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Teledyne 3060E Instruction Manual

Ultra trace oxygen analyzer
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Ultra Trace Sensor
M
U
LTRA
3060E
ODEL
T
O
RACE
XYGEN
I
NSTRUCTION
Teledyne Electronic Technologies
Analytical Instruments
A
NALYZER
M
ANUAL
Software Version 4.22
Edition: M59174-94-554
Model 3060E
P/N M59174
ECO# 96-385
May 24, 1996
i

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  • Page 1 Ultra Trace Sensor Model 3060E 3060E ODEL LTRA RACE XYGEN NALYZER NSTRUCTION ANUAL P/N M59174 Software Version 4.22 Edition: M59174-94-554 ECO# 96-385 May 24, 1996 Teledyne Electronic Technologies Analytical Instruments...
  • Page 2 This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by Teledyne or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.

  • Page 3: Table Of Contents

    Ultra Trace Sensor Model 3060E Table of Contents 1 Introduction Overview ......................1-1 Components ......................1-2 Main Features of the Analyzer ................1-2 Applications ......................1-4 2 Operational Theory Overview ......................2-1 Ultra Trace Sensor ....................2-3 Ultra Trace Sensor Components ..............2-3 Ultra Trace Sensor Operation ..............
  • Page 4 Model 3060E Ultra Trace Sensor Faradaic Calibrator ..................... 3-9 Adding Electrolyte to the Calibrator ............3-10 Adding Water to the Reservoir ..............3-14 Level Detector and Solenoid Switch ............3-15 Electrical Installation ................... 3-16 Electrical Connections .................. 3-16 Voltage Selection and Fuse Changing ............3-17 Gas Line Connections ..................
  • Page 5 Ultra Trace Sensor Model 3060E Zero Calibration ................... 4-33 Important Notes on Zero and Span Calibration ........4-37 Setup Mode: System Password ..............4-38 Setup: Alarms ..................4-40 Setup: Auto Settling ................4-42 Setup: Clock/Scheduled Span or Scheduled Zero ........ 4-47 Setup: More Options ................
  • Page 6 Model 3060E Ultra Trace Sensor Setting the Alarms ....................6-11 Auto Settling ......................6-12 Scheduled Zero and Scheduled Span ..............6-13 Filtering, Zero Display, Bypass and Reservoir ............ 6-14 Modem ......................... 6-15 Setup: Zero and Span Gas Source ............... 6-16 Negative Oxygen Display ..................

  • Page 7: Introduction

    3060E Ultra Trace Oxygen Analyzer is a highly sophisticated microprocessor- based instrument designed to measure the oxygen concentration in a gas mixture in a range as low as 0-50 parts per billion (PPB). The 3060E accurately measures and analyzes the oxygen content in inert gases such as helium, nitrogen and argon, and in flammable gases such as hydrogen and ethylene.

  • Page 8: Components

    Chapter 1 Chapter 1 Components The 3060E is designed to mount in a standard 19-inch rack. All of the operational controls are easily accessed through the well-marked front panel. Each of the following components is contained within the analyzer: •...
  • Page 9 11. Flow schematic display: This feature allows you to visually verify the exact status of each of the pneumatic valves in the sampling system. Teledyne Electronic Technologies 1–3 Analytical Instruments...

  • Page 10: Applications

    Ultra Trace sensor from the analyzer. 14. Remote capability: The 3060E can be remotely located and con- trolled from a microcomputer linked to the analyzer by a phone line. Software provided with the analyzer allows you to control analyzer functions through menus displayed on the computer.

  • Page 11: Operational Theory

    A temperature controller regulates the temperature of the Ultra Trace sensor to minimize the effects of ambient temperature variations during analysis. Figure 2-1 shows the locations of the major components of the analyzer. Teledyne Electronic Technologies Analytical Instruments...
  • Page 12 Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 Temperature Controller Figure 2-1. Main Components Teledyne Electronic Technologies Analytical Instruments...

  • Page 13: Ultra Trace Sensor

    PURGE GAS IN DETECTOR TOP STAINLESS CADMIUM ANODE STEEL PLATE ELECTROLYTE O-RING BAFFLE PLATE CATHODE SAMPLE IN ZERO GAS BUBBLES (OXYGEN-FREE) SAMPLE OUT CELL BODY SIDE STAINLESS STEEL PLATE CATHODE Figure 2-2. Ultra Trace Sensor Components Teledyne Electronic Technologies Analytical Instruments...

