007-12 Web: www.sigma-zentrifugen.de E-mail: info@sigma-zentrifugen.de Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 3 / 91 Translation of the original operating manual, part no.
  • Page 4 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 4 / 91 Translation of the original operating manual, part no. 0701802...

  • Page 5: Table Of Contents

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS Table of contents General information ......................9 Importance of the operating manual .................. 9 Intended use ........................9 Warranty and liability......................9 Copyright ........................10 Standards and regulations ....................10 Scope of supply ......................10 Layout and mode of operation ..................
  • Page 6 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Table of contents Storage and transport ....................... 25 Dimensions and weight ....................25 Storage conditions ......................25 Notes on transport ......................25 Packaging ........................26 Transport safety device ....................26 Set-up and connection ...................... 27 Installation site ........................
  • Page 7 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Table of contents Malfunctions and error correction ..................58 General malfunctions ...................... 58 7.1.1 Emergency lid release ....................59 Table of error codes ......................60 Service contact ....................... 61 Maintenance and service ....................62 Maintenance ........................
  • Page 8 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Table of contents Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 8 / 91 Translation of the original operating manual, part no. 0701802...

  • Page 9: General Information

    Leerzeil e @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 4 /100 Sigma/100 BA Z entrifug en Sigma ( Standardm odule) /010 Allgem eine Inform ationen/010- 0020 Bestimm ungsgem äß e Verw endung Sigma ------------------------------------------- @ 26\m od_1405318951312_68.docx @ 191709 @ 2 @ 1 →...

  • Page 10: Copyright

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 1 General information Pos : 8 /100 Sigma/100 BA Z entrifug en Sigma ( Standardm odule) /010 Allgem eine In form ationen/010- 0040 Urheberrec ht Sigma ----------------------------------------------------------------- @ 26\mod_1405318956858_68.doc x @ 191751 @ 2 @ 1 →...

  • Page 11: Layout And Mode Of Operation

    → Layout of the centrifuge Pos : 17 /100 Sigma/110 BA Zentrifugen Sigma (Pr ojekte) /4- 16KS_4-16KH S/020 Aufbau und Wirk ungsw eise/020-0010-0011 Funkti ons- und Bedienelem ente 4- 16KHS @ 29\m od_1405326891359_68.docx @ 198611 @ 3 @ 1 2.1.1...

  • Page 12: Name Plate

    Pos : 18 /010 U nivers almodule/Seitenw ec hsel @ 0\m od_1202116244312_0.doc x @ 105 @ @ 1 Pos : 19 /100 Sigma/110 BA Zentrifugen Sigma (Pr ojekte) /4- 16KS_4-16KH S/020 Aufbau und Wirk ungsw eise/020-0010-0020 Typensc hild 4-16KHS @ 29\mod_1405326892357_68.docx @ 198625 @ 3 @ 1 2.1.2...

  • Page 13: Mode Of Operation

    Pos : 21 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/020 Aufbau und Wirk ungsw eise/020-0020 Wirkungsweis e---------------------------------------------------------- @ 26\mod_1405318984194_68.docx @ 191807 @ 2 @ 1 → Mode of operation Pos : 22 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/020 Aufbau und Wirk ungsw eise/020-0020-0010 Prinzi p der Z entrifugati on @ 26\m od_1405318985448_68.docx @ 191821 @ 3 @ 1 → 2.2.1...

  • Page 14: Speed, Radius, And Relative Centrifugal Force

    2 Layout and mode of operation Pos : 26 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/020 Aufbau und Wirk ungsw eise/020-0020-0020- 0010 Dr ehzahl, R adius , R elativ e Zentrifugalbesc hl eunigung @ 26\mod_1405318988082_68.docx @ 191849 @ 4 @ 1 →...

  • Page 15: Safety

    Safety Pos : 32 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0010 Besc hilderung des Geräts neues Ty pens chil d (auß er 2- 16KL, 3-16KL, 3- 30KS, 4-16S) @ 62\mod_1548831855885_68.docx @ 621378 @ 2 @ 1 →...

