Page 1 Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual...
Page 2 This guide is valid for A.01.xx revisions of operating procedure, practice, or the Agilent 1100 Series Diode Array and the like that, if not correctly Multiple Wavelength Detectors software, performed or adhered to, could...
Page 3 Documentation). If a federal government DFARS 227.7202-3 (Rights in Commercial or other public sector Customer has a need for 1100 Series DAD and MWD Reference Manual I This Guide… This manual contains information for using your Diode Array and Multiple Wavelength Detectors.
Page 4: Table Of Contents
Agilent 1100 diode array detector (DAD) with the Agilent 1100 control module. 8 Specifications Performance specifications of the detector Annex A Safety Information 1100 Series DAD and MWD Reference Manual Contents Installing the Detector Site Requirements Physical Specifications...
Page 5 Sample and Reference Wavelength and Bandwidth Slit Width Optimizing Spectral Acquisition (DAD only) Margin for Negative Absorbance Optimizing Selectivity Quantifying Coeluting Peaks by Peak Suppression Ratio Qualifiers for Selective Detection of Compound Classes 1100 Series DAD and MWD Reference Manual...
Page 6 Leak Sensor Short Compensation Sensor Open Compensation Sensor Short Fan Failed Open Cover Cover Violation Visible Lamp Current Visible Lamp Voltage Communication Error Calibration Values Invalid Diode Current Leakage Holmium Oxide Test Failed 1100 Series DAD and MWD Reference Manual...
Page 7 Holmium Oxide Test Intensity Test Cell Test Dark-Current Test Filter Test Repairing the Detector Introduction into Repairing the Detector Using the ESD Strap Overview of the Repairing of the Detector Simple Repairs Exchanging a Lamp 1100 Series DAD and MWD Reference Manual...
Page 8 Entering the Serial Number using the Agilent ChemStation Exchanging the Fan (G1315A/G1365A) Replacing Fan Parts (G1315B/G1365B) Removing the Optical Unit (G1315A/G1365A) Removing the Optical Unit (G1315B/G1365B) Exchanging the Source Lens (Achromat) Assembly Replacing the Holmium Oxide Filter Motor 1100 Series DAD and MWD Reference Manual...
Page 9 Standard Flow Cell Semi-Micro Flow Cell High Pressure Flow Cell Nano Flow Cells Fan Assembly Parts Holmium Oxide Filter Coupling Lens Assembly Source Lens (Achromat) Assembly Cell Support Assembly Control Module Sheet Metal Kit (G1315A/G1365A) 1100 Series DAD and MWD Reference Manual...
Page 10 External Contact Cable RS-232 Cable Kit LAN Cables Introduction to the Detector Introduction to the Detector Optical System Overview Electrical Connections Instrument Layout Early Maintenance Feedback (EMF) EMF Counters Using the EMF Counters 1100 Series DAD and MWD Reference Manual...
Page 11 Analog Signal Output GPIB Interface CAN Interface Remote Interface RS-232C Setting the 8-bit Configuration Switch GPIB Default Addresses Communication Settings for RS-232C Communication Forced Cold Start Settings Stay-Resident Settings The Main Power Supply Assembly 1100 Series DAD and MWD Reference Manual...
Page 12 Performance Specifications Safety Information General Safety Information Lithium Batteries Information Disposal of Mercury from Deuterium Lamp Radio Interference Sound Emission UV-Radiation Solvent Information Declaration of Conformity for HOX2 Filter Agilent Technologies on Internet Index 1100 Series DAD and MWD Reference Manual...
Page 13: Installing The Detector
1100 Series DAD and MWD Reference Manual Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Installing the Detector Site Requirements Physical Specifications Unpacking the Detector Optimizing the Stack Configuration Installing the Detector Flow Connections to the Detector...
Page 14: Site Requirements
It plugs into the power-input socket at the rear of the detector. The male end of each power cord is different and designed to match the wall socket of a particular country or region. 1100 Series DAD and MWD Reference Manual...
Page 15 8 cm (3.1 inches) in the rear for air circulation and electric connections. If the bench should carry a Agilent 1100 Series system, make sure that the bench is designed to bear the weight of all modules.
Page 16: Physical Specifications
° Operating altitude Up to 2000 m (6500 ft) Non-operating altitude Up to 4600 m (14950 ft) For storing the detector Safety standards: IEC, CSA, UL, EN Installation category II, pollution degree 2 1100 Series DAD and MWD Reference Manual...
Page 17: Unpacking The Detector
Please report missing or damaged parts to your local Agilent Technologies sales and service office. Table 2 Detector Checklist Description Quantity Detector Power cable UV-lamp (Part number 5181-1530) CAN cable (Part number 5181-1516) Flow cell As ordered Reference Manual 1100 Series DAD and MWD Reference Manual...
Page 18 Hex key set 1 – 5 mm 8710-0641 Wrench open end 1/4 – 5/16 inch 8710-0510 Wrench open end 4 mm 8710-1534 ESD wrist strap 9300-1408 Fitting male PEEK Tubing Figure 1 Waste Tubing Parts 1100 Series DAD and MWD Reference Manual...
Page 19 Installing the Detector Ferrule front This side is Ferrule back preinstalled Fitting male SST Capillary Figure 2 Inlet Capillary (Col umn-Detector) Parts 1100 Series DAD and MWD Reference Manual...
Page 20: Optimizing The Stack Configuration
Installing the Detector Optimizing the Stack Configuration If your detector is part of a complete Agilent 1100 Series system, you can ensure optimum performance by installing the following configuration. This configuration optimizes the system flow path, ensuring minimum delay volume.
Page 21 Installing the Detector Figure 4 Recommended Stack Configuration (Rear View) 1100 Series DAD and MWD Reference Manual...
Page 22: Installing The Detector
Interface Board” on page 179. 2 Place the detector in the stack or on the bench in a horizontal position. 3 Ensure the line power switch at the front of the detector is OFF. 1100 Series DAD and MWD Reference Manual...
Page 23 Front View of Detector 4 Connect the power cable to the power connector at the rear of the detector. 5 Connect the CAN cable to other Agilent 1100 Series modules. 6 If a Agilent ChemStation is the controller, connect either •...
Page 24 NOTE The detector was shipped with default configuration settings. To change these settings Setting the 8- it Co figu atio S it h on page 261. 1100 Series DAD and MWD Reference Manual...
Page 25: Flow Connections To The Detector
The flow cell is shipped with a filling of isopropanol (also recommended when the NOTE instrument and/or flow cell is shipped to another location). This is to avoid breakage due to subambient conditions. 1100 Series DAD and MWD Reference Manual...
Page 26 Installing the Detector 3 Insert the flow cell and install the capillaries to the capillary holder (top is inlet, bottom is outlet). 1100 Series DAD and MWD Reference Manual...
Page 27 Installing the Detector 1100 Series DAD and MWD Reference Manual...
Page 28 Installing the Detector 7 Assemble the waste tubing from the accessory kit. 8 Connect the waste tubing to the bottom fitting holder and a waste tub 1100 Series DAD and MWD Reference Manual...
Page 29 Some types of the Agilent deuterium lamps show a light ring during operation. This is UV-Radiatio not harmful, refer to on page 307. 1100 Series DAD and MWD Reference Manual...
Page 30: How To Optmize The Detector
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual How to optmize the Detector Optimizing the Detector Performance Optimization Overview Optimizing for Sensitivity, Selectivity, Linearity and Dispersion Optimizing Selectivity...
Page 31: Optimization Overview
Follow these rules as a start for new applications. It gives rules-of-thumb for optimizing detector parameters. Optimization Overview Table 4 Optimization Overview Parameter Impact • Selection of flow cell peak resolution versus • sensitivity Choose flow cell according to used column, see Figure 1100 Series DAD and MWD Reference Manual...
Page 32 Set step to 4 nm for normal use; set small step (and slit width) if high resolution of spectra with fine structure is wanted. Typical column Typical peak Recommended flow cell length width T<= 5 cm 0.025 min High pressure flow cell for 1100 Series DAD and MWD Reference Manual...
Page 33: Optimizing For Sensitivity, Selectivity, Linearity And Dispersion
Therefore, flow cells with longer path lengths yield higher signals. Although noise usually increases little with increasing path length, there is a gain in signal-to-noise ratio. For example, in Figure 8 the noise increased by less than 10 % but a 70 % 1100 Series DAD and MWD Reference Manual...
Page 34 Path length Path length Correction factor (nominal) (actual) Standard flow cell 13 µl G1315-60012 10 mm 9.80 ± 0.07 mm 10/9.8 Semi-micro flow cell 5 µl G1315-60011 6 mm 5.80 ± 0.07 mm 6/5.8 1100 Series DAD and MWD Reference Manual...
Page 35: Peak Width (Response Time)
(response time) by factor of two from the recommended setting (over- filtering) will reduce peak height by about 20 % and reduce baseline noise by a factor of 1.4. This gives you the best possible signal-to-noise ratio, but may affect peak resolution. 1100 Series DAD and MWD Reference Manual...
Page 36: Sample And Reference Wavelength And Bandwidth
200 – 300 nm minus the average absorbance from 300 – 400 nm. As all analytes show higher absorbance at 200 – 300 nm than at 300 – 1100 Series DAD and MWD Reference Manual...
