Agilent Technologies 8355 Sulfur User Manual page 116

Chemiluminescence detectors
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7
Performance Verification
116
Table 15
NCD Checkout conditions (continued)
Septum purge
Detector
Base temperature
Burner temperature
Chiller temperature
H
flow
2
Oxidizer flow
O3 Generator
O3 Generator flow
Vacuum pump
Oven
Initial temp
Initial time
Rate 1
Ramp 1 temp
Ramp 1 hold time
Post run temp
ALS settings (if installed)
Sample washes
Sample pumps
Sample wash volume
Injection volume
Syringe size
Solvent A pre washes
Solvent A post washes
Solvent A wash volume
Solvent B pre washes
Solvent B post washes
Solvent B wash volume
Injection mode (7693A)
Airgap Volume (7693A)
Viscosity delay
15 mL/min
280°C
900 °C
On
3 mL/min
8 mL/min, Oxygen
On
On
On
50 °C
3.0 min
25 °C/min
250 °C
2 min
50 °C
2
6
8 µL (maximum)
1 µL
10 µL
0
3
8 µL (maximum)
0
3
8 µL (maximum)
Normal
0
0
SCD and NCD User Manual

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