  • Page 16: Explanation Of The Symbols And Notes

    Leerz eile @ 0\m od_1202116244500_0.doc x @ 114 @ @ 1 Pos : 34 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0020 Symbol- und Hi nweis erklär ung en @ 26\mod_1405319013955_68.docx @ 191947 @ 2 @ 1 →...

  • Page 17: Responsibility Of The Operator

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 3 Safety Pos : 36 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0030 Ver antw ortung des Betrei bers @ 26\mod_1405319015364_68.docx @ 191961 @ 2 @ 1 → Responsibility of the operator The operator is responsible for authorising only qualified personnel to work on the centrifuge (see chapter 3.4 - "Operating personnel").

  • Page 18: Safety Instructions

    Leerz eile @ 0\m od_1202116244500_0.doc x @ 114 @ @ 1 Pos : 45 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0020 M ec hanisc he Sic her heit (auß er 1-16/1-16K/1-7) @ 26\mod_1405319024314_68.docx @ 192059 @ 3 @ 1 →...

  • Page 19: Fire Prevention

    Leerz eile @ 0\m od_1202116244500_0.doc x @ 114 @ @ 1 Pos : 49 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0040 C hemische und bi ologisc he Sic her hei t @ 26\m od_1405319028141_68.docx @ 192101 @ 3 @ 1 →...

  • Page 20: Safety Instructions For Centrifugation

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 3 Safety Pos : 51 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0050 Sicherheits hi nweis e z ur Z entrifug ation @ 26\mod_1405319029632_68.doc x @ 192115 @ 3 @ 1 →...

  • Page 21: Safety Of Rotors And Accessories

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 3 Safety Pos : 55 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0070 Sicherheit von R otoren und Zubehör @ 44\m od_1470119200568_68.docx @ 437008 @ 3 @ 1 3.6.7 Safety of rotors and accessories Pos : 56 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0070- 0010 Lebens dauer (außer 8KBS) @ 26\m od_1405319032612_68.docx @ 192143 @ 3 @ 1...

  • Page 22: Marking

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 3 Safety Pos : 58 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0060-0070- 0020 Kennz eichnung @ 44\mod_1470119283352_68.doc x @ 437025 @ 4 @ 1 3.6.7.2 Marking During production, every rotor and bucket receives a batch number enabling conclusions to be drawn concerning the production process and the subsequent quality inspection.

  • Page 23: Safety Devices

    Leerz eile 8 pt @ 12\mod_1337063062114_0.docx @ 65687 @ @ 1 Pos : 67 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0070-0041 Sc hutzleiterpr üfung ohne Potenti alausgleic hssc hraube @ 27\m od_1405319044593_68.docx @ 192255 @ 3 @ 1 3.7.4...

  • Page 24: Measures In The Event Of Hazards And Accidents

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 3 Safety Pos : 75 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/030 Sic her heit/030-0080 Ver halten bei Gefahren und Unfäll en @ 27\mod_1405319051188_68.docx @ 192325 @ 2 @ 1 → Measures in the event of hazards and accidents •...

  • Page 25: Storage And Transport

    → Storage and transport Pos : 81 /100 Sigma/110 BA Zentrifugen Sigma (Pr ojekte) /4- 16KS_4-16KH S/040 Lagerung und Tr ans port/040-0011 Abm ess ungen und Gewic ht 4- 16KHS @ 29\m od_1405326912021_68.docx @ 198667 @ 2 @ 1 →...

  • Page 26: Packaging

    Leerz eile @ 0\m od_1202116244500_0.doc x @ 114 @ @ 1 Pos : 89 /100 Sigma/110 BA Zentrifugen Sigma (Pr ojekte) /4- 16KS_4-16KH S/040 Lagerung und Tr ans port/040-0050 Trans portsic herung 4- 16KS_KHS - Übersc hrift @ 29\mod_1405326914634_68.doc x @ 198709 @ 2 @ 1 Transport safety device Pos : 90 /100 Sigma/110 BA Zentrifugen Sigma (Pr ojekte) /4- 16KS_4-16KH S/040 Lagerung und Tr ans port/040-0051 Trans portsic herung 4- 16KS_KHS - Text @ 36\mod_1434606540750_68.doc x @ 263992 @ @ 1...