  • Page 14: Ultra Trace Sensor Operation

    Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 The sensing cathode used in the sensor is a high surface-area metal-catalyzed gas diffusion electrode, with a surface area of 150–180 m /g.

  • Page 15: Faradaic Calibrator

    Figure 2-3 illustrates major calibrator components. The calibrator is comprised of a top electrode assembly and a bottom mounting block containing a cup for electrolyte. An O-ring is used to make a leak-free seal between these two components. Teledyne Electronic Technologies Analytical Instruments...
  • Page 16 Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 The two platinum/gold wire electrodes are attached to a feed-through header, which is sealed to the stainless steel plate. The two electrodes are wrapped around a porous polyethylene rod.

  • Page 17: Faradaic Calibrator Operation

    To see why, assume the absolute error during calibration on any range is 2 PPB. If the analyzer is calibrated at 25 PPB, 2 PPB error constitutes an 8% error in calibration. However, if the analyzer is calibrated at 80 PPB the calibration error will be only 2.5%. Teledyne Electronic Technologies Analytical Instruments...

  • Page 18: Sample System

    Depending on the mode of operation (determined by which valves are open or closed), either a sample, span or zero gas is delivered. The 3060E sample system is designed and fabricated to insure that the O concentration of the gas is not altered (except in the O scrubber) as it travels through the sample system.
  • Page 19 The solenoid valves control the air flow to the air-activated bellows valves. The solenoid valves are controlled by the micro- processor. When de-energized, the valve outlet is open to ambient air, allowing the air-activated bellows valve to close. Teledyne Electronic Technologies Analytical Instruments...
  • Page 20 Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 • Oxygen Scrubber The O scrubber is used to remove O (down to less than 1 PPB, typically 0.5 PPB) from the sample gas. The scrubbed gas is used...

  • Page 21: Electronics

    A light emitting diode (LED) display and circuitry to actuate the valves in the sample are located outside the control module. Functional groups of analyzer electronics are: Signal Processing Temperature Control Valve Control Power Supply Teledyne Electronic Technologies 2-11 Analytical Instruments...

  • Page 22: Signal Processing Functions

    Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 Signal Processing Functions Analog signal processing is accomplished in two plug-in circuit cards operating under control of the microcomputer. One card processes analog input signals and the other processes analog output signals.
  • Page 23 16.8 Table 2-1. Range Identifier Current (I) Voltage (V) 20 mA - 1/4 Full Scale Value (0,0) (0,0) - 1/4 Full Full Full Scale Scale -0.25 Scale Value Figure 2-5. Analog Signal Output Offset Teledyne Electronic Technologies 2-13 Analytical Instruments...

  • Page 24: Digital Circuit Board

    Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 Digital Circuit Board The digital PCB is a general purpose microcomputer used to control all functions of the analyzer. The analog input PCB and the analog output PCB plug directly into connectors located on the digital PCB.

  • Page 25: Temperature Controller

    The analyzer power supply module is a replaceable assembly containing four power supplies and five alarm relays. Electronic circuitry used to drive and interface the alarm relays to the output of the microcomputer is also located inside this module. Teledyne Electronic Technologies 2-15 Analytical Instruments...
  • Page 26 Model 3060E Model 3060E Model 3060E Chapter 2 Chapter 2 Chapter 2 Model 3060E Model 3060E Chapter 2 Chapter 2 Teledyne Electronic Technologies 2-16 Analytical Instruments...

  • Page 27: Installation

    Remove the packing slip and verify that you have received all of the correct materials. Packing list: 1. Model 3060E Ultra Trace Oxygen Analyzer 2. 3060E Accessory Kit (P/N A59582) The analyzer is shipped with all the materials and special items you need to install and prepare the system for operation.

  • Page 28: Cautions And Warnings

    Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 2. Standard accessory kit for the 3060E (P/N A59582): Description G284 Gaskets, VCR-type G352 Weld glands, male, VCR-type N284 Nuts, female Wrench, open end, ¼ " - "...

