Hach DR2400 Manual page 785

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25 mL
20 mL
10 mL
17.
Wipe the prepared
sample and place it into
the cell holder.
Sample Collection, Preservation, and Storage
Accuracy Check
VolatileAci_None_Other_ESR_Eng_Ody.fm
Read
18.
Touch
.
Read
Results will appear in
mg/L HOAC.
Collect samples in clean plastic or glass bottles. Analyze as soon as possible after
collection. Samples can be stored for up to 24 hours by cooling to 4 °C (40 °F) or
below. Warm samples to room temperature before analysis.
Standard Additions Method (Sample Spike)
1. After reading test results, leave the sample cell (unspiked sample) in the
instrument.
2. Touch
. Touch
Options
additions procedure will appear.
3. Touch
to accept the default values for standard concentration, sample
OK
volume, and spike volumes. Touch
are accepted, the unspiked sample reading will appear in the top row. See
Standard Additions in the instrument manual for more information.
4. Snap the neck off a Volatile Acid Voluette
acetic acid.
5. Prepare three sample spikes. Fill three Mixing Cylinders (Cat. No. 1896-40)
with 25 mL of sample. Use the TenSette
0.3 mL of standard, respectively, to each sample and mix thoroughly.
6. Analyze each sample spike as described in the procedure above, starting with
the 0.1 mL sample spike. Accept each standard additions reading by touching
. Each addition should reflect approximately 100% recovery.
Read
7. After completing the sequence, touch
the standard additions data points, accounting for matrix interferences. Touch
, then select
View: Fit
the sample spikes and the "Ideal Line" of 100% recovery.
See Section 3.2.2 Standard Additions on page 32 for more information.
. A summary of the standard
Standard Additions
to change these values. After values
Edit
®
Ampule Standard, 62,500-mg/L as
®
Pipet to add 0.1 mL, 0.2 mL, and
Graph
and touch
Ideal Line
OK
Volatile Acids
to view the best-fit line through
to view the relationship between
Volatile Acids
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