Page 37 2.5, whereas the signal is about 75 % of a 4-nm wide band. The signal- to-noise ratio for a 30 nm bandwidth is twice that for a 4-nm bandwidth in our example. 1100 Series DAD and MWD Reference Manual...
Page 38 No reference Time (min) Grad.: 0.02 m KH /ACN from 12% ACN to 45% ACN in 12 min Figure 12 Gradient Analysis of PTH-Amino Acids (1 pmol each), with and without Refer- ence 1100 Series DAD and MWD Reference Manual...
Page 39: Slit Width
Slit width 16 nm Figure 14 Influence of the Slit Width on Baseline Noise However, with a wider slit, the spectrograph’s optical resolution (its ability to distinguish between different wavelengths) diminishes. Any photodiode receives light 1100 Series DAD and MWD Reference Manual...
Page 40 Use a wide (8 or 16 nm) slit when your sample contains very small concentrations. Always use signals with bandwidth at least as wide as the slit width. 1100 Series DAD and MWD Reference Manual...
Page 41: Optimizing Spectral Acquisition (Dad Only)
However a step of 2 nm gives a better display of the spectrum. Threshold Sets the peak detector. Only spectra from peaks higher than threshold will be stored when a peak-controlled storage mode is selected. 1100 Series DAD and MWD Reference Manual...
Page 42: Margin For Negative Absorbance
(about -100 mAU). In some special case, for example, when gradient with absorbing solvents are used, the baseline may drift to more negative values. Only for such cases, increase the margin for negative absorbance to avoid overflow of the analog-to-digital converter. 1100 Series DAD and MWD Reference Manual...
Page 43: Optimizing Selectivity
To suppress caffeine, the reference wavelength must be set to 282 nm. At this wavelength, caffeine shows exactly the same absorbance as at 222 nm. When the absorbance values are subtracted 1100 Series DAD and MWD Reference Manual...
Page 44: Ratio Qualifiers For Selective Detection Of Compound Classes
When the ratio falls within the range, the signal output corresponds to the normal absorbance, giving single, clear peaks on a flat baseline. An example is shown in Figure 17 Figure 1100 Series DAD and MWD Reference Manual...
Page 45 10%). Only when the ratio between 249 and 224 nm was within this range, is the signal plotted. Of all four peaks, only the third fulfilled the criterion (Figure 18) . The others were not plotted. 1100 Series DAD and MWD Reference Manual...
Page 46: Troubleshooting And Test Functions
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Troubleshooting and Test Functions O e ie of the Dete to ’s I di ato s a d Test Fu tio s Status Indicators Error Messages Wavelength Recalibration Test Functions...
Page 47: Status Indicators
(see on page 85). Status Indicators Two status indicators are located on the front of the detector. The lower left indicates the power supply status, the upper right indicates the detector status. 1100 Series DAD and MWD Reference Manual...
Page 48: Power Supply Indicator
Usually, an error condition requires attention (e.g. leak, defective internal components). An error condition always interrupts the analysis. 1100 Series DAD and MWD Reference Manual...
Page 49: Error Messages
This section describes the meaning of detector error messages, and provides information on probable causes and suggested actions how to recover from error conditions. 1100 Series DAD and MWD Reference Manual...
Page 50: Timeout
• A not-ready state was present during a sequence or multiple-injection run for a period longer than the timeout threshold. ✔ Suggested Actions Check the logbook for the occurrence and source of a not- ready condition. Restart the analysis where required. 1100 Series DAD and MWD Reference Manual...
Page 51: Shutdown
Ensure the instrument showing the not-ready condition is installed correctly, and is set up correctly for analysis. ✔ Exchange the remote cable. ✔ Check the instrument for defects (refer to the instrument’s reference documentation). 1100 Series DAD and MWD Reference Manual...
Page 52: Synchronization Lost
Probable Causes • Loose fittings. • Broken capillary. • Leaking flow cell. Suggested Actions ✔ Ensure all fittings are tight. ✔ Exchange defective capillaries. ✔ Exchange flow cell components. 1100 Series DAD and MWD Reference Manual...
Page 53 4 of the sampler switching valve. This tube can then be taken to waste separately. The tube which normally serves as the detector cell outlet tube can be used for this purpose. 1100 Series DAD and MWD Reference Manual...
Page 54: Leak Sensor Open
If the current falls outside the lower limit, the error message is generated. Probable Causes • Leak sensor not connected to the detector main board. • Defective leak sensor. Suggested Actions ✔ Ensure the leak sensor is connected correctly. ✔ Exchange the leak sensor. 1100 Series DAD and MWD Reference Manual...
Page 55: Leak Sensor Short
If the current increases above the upper limit, the error message is generated. Probable Causes • Defective leak sensor. Suggested Actions ✔ Exchange the leak sensor. 1100 Series DAD and MWD Reference Manual...
Page 56: Compensation Sensor Open
If the resistance across the sensor increases above the upper limit, the error message is generated. Probable Causes • Defective detector main board. Suggested Actions ✔ Exchange the detector main board. 1100 Series DAD and MWD Reference Manual...
Page 57: Compensation Sensor
If the resistance across the sensor falls below the lower limit, the error message is generated. Probable Causes • Defective detector main board. Suggested Actions ✔ Exchange the detector main board. 1100 Series DAD and MWD Reference Manual...
Page 58: Fan Failed
Probable Causes • Fan cable disconnected. • Defective fan. • Defective detector main board. Suggested Actions ✔ Ensure the fan is connected correctly. ✔ Exchange fan. ✔ Exchange the detector main board. 1100 Series DAD and MWD Reference Manual...
Page 59: Open Cover
Probable Causes • The top foam was removed during operation. • Foam not activating the sensor. Suggested Actions ✔ Replace the top foam. ✔ Exchange the foam. 1100 Series DAD and MWD Reference Manual...
Page 60: Cover Violation
Probable Causes • The top foam was removed during operation. • Foam not activating the sensor. Suggested Actions ✔ Replace the top foam. ✔ Exchange the foam. 1100 Series DAD and MWD Reference Manual...
Page 61: Visible Lamp Current
Probable Causes • Defective detector main board. • Defective power supply. Suggested Actions ✔ Exchange the detector main board. ✔ Exchange the power supply. 1100 Series DAD and MWD Reference Manual...
Page 62: Communication Error
Probable Causes • Random communication error. • Defective detector main board. Suggested Actions ✔ Switch the detector off and on again at the power switch. If the error reoccurs, exchange the detector main board. 1100 Series DAD and MWD Reference Manual...
Page 63: Calibration Values Invalid
If the data are invalid or cannot be read from the spectrometer ROM, the error message is generated. Probable Causes • Defective detector main board. • Defective optical unit. Suggested Actions ✔ Exchange the detector main board. ✔ Exchange the optical unit. 1100 Series DAD and MWD Reference Manual...
Page 64: Diode Current Leakage
If the leakage current exceeds the upper limit, the error message is generated. Probable Causes • Defective optical unit. • Defective detector main board. Suggested Actions ✔ Exchange the optical unit. ✔ Defective detector main board. 1100 Series DAD and MWD Reference Manual...
Page 65: Holmium Oxide Test Failed
If the anode current falls below the lower current limit, the error message is generated. Probable Causes • UV lamp disconnected. • Defective UV lamp or non-Agilent lamp. • Defective detector main board. • Defective power supply. 1100 Series DAD and MWD Reference Manual...
Page 66: Uv Lamp Voltage
• Defective UV lamp or non-Agilent lamp. • Defective detector main board. • Defective power supply. Suggested Actions ✔ Exchange the UV lamp. ✔ Exchange the detector main board. ✔ Exchange the power supply. 1100 Series DAD and MWD Reference Manual...
Page 67: Uv Ignition Failed
• Defective UV lamp or non-Agilent lamp. • Defective detector main board. • Defective power supply. Suggested Actions ✔ Ensure the UV lamp is connected. ✔ Replace the top foam, and turn on the lamp. 1100 Series DAD and MWD Reference Manual...
Page 68: New Messages With The G1315B And G1365B Detectors
New Messages with the G1315B and G1365B detectors With the introduction of the G1315B DAD and the G1365B MWD a few new messages have been added to address the additional heating control for stabilization of the baseline in unstable environment. 1100 Series DAD and MWD Reference Manual...
Page 69: Module Type Changed
3 because the temperature hardware is detected again (see below). Type B, Parameter 1 or 3 Probable Causes • Detector has recognized the hardware for temperature control. This is because the detector didn't find the temperature hardware at last switch-on. 1100 Series DAD and MWD Reference Manual...
Page 70 Troubleshooting and Test Functions Suggested Actions ✔ Power cycle the detector. 1100 Series DAD and MWD Reference Manual...
Page 71: Illegal Value From Temperature Sensor Mounted On The Fan
• Detector is exposed to illegal ambient conditions. Suggested Actions ✔ Ensure the connector to the detector main board is seated firmly. ✔ Verify that the ambient conditions are within the allowed range. ✔ Exchange temperature sensor assembly. 1100 Series DAD and MWD Reference Manual...
Page 72 Probable Causes • The sensor is defect • Detector is exposed to illegal ambient conditions. Suggested Actions ✔ Verify that the ambient conditions are within the allowed range. ✔ Exchange detector main board. 1100 Series DAD and MWD Reference Manual...
Page 73: Heater Failed
If the test fails an error event is created. As a result the temperature control is switched off. Probable Causes • Defective connector or cable. • Defective heater. Suggested Actions ✔ Ensure the connector to the detector main board is seated firmly. ✔ Exchange heater assembly. 1100 Series DAD and MWD Reference Manual...