  • Page 29: Ultra Trace Sensor Installation

    (see Figure 3-1). Leave all eight bolts loose until Step 3. P P B O X Y G E SIDE BOLTS BASE BOLTS Figure 3-1. Ultra Trace Sensor Bolt Installation Teledyne Electronic Technologies Analytical Instruments...

  • Page 30: Adding Electrolyte To The Ultra Trace Sensor

    Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 2. Slip the Teflon tubing (mounted inside the sensor) onto the " stainless steel tube at the bottom of the stainless steel top plate (see Figure 3-2).
  • Page 31 O -free gas. This will eliminate the O from the sensor before the addition of prepurged electrolyte. This procedure will substantially reduce the downtime associated with clean-up at the first startup of the analyzer. Teledyne Electronic Technologies Analytical Instruments...
  • Page 32 Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 After the electrolyte has been purged, it can be added to the sensor using the following procedure: 1. Remove the plastic screw cap from the anode port on the stainless steel plate on the top of the sensor body (Figure 3-4.1) and flush out...
  • Page 33 5. Remove the cadmium anode from the holder and immediately insert it into the sensor through the opening in the top mounting plate (Figure 3-5). Ensure that the O-ring is attached to the anode assem- bly. Teledyne Electronic Technologies Analytical Instruments...

  • Page 34: Ultra Trace Sensor Electrical Connections

    Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 ANODE PORT ELECTROLYTE CELL BODY Figure 3-5. Inserting the Anode Ultra Trace Sensor Electrical Connections There are two wires to be connected so that the sensor can send signals to the...

  • Page 35: Faradaic Calibrator

    LCD keeps track of the amount of time the calibrator has been used in a hh:mm format. A flashing “C=0:00” on the display indicates that the calibrator needs refilling. Teledyne Electronic Technologies Analytical Instruments...

  • Page 36: Adding Electrolyte To The Calibrator

    Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 NOTE: If you try to use the calibrator with insufficient electrolyte or without the current source leads connected, the LCD will dis- play CURRENT FAILURE MODE.
  • Page 37 Please refer to Material Safety Data Sheets to learn about potential hazards and corrective action in case of accident. Figure 3-8. Adding Electrolyte to the Calibrator. Teledyne Electronic Technologies 3-11 Analytical Instruments...
  • Page 38 Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 The analyzer is shipped with the calibrator electrode assembly installed. In order to add electrolyte to the calibrator, the electrode assembly must be removed from the calibrator block.
  • Page 39 (P/N W69) pro- vided. See Figure 3-10. 10. Reconnect the current source connector to the calibrator. Figure 3-9. Soaking the Calibrator Wick with the Electrolyte. Calibrator current source connector Figure 3-10. Installing the Calibrator. Teledyne Electronic Technologies 3-13 Analytical Instruments...

  • Page 40: Adding Water To The Reservoir

    Model 3060E Model 3060E Chapter 3 Chapter 3 Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Adding Water to the Reservoir If the analyzer is to be used continuously for on-line gas analysis, then add approximately 800 cc of distilled water to the reservoir. The rate of water addition to the sensor is controlled by the metering valve MV3 located adjacent to the reservoir, below the top cover plate.

  • Page 41: Level Detector And Solenoid Switch

    (valve 9) will remain closed regardless of the electrolyte level in the sensor. Opening MV3 will have no effect on the electrolyte level. Instability and damage to the Ultra Trace sensor will eventually result as the electrodes become dry. Teledyne Electronic Technologies 3-15 Analytical Instruments...

  • Page 42: Electrical Installation

    Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 Electrical Installation Electrical Connections All of the electrical connections originate at the back of the analyzer (see Figure 3-15). The analyzer is shipped with all of the electrical connections intact.

  • Page 43: Voltage Selection And Fuse Changing

    7. Replace the fuse block and the cover. Verify that the indicator pin is pointing to the correct voltage. Cover Fuse Block Indicator Pin Voltage Selector Card Housing Notch Figure 3-12. Removing the Voltage Card Teledyne Electronic Technologies 3-17 Analytical Instruments...
  • Page 44 Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 NOTE: Spare fuses are located in a clip attached to the power supply enclosure inside of the analyzer. To change from North American to European fuses, perform the following procedure: 1.