  • Page 27: Set-Up And Connection

    Pos : 96 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/050 Aufstellung und Ans chl uss/050- 0020 Energiev ers orgung------------------------------------------------------ @ 27\mod_1405319175630_68.docx @ 192409 @ 2 @ 1 → Power supply Pos : 97 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/050 Aufstellung und Ans chl uss/050- 0020-0012 Ansc hl uss art (Festk abel+Sc hutzs chalter) @ 7\m od_1306312098369_68.docx @ 43506 @ 3 @ 1 → 5.2.1...

  • Page 28: Customer-Provided Fuses

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 5 Set-up and connection Pos : 99 /100 Sigma/100 BA Zentrifugen Sigma (Standar dmodule)/050 Aufstellung und Ans chl uss/050- 0020-0020 Sic herungen baus eits ( außer 3-30KS) @ 7\mod_1306312302397_68.docx @ 43513 @ 3 @ 1 →...

  • Page 29: Using The Centrifuge

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 107 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/060- 0020-0010 Öffnen und Sc hließ en des Dec kels - 1 Sc hloss @ 27\m od_1405319202508_68.docx @ 192465 @ 3 @ 1 →...

  • Page 30: Installation Of An Angle Rotor With A Hermetic Lid

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 113 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/060- 0020-0020-0023 Eins etzen eines Wi nk elrotors mit H ermetikdeck el 10 Nm @ 29\m od_1405326759765_68.docx @ 198499 @ 4 @ 1 6.2.2.2...
  • Page 31 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge • Loosen the rotor tie-down screw anti-clockwise and remove the rotor together with the lid. • Loosen the lid by turning it anti-clockwise and then remove it. Rotor tie down screw Rotor Fig.

  • Page 32: Installation Of Accessories

    Pos : 115 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/060- 0020-0020-0032 Eins etzen v on Z ubehör 4+6plätzig 4- 16S und 4- 16KS/KH S @ 27\m od_1405319207709_68.docx @ 192535 @ 4 @ 1...
  • Page 33 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Centrifugation with low capacity • Install the sample vessels in a rotationally symmetrical manner so that the buckets and their suspensions are loaded evenly. • It is not permissible to load angle rotors on only one axis.

  • Page 34: Adapters

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 119 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/060- 0020-0020-0051 Gefäß e ( 4-16S, 4-16KS, 4-16KHS) @ 56\mod_1521541840863_68.doc x @ 559986 @ 4 @ 1 →...

  • Page 35: Control System "Spincontrol S

    6 Using the centrifuge Pos : 121 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030 Spinc ontrol S Steuer ung---------------------------------------------- @ 27\m od_1405320192364_68.docx @ 193109 @ 2 @ 1 →...

  • Page 36: Manual Mode

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 131 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0040 Auswahl, Anzeig e und Änderung von D aten @ 27\m od_1405320202914_68.docx @ 193207 @ 4 @ 1 →...

  • Page 37: Standard Menu

    6 Using the centrifuge Pos : 133 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0051 M enü Standard -nur KH S @ 27\mod_1405320205386_68.docx @ 193235 @ 4 @ 1 →...
  • Page 38 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Runtime The set runtime is displayed in the upper section of this field, with the remaining runtime shown below. The runtime is defined as the period from the start of the centrifuge to the beginning of the deceleration phase. The maximum value is 99 h 59 min 59 sec.
  • Page 39 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Rotor: rotor selection list This field shows the rotor that is currently being used. • Select the field "Rotor" and confirm the selection. A list with all of the possible rotors without buckets is displayed.
  • Page 40 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Acceleration This function is used to select an acceleration curve. One can select a linear rise (curves 0-9) or a quadratic rise (curves 10-19). The acceleration curves 20-29 can be programmed as desired (see chapter 11.3 - "Acceleration and deceleration curves").
  • Page 41 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Fig. 16: Program "RAPID_TEMP" • Press the start button in order to start the cooling/heating run. • During the cooling/heating run, only the set temperature can be changed. The current status of the program will be displayed on the status bar.
  • Page 42 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Progress indicator The progress indicator provides a quick overview of the remaining runtime of the running centrifugation run. For this purpose, a green progress bar and percentage value are displayed in the program field.