Page 74: Heater Power At Limit
• Ambient conditions have changed too much during the run, so that optimum results may not be guaranteed. Suggested Actions ✔ Verify that the reproducibility of your results is not affected ✔ Expose the detector to more stable ambient conditions. 1100 Series DAD and MWD Reference Manual...
Page 75: Wavelength Recalibration
Holmium Oxide Test The built-in holmium oxide filter is used for verification of wavelength accuracy at three additional wavelengths. The test evaluates the results automatically, and provides a spectrum of the holmium oxide filter. 1100 Series DAD and MWD Reference Manual...
Page 76: Holmium Oxide Test
84). When the test is started, the 1-nm slit is moved into the light path automatically. To eliminate effects due to absorbing solvents, the test should be done with water in the flow cell. 1100 Series DAD and MWD Reference Manual...
Page 77 The test fails if one or more of the maxima lies outside of the limits (see Figure 22). Figure 22 Holmium Oxide Test Results Test Failed Probable Causes • Absorbing solvent or air bubble in flow cell. • Incorrect calibration • Dirty or contaminated flow cell. 1100 Series DAD and MWD Reference Manual...
Page 78: Intensity Test
The shape of the intensity spectrum is primarily dependent on the lamp, grating, and diode array characteristics. Therefore, intensity spectra will differ slightly between instruments. Figure 23 shows a typical intensity test spectrum. 1100 Series DAD and MWD Reference Manual...
Page 79 Intensity Test Results Test Failed Probable Causes • Absorbing solvent or air bubble in flow cell. • Dirty or contaminated flow cell. • Dirty or contaminated optical components (achromat, windows). • Old or non-Agilent lamp. 1100 Series DAD and MWD Reference Manual...
Page 80: Cell Test
(typically between 0.5 and 0.7) is dependent on the degree of contamination of the flow cell windows, and on the type of flow cell used. Figure 25 Cell Test Results Test Failed (low ratio value) Probable Causes • Absorbing solvent or air bubble in flow cell. 1100 Series DAD and MWD Reference Manual...
Page 81: Dark-Current Test
26). The leakage current (represented in counts) for each diode should fall within the limits (red bands) shown in the plot (see Figure 26). Figure 26 Dark-Current Test Dark-Current Test Evaluation Figure 27 Dark-Current Test Results Test Failed Probable Causes 1100 Series DAD and MWD Reference Manual...
Page 82 Troubleshooting and Test Functions • Defective optical unit. Suggested Actions ✔ Exchange the optical unit. 1100 Series DAD and MWD Reference Manual...
Page 83: Filter Test
Holmium Oxide Maximum out of Limits Probable Causes • Holmium oxide filter not installed. • Dirty or contaminated filter. Suggested Actions ✔ Install the holmium oxide filter. ✔ Exchange the holmium oxide filter. 1100 Series DAD and MWD Reference Manual...
Page 84 Troubleshooting and Test Functions 1100 Series DAD and MWD Reference Manual...
Page 85: Repairing The Detector
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Repairing the Detector Introduction into Repairing the Detector Overview of the Repairing of the Detector Simple Repairs Exchanging Internal Parts...
Page 86: Introduction Into Repairing The Detector
When working with solvents please observe appropriate safety procedures (for WARNING example, goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the solvent vendor, especially when toxic or hazardous solvents are used. 1100 Series DAD and MWD Reference Manual...
Page 87: Using The Esd Strap
2 Unroll the rest of the band and peel the liner from the copper foil at the opposite end. 3 Attach the copper foil to a convenient and exposed electrical ground. 1100 Series DAD and MWD Reference Manual...
Page 88: Overview Of The Repairing Of The Detector
With the introduction of the G1315B/G1365B DAD/MWD some of the metal plates look different (no air openings) compared to the G1315A/G1365A DAD/MWD. The figures have changed for specific repairs only. Figure 29 shows the main assemblies and their locations. 1100 Series DAD and MWD Reference Manual...
Page 89: Simple Repairs
Table 7 Simple Repairs Procedure Typical Frequency Notes Deuterium lamp or If noise and/or drift exceeds your application limits An intensity test should be performed tungsten lamp or lamp does not ignite. after replacement. exchange 1100 Series DAD and MWD Reference Manual...
Page 90: Exchanging A Lamp
Tools required Screwdriver POZI 1 PT3 Parts required Longlife Deuterium lamp 2140-0813 ( without black cover ) Longlife Deuterium lamp 5181-1530 (with black cover) Deuterium lamp 2140-0590 (without black cover) Tungsten lamp G1103-60001 1100 Series DAD and MWD Reference Manual...
Page 91 Repairing the Detector Disconnect lamp from the connector and unscrew the lamp. Remove the lamp. Do not touch the glass bulb with your fingers. 1100 Series DAD and MWD Reference Manual...
Page 92 When replacing the vis-lamp, assure that the vis-lamp is Insert the lamp. Fix the screws and reconnect the lamp to inserted as shown (flat edge towards the deuterium lamp - connector. opposite as in the figure). Replace the front cover. 1100 Series DAD and MWD Reference Manual...
Page 93 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 94: Exchanging A Flow Cell
Semi-micro flow cell, 6 mm, 5 µl, 120 bar, G1315-60011 High pressure flow cell, 6 mm, 1.7 µl, 400 bar, G1315-60015 Na o Flo Cell - Repla i g o Clea i g Nano flow cell, refer to on page 122 1100 Series DAD and MWD Reference Manual...
Page 95 If you want to replace flow cell parts, see Repairi g the Sta dard or Se i-Micro Flow Cell Repairi g the Sta dard or on page 108 or Semi-Micro Flo Cell on page 108. 1100 Series DAD and MWD Reference Manual...
Page 96: Repairing The Standard Or Semi-Micro Flow Cell
Two 1/4 inch wrenches for capillary connections hexagonal key 4 mm Tooth picks Sta da d Flo Cell Se i-Micro Parts required For parts, see on page 186 and Flow Cell on page 188 1100 Series DAD and MWD Reference Manual...
Page 97 Turn off the flow. • from Remove the front cover. the cell • Remove the flow cell, see body. E ha gi g a Flo Cell on page 105. gasket windows assembly 1100 Series DAD and MWD Reference Manual...
Page 98 Use a tooth pick to remove the quartz window from the window assembly. If you want to replace the gasket only, continue with step 8. Do not mix the gasket #6 and # 7. They are different for standard and semi-mirco flow cell. 1100 Series DAD and MWD Reference Manual...
Page 99 Repairing the Detector Assemble the washers and the window assembly in Correct orientation of spring washers [2] is required. correct order. 1100 Series DAD and MWD Reference Manual...
Page 100 Repairing the Detector Press the window assembly onto the new or cleaned quartz window. Press the Teflon® ring into window assembly. 1100 Series DAD and MWD Reference Manual...
Page 101: Repairing The High Pressure Flow Cell
If the flow cell needs repair due to leaks or contaminations (reduced light throughput) Tools required Two 1/4 inch wrenches for capillary connections hexagonal key 4 mm Tooth picks High P essu e Flo Cell Parts required For parts see on page 190 1100 Series DAD and MWD Reference Manual...
Page 102 1 Remove the window assembly the cell body. from procedure: • Turn off the flow. • Remove the front cover. • Remove the flow cell, E ha gi g a Flow Cell on page 105. 1100 Series DAD and MWD Reference Manual...
Page 103: Replacing Capillaries On A Standard Flow Cell
Sta da d Flo Cell Parts required For parts see on page 1 Identify the inlet and outlet capillaries. Preparations for this procedure: • Turn off the flow. • Remove the front cover. 1100 Series DAD and MWD Reference Manual...
Page 104 Repairing the Detector • Remove the Inlet capillary flow cell, E ha gi g a Flo Cell on page 105. Outlet capillary 1100 Series DAD and MWD Reference Manual...
Page 105 When retightening the fittings, make sure that they carefully tightened (handtight plus turn with a wrench). Otherwise damage of the flow cell body blockage may result. Outlet capillary 1100 Series DAD and MWD Reference Manual...
Page 106 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 107 Repairing the Detector 9 The capillary and should be tied 10 Insert the fixing screw, so that the capillary cannot lays in the grove around leave the grove. 1100 Series DAD and MWD Reference Manual...
Page 108 Repairing the Detector the body (in the Screw grove) 5 times. Inlet capillary with heat 11 Fix the flow cell body to the heat exchanger. 1100 Series DAD and MWD Reference Manual...
Page 109 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 110: Replacing Capillaries On A Semi-Micro And High Pressure Flow Cell
Preparations for this procedure: • Turn off the Inlet flow. capillary • Remove the front cover. • Remove the flow cell, E ha gi g a Flo Cell on page 105. Outlet capillary 1100 Series DAD and MWD Reference Manual...
Page 111 When retightening the fittings, make sure that they carefully tightened (handtight plus turn with a wrench). Otherwise damage of the flow cell body blockage may result. Outlet capillary 1100 Series DAD and MWD Reference Manual...
Page 112 Wa ele gth Re ali atio Hol iu Perform a wavelength calibration, see on page 84 or holmium test, see O ide Test on page 86 to check the correct positioning of the flow cell. 1100 Series DAD and MWD Reference Manual...