  • Page 45: Gas Line Connections

    Check that each of the lines is hooked up to the correct connection. The lines should be connected in the following order: 1. Span Gas In If you choose to use a span gas to calibrate the analyzer, connect the span gas tank to the span gas inlet. Teledyne Electronic Technologies 3-19 Analytical Instruments...
  • Page 46 Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 2. Sparger Vent The sparger vent transports the oxygen-contaminated gas out of the system after it leaves the Ultra Trace sensor. The sparge gas vent is routed through the water reservoir (gas flows above water) to purge out any oxygen in the water reservoir.
  • Page 47 RESERVOIR RESERVOIR COOLING DRAIN CALIBRATOR BYPASS SAMPLE BYPASS RS232 SERIAL PORT (9 PIN D-SUB) (MALE) AC POWER IN SPAN GAS SAMPLE/SPAN 5 ALARM CIRCUIT VENT CONNECTIONS SAMPLE IN Figure 3-15. Gas Line/Rear Panel Connections Teledyne Electronic Technologies 3-21 Analytical Instruments...

  • Page 48: Installation Checklist

    Model 3060E Model 3060E Model 3060E Chapter 3 Chapter 3 Chapter 3 Model 3060E Model 3060E Chapter 3 Chapter 3 Installation Checklist After installing the system, confirm the following: • The sample gas connection to the analyzer sample inlet port is not leaking.

  • Page 49: Operations

    Analyz Operations Overview The Model 3060E analyzer is a computerized system that operates through a central control module consisting of the microprocessor, signal processing unit and two display panels. Operations are performed and monitored through the controls and displays on the analyzer front panel. Figure 4-1 shows various sections of the analyzer front panel.

  • Page 50: Front Panel Controls And Indicators

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Front Panel Controls and Indicators Sample System Status Panel The sample system status panel illustrates the sample system and valve modes.

  • Page 51: Led Display

    The LCD display panel can display up to seven lines of text: • Line 1 indicates the valve mode. • Lines 2–6 display up to five lines of instructions, messages, or warnings. • Line 7 lists menu options. Teledyne Electronic Technologies Analytical Instruments...
  • Page 52 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Each of the menu options corresponds with one of the touch-control buttons. TELEDYNE BROWN ENGINEERING TELEDYNE BROWN ENGINEERING Analytical Instruments...
  • Page 53 Pressing buttons in certain sequences allows you to set modes of operation. The system’s electronics subsequently operate the correct valves depending on the options that you choose. The choices are displayed on the LCD screen and vary depending on the mode. Teledyne Electronic Technologies Analytical Instruments...

  • Page 54: Sensor Compartment Temperature Controller

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 NOTE: The LCD backlight enhances the ability to read the display menu and will automatically shut off after usage. Press the red key to turn the backlight back on.

  • Page 55: Operating The Analyzer

    4. If using a span gas to calibrate, the span gas tank should be securely connected to the span gas port. Span gas pressure should be between 10 and 30 psig. Teledyne Electronic Technologies Analytical Instruments...

  • Page 56: Modes Of Operation

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 5. Confirm that the electrolyte level in the Ultra Trace sensor is be- tween the green and yellow markers on the main body of the Ultra Trace sensor (see Chapter 3).

  • Page 57: Warm Start

    COLD START the power OFF, wait for 10 seconds and then hold down the red key on the touch panel while flipping the analyzer power switch to ON. The very first screen will indicate COLD START Teledyne Electronic Technologies Analytical Instruments...

  • Page 58: Forcing A Cold Start Without First Shutting Down

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Forcing a Cold Start Without First Shutting Down To force a at the next power-up after the analyzer has been used, COLD START follow the procedure outlined below.

  • Page 59: Full Start Mode

    SET TIM E/DATE 1-01-93 12 : 03 AM forming scheduled zero and span operations at this time. You may set SELEC DOW N ACCPT time/date any time by pressing SETUP from Analyzer mode. Teledyne Electronic Technologies 4-11 Analytical Instruments...
  • Page 60 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 VALVES: OFF 2. After a few minutes, the screen displays W ARNING: IF THIS IS THE FIRST the options start mode.

