Teledyne 3060E Instruction Manual page 31

Ultra trace oxygen analyzer
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Installation
Installation
Installation
Installation
Installation
Prior to adding electrolyte to the Ultra Trace sensor, the electrolyte must be
purged with nitrogen (N
will reduce the time required to remove the dissolved O
by sparging it with N
purge the electrolyte:
1. Prepare the sensor electrolyte by following procedure MP-A56133
included in the Accessory Kit.
2. Open the cap of the electrolyte bottle.
3. Insert the fritted glass tube (P/N T1052) through the opening in the
bottle and bubble O
of the N
can be seen dispersing through the electrolyte.
Teflon/Nylon
4. Purge the electrolyte for about one hour.
NOTE: TET/AI recommends that the sensor be purged before adding
electrolyte. This is done by lowering a plastic/Teflon tube (clean
and free of any oil/grease and/or particulates) into the sensor
through the opening on the top of the stainless steel mounting plate
and flushing the sensor with O
sensor while flushing the sensor with O
eliminate the O
electrolyte. This procedure will substantially reduce the downtime
associated with clean-up at the first startup of the analyzer.
) to remove most of the dissolved oxygen (O
2
inside the sensor and hence, shorten the start-up time. To
2
-free N
2
should be adjusted so that a large number of small bubbles
2
tube
KOH
electrolyte
Nitrogen
bubbles
Figure 3-3. Electrolyte Bottle with Fritted Tube
from the sensor before the addition of prepurged
2
Teledyne Electronic Technologies
Analytical Instruments
Ultra
Ultra T T T T T race Oxyg
Ultra
race Oxyg
race Oxyg
Ultra
Ultra
race Oxyg
race Oxygen Anal
from the electrolyte
2
through the electrolyte. The flow rate
2
Nitrogen
Fritted tube
P/N T1052
Electrolyte
bottle
P/N BTL-P-32OZ
-free gas. Add electrolyte into the
2
-free gas. This will
2
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