Page 113: Nano Flow Cell - Replacing Or Cleaning
For details refer to the technical that comes with the nano-flow cell kit. NOTE NOTE The quartz block can be cleaned with alcohol. DO NOT touch the inlet and outlet windows at the quartz block. 1100 Series DAD and MWD Reference Manual...
Page 114 3 Unscrew the capillaries from the flow cell. DO NOT Using for press on the example use the adapter at this time! plastic part toothpick, and slide the quartz body out of the cell housing. 1100 Series DAD and MWD Reference Manual...
Page 115 9 Insert the flow cell capillaries and tighten them 10 Reassemble the flow cell body to the holder. fingertight. Use the wrench and torque adapter as described on page 126 and tighten the fittings alternately. 1100 Series DAD and MWD Reference Manual...
Page 116 (inlet) and waste assembly (outlet). NOTE With the instrument accessory kit comes a 4-mm wrench and with the Sealing Kit a special adapter. Both together work as a torque wrench with pre-defined torque (maximum allowed torque 1100 Series DAD and MWD Reference Manual...
Page 117 0.7 Nm). It can be used to tight the capillary fittings at the flow cell body. The wrench has to be plugged into the adapter as shown in Figure Figure 30 Wrench plus Torque Adapter 1100 Series DAD and MWD Reference Manual...
Page 118: Cleaning Or Exchanging The Holmium Oxide Filter
A pair of tweezers Parts required Holmium oxide filter 79880-22711 De la atio of Co fo it fo HOX Filte See also on page 310. NOTE If not already in this position, move the filter up. 1100 Series DAD and MWD Reference Manual...
Page 119 Repairing the Detector While re 1100 Series DAD and MWD Reference Manual...
Page 120 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 121 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 122 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 123 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 124: Correcting Leaks
4 Replace the front cover. Figure 31 Observing for Leaks Replacing Leak Handling System Parts When required If the parts are corroded or broken Tools required None Parts required Leak funnel 5061-3356 1100 Series DAD and MWD Reference Manual...
Page 125: Cleaning Or Replacing Coupling Lens Assembly
It may be replaced when light transmission is reduced and a lamp exchange or window cleaning does not improve the light throughput. Tools required Screwdriver POZI 1 PT3 hexagonal key 1.5 1100 Series DAD and MWD Reference Manual...
Page 126 Repairing the Detector mm A pointed pair of pliers Parts required Coupling lens assembly G1103-68001 Use the 1.5-mm hex key to loos atio this ure: • 1100 Series DAD and MWD Reference Manual...
Page 127 Repairing the Detector ecto use, hot. five utes unti cool off. • fron cove • 1100 Series DAD and MWD Reference Manual...
Page 128 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 129 Carefully slide the lens assembly to the right into the deuterium lamp area by pushing it from the tungsten lamp side with the he The assembly may be disassembled using a pair of pliers to remove the retainer ring. The lens may be cleaned or the complete assembly must be exchanged. 1100 Series DAD and MWD Reference Manual...
Page 130: Cleaning Or Replacing Cell Support Window
Screwdriver POZI 1 PT3 hexagonal key 1.5 mm Pointed pair of pliers Parts required Cell support window 79880-28111 Cell support window assembly G1315-65202 Cell Suppo t Asse For others., see on page 200 1100 Series DAD and MWD Reference Manual...
Page 131 Insert the rebuilt or new lens assembly and slide it into its holder. Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 132 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 133: Exchanging Internal Parts
Always ensure the detector is disconnected from the line power when the main cover is removed. The security lever at the power input socket prevents that the detector cover is taken off when line power is still connected. 1100 Series DAD and MWD Reference Manual...
Page 134 With the introduction of the G1315B/G1365B DAD/MWD some of the metal plates look NOTE different (no air openings) compared to the G1315A/G1365A DAD/MWD. The figures have changed for specific repairs only. 1100 Series DAD and MWD Reference Manual...
Page 135: Removing The Top Cover And Foam
Disconnect capillaries. • Remove detector from stack and place it on the working bench. Install the ESD strap. If installed, unscrew and interface board. Place the board on the ESD kit. remove the 1100 Series DAD and MWD Reference Manual...
Page 136 Repairing the Detector plate towards the ide it towards the rear. Lift the cover up and sl 1100 Series DAD and MWD Reference Manual...
Page 137: Exchanging The Detector Main Board
Screwdriver POZI 1 PT3 Hexagonal wrenches 5 mm, 7 mm and 15 mm Parts required Detector main board (DAM) G1315-69540 (exchange assembly) for G1315A/B Detector main board (MWM) G1365-69540 (exchange assembly) for G1365A/B 1100 Series DAD and MWD Reference Manual...
Page 138 5 Use a 5-mm and 7-mm wrench to unscrew the REMOTE and the GPIB connector and a 15-mm wrench to unscrew the nuts of the ANALOG connectors. 6 Disconnect all connectors from the detector main board. When removing connectors, counter-hold with one hand on connector J13. NOTE 1100 Series DAD and MWD Reference Manual...
Page 139 10 Install the new detector main board and reconnect the connectors. Assure that the board is fitted correctly into the board recess in the rear panel. 1100 Series DAD and MWD Reference Manual...
Page 140: Entering The Serial Number Using The Control Module
In this case, the module can no longer be recognized by either the control module or the Agilent ChemStation. The main board must then be replaced. 6 Turn the detector off, then on again. The Records screen should display the correct serial number for this module. 1100 Series DAD and MWD Reference Manual...
Page 141: Entering The Serial Number Using The Agilent Chemstation
The reply line will give the module serial number. Exchanging the Fan (G1315A/G1365A) Use this procedure for the the G1315A/G1365A only. For G1315B/G1365B detectors refer NOTE Repla i g Fa Pa ts G on page 150. 1100 Series DAD and MWD Reference Manual...
Page 142 The figure below shows the required air flow see arrow on the fan) to ensure optimum cooling direction. and operation of the detect or. The direction of air flow is from the front towards the rear. AIRFLOW G1315/65A G1315/65B 1100 Series DAD and MWD Reference Manual...
Page 143: Replacing Fan Parts (G1315B/G1365B)
If the fan is defective or noisy, if the temperature sensor or the heater fails Tools required Screwdriver POZI 1 PT3, a pair of pliers Parts required Fan assembly 3160-1016, Temperature sensor assembly G1315-60000, Heater assembly G1315-60003 1100 Series DAD and MWD Reference Manual...
Page 144 Remove detector from stack and place it on the working bench. • Remove front cover, top cover and top foam Re o i g the Top Co e a d Foa section, see on page 140. 1100 Series DAD and MWD Reference Manual...
Page 145 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 146 Repairing the Detector The figure below shows the required air flow 8 Insert the fan assembly into its location. direction. AIRFLOW G1315/65A G1315/65B 1100 Series DAD and MWD Reference Manual...
Page 147: Removing The Optical Unit (G1315A/G1365A)
Re o i g the Opti al U it G on page 156. When required For all repairs inside the optical unit Tools required Screwdriver POZI 1 PT3 Parts required Optical unit G1315-69002 (exchange assembly) Individual parts depending on the following procedures 1100 Series DAD and MWD Reference Manual...
Page 148 102 (G1315A/G1365A only!). “Exchanging a Flow Cell” 6 Remove flow cell, see on page 105. “Cleaning or Exchanging the Holmium Oxide Filter” 7 Remove flow cell cover, see page 127 (G1315A/G1365A only!). 1100 Series DAD and MWD Reference Manual...
Page 149: Removing The Optical Unit (G1315B/G1365B)
Removing the Optical Unit (G1315B/G1365B) When required For all repairs inside the optical unit NOTE Tools required Screwdriver POZI 1 PT3 Parts required Optical unit G1315-69002 (exchange assembly) Individual parts depending on the following procedures 1100 Series DAD and MWD Reference Manual...
Page 150 Remove detector from stack and place it on working bench. • Remove front cover, top cover and top foam Re o i g the Top Co e a d Foa section, see on page 140. 1100 Series DAD and MWD Reference Manual...
Page 151: Exchanging The Source Lens (Achromat) Assembly
Tools required Screwdriver POZI 1 PT3 hexagonal key 1.5 mm A pointed pair of pliers Parts required Source lens (achromat) assembly G1315-65201(includes filter lever G1315-45001) 1100 Series DAD and MWD Reference Manual...
Page 152 Co e a d Foa on page 140. • Remove the optical unit, see Re o i g the Optical Unit on page 154 or Re o i g the Optical Unit on page 156. 1100 Series DAD and MWD Reference Manual...
Page 153 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 154 Repairing the Detector 8 Re 11 Replace the achromat assem spri ctro der. 9 Cle (wit 1100 Series DAD and MWD Reference Manual...
Page 155 Repairing the Detector lint- free clot repl ctro clean achro matic lens with liquid . To clean only. 10 Rep lace into tigh lens 1100 Series DAD and MWD Reference Manual...
Page 156 Repairing the Detector 12 Before installing the filter motor, press the filter lever in from the other side. 1100 Series DAD and MWD Reference Manual...
Page 157 Re o i g on page 171 or the Opti al U it G on page 156. • E ha gi g a Flo Cell Reinstall the flow cell, see on page 105. 1100 Series DAD and MWD Reference Manual...