  • Page 43: Process Library Menu

    6 Using the centrifuge Pos : 135 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0055 M enü Prozes sbi bliothek @ 27\m od_1405320209123_68.docx @ 193276 @ 4 @ 1 6.3.2.6...

  • Page 44: Parameters Menu

    6 Using the centrifuge Pos : 137 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0061 M enü Param eter - nur KHS @ 27\m od_1405320221554_68.docx @ 193319 @ 4 @ 1 →...
  • Page 45 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Radius The radius determines the values of the relative centrifugal force (RCF) that the sample is subjected to. Normally, the maximum RCF value is displayed. If the value is reduced manually, a downward facing arrow "" will be displayed in the RCF field.
  • Page 46 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Temperature monitoring The control system includes a temperature monitoring function. If the actual temperature difference with regard to the set value deviates from the set temperature difference, the centrifuge will stop and an error message will be issued.
  • Page 47 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Lock In order to prevent any unauthorised use of the centrifuge, the following functions can be blocked: • Saving of programs (level 01) • Changing of parameters, short run (level 02) •...

  • Page 48: Setup Menu

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Pos : 139 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0070 M enü Setup @ 27\mod_1405320225479_68.docx @ 193361 @ 4 @ 1 →...
  • Page 49 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Start delay If the start delay function is active, the centrifuge will not start until the preset time has elapsed. The symbol "" will be displayed in the runtime field.
  • Page 50 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge System Cycles This field shows the number of cycles as well as the runtime of the rotor and buckets that are used. Info This item provides information on the software versions that are used in this centrifuge.

  • Page 51: Curve Menu

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Pos : 141 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0080 M enü Kurve @ 27\mod_1405320228169_68.docx @ 193389 @ 4 @ 1 →...

  • Page 52: 6.3.2.10 Help Menu

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 143 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0090 M enü Hilfe @ 27\mod_1405320230870_68.docx @ 193417 @ 4 @ 1 →...

  • Page 53: 6.3.2.11 Changing The Contrast

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 6 Using the centrifuge Pos : 145 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0020-0100 Kontr aständerung @ 27\m od_1405320232376_68.docx @ 193431 @ 4 @ 1 →...

  • Page 54: Saving A Program

    6 Using the centrifuge Pos : 149 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0030-0010 Programm speic her n @ 27\m od_1405320237832_68.docx @ 193487 @ 4 @ 1 →...

  • Page 55: Executing A Program

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 155 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0030-0040 Programm l ösc hen @ 27\mod_1405320245137_68.docx @ 193557 @ 4 @ 1 →...

  • Page 56: Automatic Program Rotation

    6 Using the centrifuge Pos : 157 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+S/Spinc ontrol S (Z ent7)/060- 0030-0030-0050 Autom atis che Programmrotation @ 27\m od_1405320248329_68.docx @ 193585 @ 4 @ 1 →...

  • Page 57: Options For Data Input And Output

    Pos : 159 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/060 Betrieb_Spi nc ontr ol L+ S/Spinc ontrol S (Z ent7)/060- 0030-0040 Opti onen z ur Ein- und Ausgabe von D aten (auß er 8KS) @ 27\m od_1405320251483_68.docx...

  • Page 58: Malfunctions And Error Correction

    Malfunctions and error correction Pos : 165 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/070 Störungen und F ehl ersuche/070-0012 Allgemei ne Stör ung en_Spi ncontr ol S_Tr ans portsc hrauben @ 28\m od_1405320578639_68.docx @ 194691 @ 2 @ 1 →...

