Nitrite; Method 8153; Powder Pillows - Hach DR2400 Manual

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DR/2400

Method 8153

Powder Pillows

Scope and Application:
* Adapted from McAlpine, R. and Soule, B., Qualitative Chemical Analysis, New York, 476, 575 (1933)
Tips and Techniques
• For more accurate results, determine a reagent blank value for each new lot of reagent. Follow the procedure using deionized
water in place of the sample. Subtract the reagent blank value from the final results or perform a reagent blank adjust
instrument manual for more information on Running a Reagent Blank.
• After adding the reagent, a greenish-brown color will develop if nitrite is present.
• Wipe the outside of sample cells before each insertion into the instrument cell holder. Use a damp towel followed by a dry one to
remove fingerprints or other marks.
Powder Pillows
Hach Programs
1.
Touch
Hach Programs
Select program
.
373 N, Nitrite HR
Touch
.
Start
Nitrite_PP_High_FES_Eng_Ody.fm
For water and wastewater
2.
Fill a round sample
cell with 10 mL of
sample.
3.
Add the contents of
®
one NitriVer

2 Nitrite

Reagent Powder Pillow.
Cap and shake to
dissolve (this is the
prepared sample).
Nitrite
Ferrous Sulfate Method*
HR (2 to 250 mg/L NO
.
See the
Method 8153
4.
Touch the timer icon.
Touch
.
OK
A ten-minute reaction
period will begin.
To prevent low results,
leave the sample on a flat
surface and do not
disturb it during the
reaction period.
Nitrite
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