Page 158: Replacing The Holmium Oxide Filter Motor
Turn off the lamp. • Switch off the detector, and disconnect the power cable. • Remove detector from stack and place it on working bench. • Remove front cover, top cover and top foam 1100 Series DAD and MWD Reference Manual...
Page 159 Co e a d Foa on page 140. • Remove optical unit, see Re o i g the Optical Unit on page 154 or Re o i g the Optical Unit on page 156. 1100 Series DAD and MWD Reference Manual...
Page 160 Repairing the Detector 4 While counter-holding the filter lever, press the filter motor onto the filter shaft until it clicks into the final position. 1100 Series DAD and MWD Reference Manual...
Page 161: Exchanging The Power Supply
“Replacing Fan Parts (G1315B/G1365B)” 148 or on page 150. “Removing the Optical Unit (G1315A/G1365A)” 7 Remove the optical unit, see “Removing the Optical Unit (G1315B/G1365B)” page 154 or on page 156. 1100 Series DAD and MWD Reference Manual...
Page 162 7 Press down the power switch light pipe to remove it from the coupler. Power switch light pipe Coupler The repair level of the power supply assembly is exchange of the complete assembly. No serviceable parts inside. 1100 Series DAD and MWD Reference Manual...
Page 163 Repairing the Detector 11 Reinstall bottom foam part. Slide it in underneath Next step the leak drain. • Reinsta proces the Det Boa d 143. • Reinsta assemb E ha on pag Repla Parts 1100 Series DAD and MWD Reference Manual...
Page 164: Exchanging The Leak Sensor
Exchanging the Leak Sensor When requiredIf defective Tools required Screwdriver POZI 1 PT3 Parts required Leak sensor assembly 5061-3356 WARNING Do not switch on the detector when the cover is removed. 1100 Series DAD and MWD Reference Manual...
Page 165 On the G1315B DAD and G1365B MWD the leak sensor can be pulled out without the NOTE removing the leak pan (the next steps describe the procedure for the G1315A/G1365A). 12 Remove the leak pan from the cabinet bottom. 1100 Series DAD and MWD Reference Manual...
Page 166 Repairing the Detector 14 Replace the leak sensor assembly into the leak pan. 15 R 1100 Series DAD and MWD Reference Manual...
Page 167 Repairing the Detector 16 Replace the leak pan into the cabinet bottom. 1100 Series DAD and MWD Reference Manual...
Page 168: Replacing Status Light Pipe
When required When repairs have been completed Tools required Screwdriver POZI 1 PT3 Use this procedure for the the G1315A/G1365A only. For G1315B/G1365B detectors refer NOTE I stalli g the Opti al U it G on page 173 1100 Series DAD and MWD Reference Manual...
Page 169 E ha gi g the Fa G detector, see on page 148. CAUTION Preparations Check that the shock abso for this procedure: • The power supply, the fan and the processor board are already installed. 1100 Series DAD and MWD Reference Manual...
Page 170 Repairing the Detector 4 Replace the two rubber shock absorbers and reconnect the ground connector. 1100 Series DAD and MWD Reference Manual...
Page 171: Installing The Optical Unit (G1315B/G1365B)
Installing the Optical Unit (G1315B/G1365B) When required When repairs have been completed 1100 Series DAD and MWD Reference Manual...
Page 172 Repla i g Fa Pa ts G operation of the detector, see on page 150. Preparations Check that the shock abso for this procedure: • The power supply, the fan and the processor board are already installed. NOTE 1100 Series DAD and MWD Reference Manual...
Page 173: Replacing The Foam And The Top Cover
Replacing the Foam and the Top Cover When required When all repairs have been completed 1100 Series DAD and MWD Reference Manual...
Page 174 Repairing the Detector Tools required Screwdriver POZI 1 PT3 Prerequisites The detector is open and other procedures have been carried out 1100 Series DAD and MWD Reference Manual...
Page 175 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 176 Repairing the Detector 1100 Series DAD and MWD Reference Manual...
Page 177: Assembling The Main Cover
In case you insert the left or right side in the opposite position, you may not be able to remove the side from the top part. 3 Replace the detector into the stack and reconnect the cables and capillaries. 4 Turn on the detector. 1100 Series DAD and MWD Reference Manual...
Page 178: Replacing The Interface Board
Interface board (BCD) G1351-68701 with external BCD Boa d contacts and BCD outputs, see on page 253 LAN Co u i atio Interface board (LAN) see I te fa e Boa d on page 255. Tools required None 1100 Series DAD and MWD Reference Manual...
Page 179: Repla I G The Dete To 'S Fi A E
3 If detector main board was replaced, reenter the serial number information of the “Entering the Serial Number using the module through the user interface, see Control Module” “Entering the Serial Number using the Agilent on page 146 or ChemStation” on page 147. 1100 Series DAD and MWD Reference Manual...
Page 180: Identifying Parts And Materials
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Identifying Parts and Materials Overview of Main Assemblies Optical Unit Assembly Standard Flow Cell Semi-Micro Flow Cell High Pressure Flow Cell Nano Flow Cells Fan Assembly Parts Holmium Oxide Filter...
Page 181: Overview Of Main Assemblies
Identifying Parts and Materials Agilent Technologies Overview of Main Assemblies Figure 35 Overview of Main Assemblies Table 8 Main Assemblies Item Description Part Number Main board DAM for G1315A/B DAD (exchange assembly) G1315-69540 1100 Series DAD and MWD Reference Manual...
Page 182 Hexagonal nut for RS-232C connector 1251-7788 Nut for analog connector 2940-0256 Washer for analog connector 2190-0699 Cable CAN to Agilent 1100 Series modules 5181-1516 Power supply, for power and status light parts see page 206 0950-2528 Interface board BCD (BCD/external contacts)
Page 183: Optical Unit Assembly
Screws M3 for flow cell door (6 ×) 5022-2112 Plug hole for lamp housing 6960-0002 Holmium oxide filter parts, see page 197 Spring, for other holmium oxide filter parts, see page 197 1460-1510 1100 Series DAD and MWD Reference Manual...
Page 184 198 G1103-68001 Source lens (achromat) assembly, for other source lens assembly parts, see page 199 G1315-65201 Cell support assembly, for other cell support assembly parts, see page 200 G1315-65202 Sealing for G1315B/G1365B G1315-47103 1100 Series DAD and MWD Reference Manual...
Page 185: Standard Flow Cell
Identifying Parts and Materials Standard Flow Cell Table 10 Standard Flow Cell Parts 1100 Series DAD and MWD Reference Manual...
Page 186 Seal kit FRONT for STD flow cell, qty=12 of item 7 G1315-68710 Window screw kit, includes 2 quartz windows, 2 compression 79883-68703 washers, 2 window holders, 2 window screws and 10 spring washers NOTE Gaskets # 6 and #7 have different hole diameters. 1100 Series DAD and MWD Reference Manual...
Page 187: Semi-Micro Flow Cell
2 - spring washers 3 - compression washer 4 - window holder 5 - quartz window 6 - Gasket Figure 38 Orientation of Spring Washers. Semi-Micro Flow Cell Table 11 Semi-Micro Flow Cell Parts 1100 Series DAD and MWD Reference Manual...
Page 188 Seal kit FRONT for semi-micro flow cell, qty=12 of item 7 G1315-68710 Window screw kit, includes 2 quartz windows, 2 compression 79883-68703 washers, 2 window holders, 2 window screws and 10 spring washers NOTE 1100 Series DAD and MWD Reference Manual...
Page 189 Gaskets # 6 and #7 have different hole diameters. 1 - window screw 2 - spring washers 3 - compression washer 4 - window holder 5 - quartz window 6 - Gasket Figure 40 Orientation of Spring Washers. 1100 Series DAD and MWD Reference Manual...
Page 190: High Pressure Flow Cell
Screw M 2.5, 4 mm lg for cell body/clamp unit 0515-1056 Capillary (0.12 mm, 150 mm lg) G1315-87312 Capillary (0.17 mm, 380 mm lg) G1315-87311 Cell Repair Kit Agilent, includes 1 quartz window, 79883-68700 5 spring washers, 2 seal rings 1100 Series DAD and MWD Reference Manual...
Page 191: Nano Flow Cells
Identifying Parts and Materials Nano Flow Cells The following kits are available: Table 13 Nano-flow cell kits Description Part number 1100 Series DAD and MWD Reference Manual...
Page 192 Fitting Screw (for 4 mm wrench), QTY=2 (reorder 10/pk) 5063-6593 Cell ferrules are factory installed PEEK fitting 1/32" (not attached to capillaries), (reorder 10/pk) 5065-4422 Litetouch ferrules LT-100, (1/32" Ferrule and SS lock ring), QTY=2 (reorder 10/pk) 5063-6592 1100 Series DAD and MWD Reference Manual...
Page 193 Fitting FT (#5) PEEK coated fused silica capillary Outlet (50 µm), G1315-87328 alternative, includes Outlet capillary, 120 mm long, 50 µm i.d. with pre-fixed ferrules (#4) and fitting (#3), plus one PEEK Fitting FT (#5) 1100 Series DAD and MWD Reference Manual...
Page 194 Fitting FT (#5) PEEK coated fused silica capillary Outlet (25 µm) G1315-87318 alternative, includes Outlet capillary, 600 mm long, 25 µm i.d. with pre-fixed ferrules (#4) and fitting (#3), plus one PEEK Fitting FT (#5) 1100 Series DAD and MWD Reference Manual...