  • Page 59: Emergency Lid Release

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 7 Malfunctions and error correction Pos : 167 /100 Sigma/110 BA Z entrifugen Sigma (Proj ekte)/4-16KS_4- 16KHS/070 Stör ungen und F ehl ersuche/070-0010- 0010 N otentriegel ung 4-16KS_KH S @ 29\m od_1405326955390_68.docx @ 198793 @ 3 @ 1 7.1.1...

  • Page 60: Table Of Error Codes

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 7 Malfunctions and error correction Pos : 169 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/070 Störungen und F ehl ersuche/070-0020 T abell e der F ehlerm eldung en @ 28\mod_1405320582996_68.docx @ 194761 @ 2 @ 1 →...

  • Page 61: Service Contact

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 7 Malfunctions and error correction Pos : 171 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/070 Störungen und F ehl ersuche/070-0030 Kontak t im Servic efall @ 28\m od_1405320584361_68.docx @ 194775 @ 2 @ 1 →...

  • Page 62: Maintenance And Service

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 8 Maintenance and service Pos : 174 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080 Wartung und Instandhaltung========================= @ 28\m od_1405320612731_68.docx @ 194789 @ 1 @ 1 →...

  • Page 63: Condenser (Only Refrigerated Centrifuges With An Air-Cooled Refrigeration System)

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 181 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0010- 0020 Zubehör (auß er 8K) @ 28\m od_1405320618247_68.docx @ 194845 @ 3 @ 1 →...

  • Page 64: Plastic Accessories

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 185 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0010- 0030 Rotor, Bec her und Vi elfac htr äger ( auß er Basic) @ 28\mod_1405320621063_68.docx @ 194873 @ 3 @ 1 →...

  • Page 65: Load Bearing Bolts

    8 Maintenance and service Pos : 187 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0010- 0040 Tragbolz en (außer 2-6, 2-6E, 2-7, 2-16P, 2- 16KL) @ 28\m od_1405320624792_68.docx @ 194915 @ 3 @ 1 →...

  • Page 66: Glass Breakage

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 191 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0020 Sterilisati on und Desinfek tion v on Rotork ammer und Zubehör @ 28\m od_1405320626090_68.docx @ 194929 @ 2 @ 1 →...

  • Page 67: 8.2.1 Autoclaving

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 8 Maintenance and service Pos : 193 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0020- 0010 Autoklavi eren @ 28\mod_1405320627440_68.doc x @ 194943 @ 3 @ 1 →...

  • Page 68: Service

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 8 Maintenance and service Pos : 195 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0030 Ins tandhaltungs arbeiten @ 28\mod_1405320628810_68.docx @ 194957 @ 2 @ 1 → Service In the event of service work that requires the removal of the panels, there is a risk of electric shock or mechanical injury.

  • Page 69: Return Of Defective Centrifuges Or Parts

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 8 Maintenance and service Pos : 197 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/080 War tung und Instandhaltung/080-0040 R ücks endung defekter T eile @ 28\mod_1405320630226_68.doc x @ 194971 @ 2 @ 1 →...
  • Page 70 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 8 Maintenance and service The defective part/unit must be packaged in a transport-safe manner. Please use the original packaging for the unit, if at all possible. If the product is dispatched to us in unsuitable packaging, you will be charged the cost for returning it to you in new packaging.

  • Page 71: Disposal

    Pos : 201 /010 Univ ers almodul e/ Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 202 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/090 Entsorgung/090-0010 Entsorgung der Z entrifuge---------------------------------------------- @ 28\m od_1405320660029_68.docx @ 194999 @ 2 @ 1 →...

  • Page 72: 10 Technical Data

    Pos : 208 /100 Sigma/110 BA Z entrifugen Sig ma (Proj ekte)/4-16KS_4- 16KHS/100 T ec hnisc he D aten/100 T ec hnis che D aten 4- 16KH S - T ext ============================== @ 29\m od_1405326981390_68.docx @ 198807 @ @ 1...

  • Page 73: Ambient Conditions

    Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1 Pos : 213 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/100 T ec hnisc he D aten/100- 0020 Technisc he Dok um entation @ 28\m od_1405320681369_68.docx @ 195055 @ 2 @ 1 →...