  • Page 61: Full Start Options

    VALVES: PURGE-TO-SPAN system performs a sample line PURGE IN PROGRESS TIM E REM AINING 00 : 01 : 00 purge, then automatically contin- PLEASE W AIT . . . ues on to step 10. SKIP Teledyne Electronic Technologies 4-13 Analytical Instruments...
  • Page 62 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 10. The system directs you to check VALVES: SAMPLE PURGE CHECK THE FLOW RATE FOR the flow rate for 150 cc/min and...

  • Page 63: Setup For Span Gas Use (Full Start)

    PURGE IN PROGRESS system performs a purge-from-span, TIM E REM AINING 00 : 01 : 00 and automatically continues to step 21. PLEASE W AIT . . . SKIP FROM HERE GO TO STEP 21 Teledyne Electronic Technologies 4-15 Analytical Instruments...

  • Page 64: Setup For Both Span Gas & Internal Calibrator (Full Start)

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Setup for Both Span Gas & Internal Calibrator (Full Start) 15. After saying to the internal calibra- VALVES: OFF CAREFULLY FILL THE CALIBRATOR...
  • Page 65 NOTE: If the system shuts down due to high oxygen concentration, check for leaks around gas connections. Check that gas concentrations are not more than 30 PPM. Check that there is no back pressure in the analyzer vent lines. Repeat Full Start. Teledyne Electronic Technologies 4-17 Analytical Instruments...
  • Page 66 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 25. The screen indicates VALVES: ZERO LINE PURGE ZERO LINE PURGE and directs you to open the MV1 valve OXYGEN = 5.0 PPM O2 FLOW = 150.0 CC/M IN...
  • Page 67 TIME REMAINING 00 : 05 : 00 matically in the Analyze mode. PLEASE WAIT . . . After a 5 minute repurge of the SKIP sample system, the system auto- matically continues to step 31. Teledyne Electronic Technologies 4-19 Analytical Instruments...

  • Page 68: Quick Start Mode

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 31. The Ultra Trace sensor is reconnected. VALVES: ANALYZE After the sensor connects, the system CONNECTING SENSOR automatically returns you to the Ana- PLEASE WAIT .
  • Page 69 FLOW BELOW 20 SCCM. If this occurs, check the sample/span gas and air pressure. Make sure that they are within the recommended Teledyne Electronic Technologies 4-21 Analytical Instruments...
  • Page 70 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 VALVES: FLOW SET 9. When you press , the screen indi- PURGE IN PROGRESS TIME REMAINING 00 : 05 : 00 cates that the sample line is being PLEASE WAIT .

  • Page 71: Analyze Mode

    This is done by introducing a span gas between 5–9 PPM (either from an external source or generated by the built- in Faradaic calibrator) until the sensor output is at least of the span gas. Teledyne Electronic Technologies 4-23 Analytical Instruments...
  • Page 72 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 CAUTION: If the internal Faradaic calibrator is used to condition the Ultra Trace sensor, the calibrator must be refilled with calibration electrolyte after 10 hours of operation (see Chapter 3).

  • Page 73: Span Calibration Using An External Span Gas

    150 CC/MIN --- PRESS ACK WHEN READY --- Press when ready. If the span gas is not connected, the display will ask you to connect it, check the flow rate, and press when ready. Teledyne Electronic Technologies 4-25 Analytical Instruments...
  • Page 74 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 6. The screen displays the oxygen content VALVES: GAS SPAN OXYGEN = 5.0 PPM O2 and the flow rate. Use the FLOW = 150.0 CC/M IN...
  • Page 75 USER ABORTED AUTO SETTLE M ODE adjusted. You will receive a warning -- PRESS ACK W HEN READY -- that settling was aborted, and the system will return automatically to the Analyze mode main menu. Teledyne Electronic Technologies 4-27 Analytical Instruments...
  • Page 76 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 10. After pressing , the screen indicates VALVES: GAS SPAN CALIBRATION IN PROGRESS that the system is calibrating and PLEASE WAIT . . .