Page 195: Fan Assembly Parts
Item Description Part Number Fan (for all DAD/MWDs) 3160-1016 Heater assembly (G1315/65B only) G1315-60000 Temperature sensor assembly (G1315/65B only) G1315-60003 Sensor holder (G1315/65B only) G1315-22300 Figure 43 Fan Assembly Parts Holmium Oxide Filter 1100 Series DAD and MWD Reference Manual...
Page 196 Holmium oxide filter 79880-22711 Spring 1460-1510 When the filter motor has been removed, the filter lever should not be reused. Use always a new filter lever to assure correct fit on the filter motor shaft. 1100 Series DAD and MWD Reference Manual...
Page 197: Coupling Lens Assembly
Table 19 Coupling Lens Assembly Item Description Part Number Coupling lens assembly G1103-68001 Retainer ring Washer-spring wavy Lens support Lens Lens holder Figure 45 Coupling Lens Assembly Parts Source Lens (Achromat) Assembly Table 20 Source Lens Assembly 1100 Series DAD and MWD Reference Manual...
Page 198: Cell Support Assembly
When the filter motor has been removed, the filter lever should not be reused. Use always a new filter lever to assure correct fit on the filter motor shaft. NOTE Figure 46 Source Lens (Achromat) Assembly Parts Cell Support Assembly Table 21 Cell Support Assembly 1100 Series DAD and MWD Reference Manual...
Page 199: Control Module
Table 22 Cotrol Module Parts Item Description Part Number Control Module, replacement part including cable G1323-67001 Plastic Housing Kit, includes front, back and a clamp 5062-8583 CAN cable Agilent 1100 module to control module G1323-81600 1100 Series DAD and MWD Reference Manual...
Page 200: Sheet Metal Kit (G1315A/G1365A)
Sheet metal kit includes case and top cover G1315-68701 Screws M3 for cover and flow cell door 5022-2112 Thumb screw for union holder 0515-2769 Zero dead volume fitting 0100-0900 Union holder clamp G1315-05205 1100 Series DAD and MWD Reference Manual...
Page 201: Sheet Metal Kit (G1315B/G1365B)
Sheet metal kit includes case, top cover and front G1315-68721 Screws M3 for cover and flow cell door 5022-2112 Thumb screw for union holder 0515-2769 Zero dead volume fitting 0100-0900 Union holder clamp G1315-05205 1100 Series DAD and MWD Reference Manual...
Page 202: Plastic Parts
Figure 50 Sheet Metal Kit Parts (G1315B/G1365B) Plastic Parts Table 25 Plastics Parts NOTE Item Description Part Number Front cover 5062-8582 Plastics, includes base, sides and top 5062-8565 Name plate Agilent 1100 Series 5042-1381 1100 Series DAD and MWD Reference Manual...
Page 203: Foam Parts
1, 2 EPP foam kit, includes base and top G1315-68722 Damper kit (includes 7 bumpers) G1315-68706 Guides for interface board 5041-8395 Do not order the individual part numbers mentioned on the NOTE foam. 1100 Series DAD and MWD Reference Manual...
Page 204: Power And Status Light Pipes
Item Description Part Number Power supply assembly 0950-2528 Screw M4 x 0.7, 8 mm lg, to fix power supply at rear panel 0515-0910 Washer 2190-0409 Power light pipe 5041-8382 Status light pipe 5041-8384 1100 Series DAD and MWD Reference Manual...
Page 205: Leak Parts
Leak sensor assembly 5061-3356 Leak pan G1315-45501 Leak funnel 5041-8388 Leak funnel holder 5041-8389 Clip 5041-8387 Corrugated tubing, 120 mm lg, re-order 5 m 5062-2463 Corrugated tubing, 120 mm lg, re-order 5 m 5062-2463 1100 Series DAD and MWD Reference Manual...
Page 206: Accessory Kit
5 m Fitting male PEEK, Qty=1 0100-1516 Capillary column – detector 380 mm lg, 0.17 i.d. includes G1315-87311 items 4 , 5 and 6 (not assembled ) Ferrule front SST, qty=2 0100-0043 1100 Series DAD and MWD Reference Manual...
Page 207 Wrench open end 4 mm 8710-1534 ESD wrist strap 9300-1408 For item number refer to Figure 55 Figure Figure 55 Waste Tubing Parts This end is pre-installed Figure 56 Inlet Capillary (Column-Detector) Parts 1100 Series DAD and MWD Reference Manual...
Page 208: Cable Overview
03394-60600 3396 Series II / 3395A integrator, see page 217 3396 Series III / 3395B integrator 03396-61010 Agilent 1100 / 1050 modules / 1046A FLD 5061-3378 1046A FLD 5061-3378 35900A A/D converter 5061-3378 1100 Series DAD and MWD Reference Manual...
Page 209 Cross-over network cable (shielded, 3 5023-0203 m long), ( for point to point cable connection ) Twisted pair network cable (shielded, 5023-0202 7 m long) ( for hub connections ) 1100 Series DAD and MWD Reference Manual...
Page 210: Analog Cables
Connected to pin 6 Shield Analog - Connected to pin 4 Not connected Agilent 1100 to 3394/6 Integrators Connector Signal Name 35900-60750 3394/6 Agilent 1100 Not connected Shield Analog - Center Analog + 1100 Series DAD and MWD Reference Manual...
Page 211 Connector Signal Name 8120-1840 Agilent 1100 Shield Shield Analog - Center Center Analog + Agilent 1100 to General Purpose Connector Signal Name 01046-60105 3394/6 Agilent 1100 Not connected Black Analog - Analog + 1100 Series DAD and MWD Reference Manual...
Page 212 Identifying Parts and Materials 1100 Series DAD and MWD Reference Manual...
Page 213: Remote Cables
Remote Cables One end of these cables provides a Aligent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent 1100 Series modules. The other end depends on the instrument to be connected to. Agilent 1100 to 3390 Integrators...
Page 214 5,14 7 - Red Ready High 8 - Green Stop 1 13, 9 - Black Start request connected START and STOP are connected via diodes to pin 3 of the 3394 connector. NOTE 1100 Series DAD and MWD Reference Manual...
Page 215 Agilent 1100 to 3396 Series III / 3395B Integrators Connector Signal Name Active 03396-61010 33XX Agilent 1100 ( TTL ) 1 - White Digital ground 2 - Brown Prepare run 3 - Gray Start 4 - Blue Shut down 1100 Series DAD and MWD Reference Manual...
Page 216 9 - Black 9 - Black Start request Agilent 1100 to HP 1090 LC or Signal Distribution Module Connector Signal Name Active 01046-60202 HP 1090 Agilent 1100 ( TTL ) 1 - White Digital ground 1100 Series DAD and MWD Reference Manual...
Page 217 3 - Gray Start 4 - Blue Shut down 5 - Pink Not connected 6 - Yellow Power on High 7 - Red Ready High 8 - Green Stop 9 - Black Start request 1100 Series DAD and MWD Reference Manual...
Page 218: Bcd Cables
Identifying Parts and Materials BCD Cables One end of these cables provides a 15-pin BCD connector to be connected to the Agilent 1100 Series modules. The other end depends on the instrument to be connected Agilent 1100 to General Purpose Connector...
Page 219 Agilent 1100 to 3396 Integrators Connector Signal Name Digit 03396-60560 3392/3 Agilent 1100 BCD 5 BCD 7 BCD 6 BCD 4 BCD0 BCD 3 BCD 2 BCD 1 Digital ground + 5 V 1100 Series DAD and MWD Reference Manual...
Page 220: Auxiliary Cable
DC + 5 V IN Pink Vent CAN Cable Both ends of this cable provide a modular plug to be connected to Agilent 1100 Series module’s CAN-bus connectors. Agilent 1100 module to module, 0.5 m 5181-1516 Agilent 1100 module to module, 1 m...
Page 221: External Contact Cable
Identifying Parts and Materials External Contact Cable One end of this cable provides a 15-pin plug to be connected to Agilent 1100 Series module’s interface board. The other end is for general purpose. Agilent 1100 Series Interface Board to general purposes...
Page 222: Lan Cables
Part number Cross-over network cable (shielded, 3 m long), 5023- 0203 ( for point to point connection ) Twisted pair network cable (shielded, 7 m long) ( 5023- for hub connections ) 0202 1100 Series DAD and MWD Reference Manual...
Page 223: Introduction To The Detector
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Introduction to the Detector Introduction to the Detector Optical System Overview Electrical Connections Instrument Layout Early Maintenance Feedback (EMF) Electronics Detector Main Board (DAM/MWM) Firmware Description Raw Data Conversion to Absorbance...
Page 224: Introduction To The Detector
Each cell room and lamp are separated by a quartz window which can be cleaned or replaced. In the spectrograph, light is being dispersed onto the diode array by a holographic grating. This allows simultaneous access to all wavelength information 1100 Series DAD and MWD Reference Manual...
Page 225 The flow cell can be removed to check the optical and electronic performance of the detector without having influences from the flow cell. 1100 Series DAD and MWD Reference Manual...
Page 226 Diode Array The diode array is a series of 1024 individual photodiodes and control circuits located on a ceramic carrier. With a wavelength range from 190 – 950 nm the sampling interval is < 1 nm. 1100 Series DAD and MWD Reference Manual...
Page 227: Connections
262) which is recognized once after power is switched on. • The CAN bus is a serial bus with high speed data transfer. The two connectors for the CAN bus are used for internal Agilent 1100 Series module data transfer and synchronization.