  • Page 74: 11 Appendix

    → 11 Appendix Pos : 217 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/110 Anhang/110-0010 Z ubehör programm (ohne T abell e, mit Hinw eis Beil agebl ätter) @ 56\m od_1523438203637_68.docx @ 560428 @ 2 @ 1 → 11.1...

  • Page 75: Speed-Gravitational-Field-Diagram

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  • Page 76: Acceleration And Deceleration Curves

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix Pos : 224 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/110 Anhang/110-0031 Beschl eunigungs- und Bremsk urven Spinc ontrol S @ 28\mod_1405320708834_68.doc x @ 195181 @ 2 @ 1 →...
  • Page 77 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix Fig. 39: Diagram of linear curves Fig. 40: Diagram of quadratic curves Pos : 225 /010 Univ ers almodul e/Seitenwechs el @ 0\mod_1202116244312_0.docx @ 105 @ @ 1 Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 77 / 91 Translation of the original operating manual, part no.

  • Page 78: Table Of The Service Life Of Rotors And Accessories

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  • Page 79: Resistance Data

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix Pos : 228 /100 Sigma/100 BA Z entrifugen Sigma (Standardm odul e)/110 Anhang/110-0050 Beständigkeits tabelle @ 28\mod_1405320711439_68.doc x @ 195209 @ 2 @ 1 → 11.5 Resistance data The data refer to resistance at 20°C.
  • Page 80 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Chromic acid Chromic potassium KCr(SO saturated sulphate Citric acid Citric acid Copper sulphate CuSO x 5H...
  • Page 81 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Isopropyl alcohol Lactic acid Magnesium chloride MgCl Mercuric chloride HgCl Mercury Methyl acetate Methyl alcohol...
  • Page 82 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Sodium bisulphite NaHSO Sodium carbonate Sodium chloride NaCl Sodium hydroxide NaOH Sodium hydroxide NaOH Sodium sulfate...

  • Page 83: Ec Declaration Of Conformity

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  • Page 84 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 84 / 91 Translation of the original operating manual, part no. 0701802...

  • Page 85: Declaration Of Conformity - China Rohs 2

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix Declaration of conformity – China RoHS 2 11.7 Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 85 / 91 Translation of the original operating manual, part no. 0701802...
  • Page 86 Refrigerated Centrifuge with Heating System Sigma 4-16KHS 11 Appendix === Ende der Liste für T extm arke Inhalt === Version 10/2012, Rev. 1.22 of 08/05/2020 • sb 86 / 91 Translation of the original operating manual, part no. 0701802...

  • Page 87: 12 Index

    Refrigerated Centrifuge with Heating System Sigma 4-16KHS Index 12 Index Centrifugation with vessels of various sizes 32 Centrifuge cannot be started ...... 58 Acceleration ..........40 Centrifuge decelerates during operation ..58 Acceleration curve ......40, 51, 76 Centrifuge is inclined ........58 Acceleration curve (changing) ....
  • Page 88 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Index Dangerous materials ........66 Functional and operating elements .... 11 Date of manufacture ........12 Fuses have tripped ........58 Deactivating the help function ....52 Deceleration (brake) ........40 General conditions ........9 Deceleration curve ......
  • Page 89 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Index No power in the mains supply ....58 Noise level ..........72 Kinetic energy ........12, 72 Nominal voltage ......... 12 Notes on safety and hazards ....... 9 Language ........... 49 Notes on transport ........25 Layout of the centrifuge......
  • Page 90 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Index Screws of the transport safety device are not removed ..........58 Radioactive substances ....... 19, 62 Selection, display, and modification of data 36 Radius ..........14, 45 Serial number ........ 12, 61, 68 RAPID_TEMP program ......
  • Page 91 Refrigerated Centrifuge with Heating System Sigma 4-16KHS Index Type............. 12, 72 Type of connection ........27 Table of error codes ........60 Type of the centrifuge ......61, 68 Table of rotors and accessories with a different service life ......21, 78 Technical data ...........

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