Agilent Technologies 8355 Sulfur User Manual page 117

Chemiluminescence detectors
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SCD and NCD User Manual
Table 15
NCD Checkout conditions (continued)
Solvent Wash Draw Speed (7693A)
Solvent Wash Dispense Speed
(7693A)
Sample Wash Draw Speed (7693A)
Sample Wash Dispense Speed
(7693A)
Inject Dispense Speed (7693A)
Plunger speed (7683)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
Data system
Data rate
7
If using a data system, prepare the data system to perform
one run using the loaded checkout method. Make sure that
the data system will output a chromatogram. If not using a
data system, create a one sample sequence using the GC
keypad.
8
Start the run. If performing an injection using an
autosampler, start the run using the data system or press
[Start] on the GC.If performing a manual injection (with or
without a data system):
Press [Prep Run] to prepare the inlet for splitless injection.
a
b
When the GC becomes ready, inject 1 μL of the checkout
sample and press [Start] on the GC.
Performance Verification
150
1500
150
1500
3000
Fast, for all inlets except COC.
0
0
1 µL
5 Hz (Front detector, NCD)
7
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