Page 228: Instrument Layout
• the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. 1100 Series DAD and MWD Reference Manual...
Page 229: Early Maintenance Feedback (Emf)
(or values slightly less than the displayed values) as EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. 1100 Series DAD and MWD Reference Manual...
Page 230: Electronics
The electronics are comprised of four main components: • detector main board (DAM/MWM), see page 238. • power supply, see page 266. Optional: • interface board (BCD/external contacts), see page 253. • interface board (LAN), see page 255. 1100 Series DAD and MWD Reference Manual...
Page 231: Detector Main Board (Dam/Mwm)
Conversion and subsequent calculation to achieve absorbance values include the following tasks: • dark current correction, • PDA (photo diode array) temperature compensation, • absorbance calculation, and • signal averaging. SIMM Memory Module 1100 Series DAD and MWD Reference Manual...
Page 232 On-board Battery An on-board lithium battery buffers the electronic memory when the module is turned off. “Lithium Batteries Information” For safety information on lithium batteries see on page 303. 1100 Series DAD and MWD Reference Manual...
Page 233 PDA and detector main board. In addition, wavelength calibration data and manufacturing data from the manufacturing process (for example, serial number, dates, and so on) are stored in the EEPROM. 1100 Series DAD and MWD Reference Manual...
Page 234 (PWM). The PWM signal is then fed to an amplitude modulator, which precisely turns the reference signal on and off. This signal then passes to a low-pass filter section. 1100 Series DAD and MWD Reference Manual...
Page 235 600 VDC for the lamp, resulting in lamp ignition. After ignition this voltage is disabled. The other part is a constant current source of 320 mA at an operating voltage of about 85 VDC for stable operating conditions and light emission of 1100 Series DAD and MWD Reference Manual...
Page 236 The tungsten lamp voltage is generated by the tungsten lamp voltage control circuit which is enabled by the processor. This circuit provides a constant voltage of 6 VDC to operate the tungsten lamp. 1100 Series DAD and MWD Reference Manual...
Page 237 The digital values are transferred via the control bus on the detector main board. When values are outside the normal range, an appropriate error message is generated and the lamps will be switched off. 1100 Series DAD and MWD Reference Manual...
Page 238: Firmware Description
• a non-instrument specific section, called resident system, • an instrument specific section, called main system. Resident System This resident section of the firmware is identical for all Agilent 1100 series modules. Its properties are: • the complete communication capabilities (GPIB, CAN and RS-232C), • memory management, •...
Page 239: Firmware Updates
104 is revision 1.04 For instructions refer to your user interface. NOTE Update of main system can be done in the resident system only. Update of the resident system can be done in the main system only. 1100 Series DAD and MWD Reference Manual...
Page 240: Raw Data Conversion To Absorbance
These gain values are stored in a table. They are used to adjust the amplification factor in the signal conditioning electronics. This process is used to adjust small signal levels to the optimum range of the A/D converter. 1100 Series DAD and MWD Reference Manual...
Page 241 The quantum efficiency of the photodiode array depends on the temperature and is different for each wavelength. The temperature dependency follows a monotone increasing function over the wavelength scale, which means it increases with longer wavelengths (above 600 nm). 1100 Series DAD and MWD Reference Manual...
Page 242 EEPROM (electrically erasable PROM), which is part of the spectrograph electronics. Actually two sets of coefficients are used, one set for the wavelength range below the second order filter, located on the photodiode array, and one set for the upper 1100 Series DAD and MWD Reference Manual...
Page 243: Rawdata File
Spectra Acquisition Modes (DAD only) The spectra acquisition mode allows automatic storage of spectra during a run. The mode can be changed during the run by time-programming. The modes in detail are: Table 32 Spectra Acquisition Modes 1100 Series DAD and MWD Reference Manual...
Page 244: Optional Interface Boards
2nd spectra is stored (50 % of mode all). Optional Interface Boards The Agilent 1100 Series modules have one optional board slot that allows addition of an interface board to the modules. Table 33 Optional Interface Boards...
Page 245 220 and the external outputs, see page 224 to external devices. Table 34 Detailed connector layout (1100) Signal name BCD digit BCD 5 BCD 7 BCD 6 BCD 4 BCD 0 BCD 3 BCD 2 1100 Series DAD and MWD Reference Manual...
Page 246: Lan Communication Interface Board
ChemStation software revision A.06.01 or above. The following cards can be used with the Agilent 1100 modules. Table 35 LAN Boards Type Vendor Supported networks G1369A Agilent Fast Ethernet, Ethernet/802.3, RJ-45 (10/100Base-TX) Technologies recommended for re-ordering G1369- 60001 1100 Series DAD and MWD Reference Manual...
Page 247: Interfaces
) Twisted pair network cable (shielded, 7 m long) 5023-0202 ( for hub connections ) Interfaces The Agilent 1100 Series modules provide the following interfaces : Table 36 Agilent 1100 Series Interfaces Interface Type Pumps Autosampler...
Page 248: Analog Signal Output
Interface board The vacuum degasser will have a special connector for specific use. For details see description of main board. • CAN connectors as interface to other Agilent 1100 Series modules, • GPIB connector as interface to the Agilent ChemStation, •...
Page 249: Can Interface
• standard TTL levels (0 V is logic true, + 5 V is false), • fan-out is 10, • input load is 2.2 kOhm against + 5 V, and • outputs are open collector type, inputs/outputs (wired-or technique). Table 38 Remote Signal Distribution Signal Description 1100 Series DAD and MWD Reference Manual...
Page 250: Rs-232C
GPIB connector. The RS-232C is designed as DCE (Data Communication Equipment) with a 9- pin male SUB-D type connector. The pins are defined as follows : Table 39 RS-232C Connection Table Direction Function 1100 Series DAD and MWD Reference Manual...
Page 251 Introduction to the Detector Ground Instrument Male Female Female Male Figure 65 RS-232 Cable 1100 Series DAD and MWD Reference Manual...
Page 252: Setting The 8-Bit Configuration Switch
In the non-volatile memory, the parameters are kept, regardless of whether you turn the instrument off and on again. They will be kept until the same set of parameters is 1100 Series DAD and MWD Reference Manual...
Page 253: Gpib Default Addresses
Switches 1 in down and 2 in up position define that the RS-232C parameters will be changed. Once the change has been completed, the instrument must be powered up again in order to store the values in the non-volatile memory. Table 42 Communication Settings for RS-232C Communication 1100 Series DAD and MWD Reference Manual...
Page 254 No Parity Odd Parity Even Parity One start bit and one stop bit are always used (not selectable). Per default, the module will turn into 19200 baud, 8 data bit with no parity. 1100 Series DAD and MWD Reference Manual...
Page 255: Settings
Table 47 Stay Resident Settings Mode Select 1 TEST/BOOT To return to normal operation, set switches back to your GPIB or RS-232C configuration settings. 1100 Series DAD and MWD Reference Manual...
Page 256: The Main Power Supply Assembly
No accessible hardware fuse is needed because the main power supply is safe against any short circuits or overload conditions on the output lines. When overload conditions occur, the power supply turns off all output voltages. Turning the line power off and on 1100 Series DAD and MWD Reference Manual...
Page 257 Output 1 + 24 V / 4.5 A (maximum) total power consumption of + 24 V and + 36 V must not exceed 107 W. Output 2 + 36 V / 2.5 A (maximum) 1100 Series DAD and MWD Reference Manual...
Page 258 Introduction to the Detector Output 3 + 5 V / 3 A Output 4 + 15 V / 0.3 A Output 5 - 15 V / 0.3 A 1100 Series DAD and MWD Reference Manual...
Page 259: Control Module Screens For Agilent 1100 Dad And Mwd
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Control Module Screens for Agilent 1100 DAD and MWD Major keys on the Agilent 1100 Control Module Control Module - Unsupported Module Screens available from the Analysis screen Screens available from the System screen...
Page 260: Major Keys On The Agilent 1100 Control Module
CAN bus, unplug the control module from the LC module and reconnect. 1100 Series DAD and MWD Reference Manual...
Page 261: Control Module - Unsupported Module
In case the control module shows the following screen and the yellow LED on the detector is not flashing, the used firmware in the Control Module is not able to control the G1315B DAD or G1365B MWD. These detectors require firmware revision B.01.04 or above (G1323B). 1100 Series DAD and MWD Reference Manual...
Page 262: Screens Available From The Analysis Screen
Agilent 1100 modules. Restart re-boots the control module. Lamp ON/OFF Use the F8 key (On/Off) to turn on the lamp(s). If more than one module is available, select the DAD or MWD from the pop-up menu. 1100 Series DAD and MWD Reference Manual...
Page 263 Maximum 4 modules are shown automatically. If more modules are in the system, you have to chose in Setup view. 1100 Series DAD and MWD Reference Manual...
Page 264 Use the m-key for the context sensitive menu. The Status command pulls up a monitor screen displaying signals and spectra as programmed. Reset will load the DAD or MWD default parameters. Balance brings the baseline back to set offset. 1100 Series DAD and MWD Reference Manual...
Page 265 Selecting More and Settings pull down menu you can enter special DAD or MWD setpoints. Selecting More and Signals C-E on the pull down menu you can enter additional DAD or MWD signal parameters. 1100 Series DAD and MWD Reference Manual...
