Agilent Technologies 8355 Sulfur User Manual page 111

SCD and NCD User Manual
Table 14 SCD Checkout conditions (continued)
Burner temperature
Upper H flow
2
Lower H flow
2
Oxidizer flow
O3 Generator
O3 Generator flow
Vacuum pump
FID-SCD Tandem settings
FID temp
FID hydrogen flow
FID air flow
FID N makeup flow
2
SCD oxidizer flow
SCD upper H flow
2
Lower H flow
2
Oven
Initial temp
Initial time
Rate 1
Ramp 1 temp
Ramp 1 hold time
Post run temp
ALS settings (if installed)
Sample washes
Sample pumps
Sample wash volume
Injection volume
Syringe size
Solvent A pre washes
Solvent A post washes
Solvent A wash volume
Solvent B pre washes
Performance Verification
800 °C
38 mL/min
8 mL/min
50 mL/min, Air
On
On
On
350 °C
35 mL/min
500 mL/min
20 mL/min
0
40 mL/min
Not applicable for FID-SCD
50 °C
3.0 min
25 °C/min
160 °C
2 min
50 °C
2
6
8 µL (maximum)
1 µL
10 µL
0
3
8 µL (maximum)
0
7
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