Page 266 Press the F7 key (Insert) to add a timetable events. Use the F6 key (Done) to view the entered lines of the timetable. Use the m-key for the context sensitive menu. It gives you additional tools for the timetable. 1100 Series DAD and MWD Reference Manual...
Page 267 FOR G1365A/B MWD: You can change the settings for the spectrum acquisition “Sample, Holmium and Dark Current (STOP FLOW). The spectrum is started via Spectrum” on page 291. Settings - Run times 1100 Series DAD and MWD Reference Manual...
Page 268 Here you can observe the online signal(s). To add additional online signals (maximum 3), press F6 key (Select). If more than one signal is configured (see next), use the 1-2-3 number key to switch between the signals. 1100 Series DAD and MWD Reference Manual...
Page 269 PC-Card and Instrument window. Use the UP/Down arrows to select the method. Use the F7/F8 keys (Copy) to enter available signals into the box for selected signals or vice versa. 1100 Series DAD and MWD Reference Manual...
Page 270: Screens Available From The System Screen
Use the F1 key (Control) to select the FL-Detector. Here you receive information about the not-ready conditions if needed. F2 key (Reset) does a re-initialization of the DAD or MWD. System - Configuration 1100 Series DAD and MWD Reference Manual...
Page 271: Screens Available From The Records Screen
Use the Esc key to receive Views on the F5 key. Choose System from the pull-down menu. Use the F4 key (Records) to select the DAD or MWD. Errors are reported either into the System Log (F2) or Error Log (F3). 1100 Series DAD and MWD Reference Manual...
Page 272 Use the F1 key (EMF) to set EMF parameters. Choose menu item 1 (Setup limits) to select lamp-on level for the UV and Vis lamp at which you want to receive a warning. 1100 Series DAD and MWD Reference Manual...
Page 273 Use the Esc key to receive Views on the F5 key. Choose System from the pull-down menu. Use the F3 key (Records) to select the Generic module. In this screen the resident firmware revision is shown. 1100 Series DAD and MWD Reference Manual...
Page 274 In case the serial number of the module has to be added, use the m-key to open the menu Enter Serial#. Choose System from the pull-down menu. Use the F3 key (Records) to select the DAD or MWD. Use the F4 key (Maint log) to view and edit the maintenance logbook. 1100 Series DAD and MWD Reference Manual...
Page 275: Diagnostics And Tests
Tests screen Use the Esc key to receive Views on the F5 key. Choose System from the pull-down menu. Use the F3 key (Tests) to select the DAD or MWD. Several tests are available 1100 Series DAD and MWD Reference Manual...
Page 276 Wavelength Calibration Use the F1 key (Calibrate) and then F8 key (Execute) to start the DAD or MWD wavelength calibration (with water in the flow cell). If a deviation is found, press Adjust. 1100 Series DAD and MWD Reference Manual...
Page 277 To start the built-in test chromatogram, use the F8 key (Execute) to enable the simulation. Then press the m-key to open the pop-up menu. Select Start to start a run (all modules in the Agilent 1100 system must be in ready state ). 1100 Series DAD and MWD Reference Manual...
Page 278 The signal is also available on the analog output. A change of the peak width will change the retention times. Slit Test Use the F3 key (Slit Test) to test the movement of the electromechanical slit assembly. 1100 Series DAD and MWD Reference Manual...
Page 279 Control Module Screens for Agilent 1100 DAD and MWD 1100 Series DAD and MWD Reference Manual...
Page 280: Specifications
Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Specifications Performance Specifications 1100 Series DAD and MWD Reference Manual...
Page 281: Performance Specifications
Agilent Technologies Specifications Performance Specifications Table 50 Performance Specifications Agilent 1100 Series DAD and MWD Type Specification Comments Detection type 1024- element photodiode array Light source Deuterium and tungsten lamps 190 – 950 nm Wavelength range o page 9 Short term noise ±...
Page 282 500 nano: 0.5 µl volume, 10 mm cell path length and 50 bar (725 psi) pressure maximum Specifications Table 50 Performance Specifications Agilent 1100 Series DAD and MWD, continued Type Specification Comments Control and data Agilent ChemStation for LC...
Page 283 Reference conditions: cell path length 10 mm, response time 2 s, flow 1 ml/min LC- grade Methanol, slit width 4 nm. Linearity measured with caffeine at 265 nm. E i o For environmental conditions refer to on page 15. 1100 Series DAD and MWD Reference Manual 8 Specifications...
Page 284 Agilent 1100 Series Diode Array and Multiple Wavelength Detectors Reference Manual Safety Information General Safety Information Lithium Batteries Information Disposal of Mercury from Deuterium Lamp Radio Interference Sound Emission UV-Radiation Solvent Information Declaration of Conformity for HOX2 Filter Agilent Technologies on Internet...
Page 285 Agilent Technologies...
Page 286: A Safety Information
The operator of this instrument is advised that if the equipment is used in a manner CAUTION not specified in this manual, the protection provided by the equipment may be impaired. 1100 Series DAD and MWD Reference Manual...
Page 287 Safety Symbols Table 51 shows safety symbols used on the instrument and in the manuals. 1100 Series DAD and MWD Reference Manual...
Page 288 A caution alerts you to situations that could cause a possible loss of data. Do not CAUTION proceed beyond a caution until you have fully understood and met the indicated conditions. WARNING 1100 Series DAD and MWD Reference Manual...
Page 289: Lithium Batteries Information
Lithiumbatteri - Eksplosionsfare. Ved udskiftning benyttes kun batteri som anbefalt WARNING av apparatfabrikanten. Brukt batteri returneres appararleverandoren. Bij dit apparaat zijn batterijen geleverd. Wanneer deze leeg zijn, moet u ze niet NOTE weggooien maar inleveren als KCA. 1100 Series DAD and MWD Reference Manual...
Page 290: Disposal Of Mercury From Deuterium Lamp
Disposal of Mercury from Deuterium Lamp The long-life deuterium lamp (part number 5181-1528) includes a timer, which contains mercury. The timer has to be disposed of locally according to national waste disposal regulations. 1100 Series DAD and MWD Reference Manual...
Page 291: Radio Interference
If test and measurement equipment is operated with equipment unscreened cables and/or used for measurements on open set-ups, the user has to assure that under operating conditions the radio interference limits are still met within the premises. 1100 Series DAD and MWD Reference Manual...
Page 292: Sound Emission
This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB ( A ) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1100 Series DAD and MWD Reference Manual...
Page 293: Uv-Radiation
UV-Radiation Typical Values Position Effective Irradiance Lamp installed, 50 cm distance Average 0.016 µW/cm Lamp installed, 50 cm distance Maximum 0.14 µW/cm Solvent Information Observe the following recommendations on the use of solvents. Flow Cell 1100 Series DAD and MWD Reference Manual...
Page 294 For example, a 1-% solution of acetic acid in methanol will attack steel. • Solutions containing strong complexing agents (for example, EDTA, ethylene diamine tetra-acetic acid). • Mixtures of carbon tetrachloride with 2-propanol or THF. 1100 Series DAD and MWD Reference Manual...
Page 295: Declaration Of Conformity For Hox2 Filter
361.0 nm - 418.9 nm - 453.7 nm - 536.7 nm (spectral bandwidth: 2 nm ). Agilent Technologies guarantees the traceability of the specified absorbance maxima to a National Institute of Standards & Technology (NIST) holmium oxide solution standard with a lot-to-lot tolerance of ±0.3nm.
Page 296: Agilent Technologies On Internet
For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com Select “Products” - “Chemical Analysis” It will provide also the latest firmware of the Agilent 1100 series modules for download. 1100 Series DAD and MWD Reference Manual...
Page 297 Safety Information 1100 Series DAD and MWD Reference Manual...
Page 298: Index
APG remote, diode width, connecting CAN, disposal connecting GPIB, mercury, visible lamp current, visible connecting the ChemStation, lamp voltage, wavelength connecting the power, calibration failed, overview and identification, (electrostatic discharge) strap, exchanging. see repairs 1100 Series DAD and MWD Reference Manual...
Page 299 Identifying, information on uv- parts identification, 1100 Series DAD and MWD Reference Manual...
Page 300 Index spectra weight acquisition, acquisition dimensions, modes, acquisition power range, acquisition step considerations, simple repairs overview, threshold, power high pressure flow cell, buffer, consumption, standard/semi-micro flow cell, Index 1100 Series DAD and MWD Reference Manual...
Page 301 85, holmium oxide, 85, intensity, 85, overview, tests control module, threshold, troubleshooting error messages, 50, status indicators, unpacking, unsupported Module, using EMF, uv-radiation, variable entrance slit, wavelength accuracy and bunching, 1100 Series DAD and MWD Reference Manual...
Page 302 This manual contains technical reference information about Agilent 1100 Series diode array detectors. The manual describes the following: • installing the detector, • introduction to the diode array detector and its optimization, • diagnostics and troubleshooting, • repairing the detector, •...

Agilent Technologies 1100 Series Reference Manual

1 Installing the Detector

2 How to Optmize the Detector

3 Troubleshooting and Test Functions

4 Repairing the Detector

5 Identifying Parts and Materials

7 Control Module Screens for Agilent 1100 DAD and MWD

8 Specifications

Quick Links

Related Manuals for Agilent Technologies 1100 Series

Summary of Contents for Agilent Technologies 1100 Series