  • Page 77: Span Calibration Using The Internal Calibrator

    CURRENT FAILURE. If this occurs, press ACK to return to the Analyze mode. Fill the calibrator and start the calibration again. For more detail, see Conditioning the Ultra Trace Sensor earlier in this chapter. Teledyne Electronic Technologies 4-29 Analytical Instruments...
  • Page 78 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 The internal calibrator is designed to generate a calibration gas of up to 8 PPM. TBE recommends calibrating with a span gas of at least 80 PPB on the 100 PPB range.
  • Page 79 "CELL TOO STRONG" will be displayed. Press the START key to reset the analyzer to the factory settings. Teledyne Electronic Technologies 4-31 Analytical Instruments...
  • Page 80 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 10. If you press , go to step 14. If you VALVES: CALIBRATOR SPAN AUTO OXYGEN = 5.0 PPM O2 FLOW = 150.0 CC/M IN...

  • Page 81: Zero Calibration

    ANALY 3. The display will ask you to select VALVES: ANALYZE between manual or automatic calibrator CHOOSE M ANUAL OR AUTO SETTLING settling. If you press , continue to step 5. AUTO M AN Teledyne Electronic Technologies 4-33 Analytical Instruments...
  • Page 82 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 4. If you have chosen Auto settling, the screen displays the present oxygen concentration and the flow rate. It also checks whether the background signal is within the acceptable range.
  • Page 83 5–7 days, replace the electrolyte with freshly prepurged electrolyte. Replacing the electrolyte re- moves the dissolved oxygen from the Ultra Trace sensor and the background will will drop below the acceptable limit quickly. Teledyne Electronic Technologies 4-35 Analytical Instruments...
  • Page 84 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 7. If you press to change the electro- VALVES: ZEROING T=25C CAREFULLY REPLACE ELECTROLYTE lyte, replace the electrolyte and press...

  • Page 85: Important Notes On Zero And Span Calibration

    After this time, the analyzer should be calibrated once a month. TET/AI recommends calibrating the analyzer in the 0–1 or 0–10 PPM range with a typical span gas value of 500–700 PPB. Teledyne Electronic Technologies 4-37 Analytical Instruments...

  • Page 86: Setup Mode: System Password

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Immediately after entering Before zeroing background After zeroing, background Zero mode signal = 65 ppb signal = 60 ppb signal = 0.0 ppb...
  • Page 87 If you fail to enter the true authorization code, the system will not allow you to enter in the menus of the SETUP mode. If you loose the authorization code, you must perform a Cold Start to erase the previously entered code. Teledyne Electronic Technologies 4-39 Analytical Instruments...

  • Page 88: Setup: Alarms

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Setup: Alarms 1. After completing initial start-up, select VALVES: ANALYZE C=9:59 T=25C FLOW = 150.0 CC/M IN from the Analyze mode menu to SETUP 5.00...
  • Page 89 Analyze mode main menu. The appro- 5.00 PPM 02 priate alarm number and type flashes in AUTORANGE: 10 PPM the upper right-hand corner of the STDBY SETUP RANGE ALRMR display if the alarm is tripped. Teledyne Electronic Technologies 4-41 Analytical Instruments...

  • Page 90: Setup: Auto Settling

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Setup: Auto Settling The Auto Settling setup mode allows the user to set parameters (Period and Slope) for the automatic calibration cycles to achieve optimum instrument accuracy based on the user's needs.
  • Page 91 7. To continue modifying the auto settling VALVES: ANALYZE C=9:59 T=25C parameters, select to modify the SELECT AUTO-SETTLE PARAM ETER SLOPE TO M ODIFY - PERIOD, SLOPE OR AUTO CALIBRATOR OFFSET slope for settling. PEROD SLOPE OFFST Teledyne Electronic Technologies 4-43 Analytical Instruments...
  • Page 92 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Figure 4-9. Setting Period Settling Figure 4-10. Setting Slope Zero Settling Figure 4-11. Setting Slope Span Settling Teledyne Electronic Technologies...
  • Page 93 20–40 minutes. However, by increasing the span settling value, calibration may be achieved much quicker (10–20 minutes) but will be less accurate. Figure 4-13 shows how accuracy is affected by changing span settling slope values. Teledyne Electronic Technologies 4-45 Analytical Instruments...
  • Page 94 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Figure 4-12. Effect of the Zero Settling Slope on the Accuracy of the Base Line Figure 4-13. Effect of Span Settling Slope on the...

  • Page 95: Setup: Clock/Scheduled Span Or Scheduled Zero

    ENTER AUTHORIZATION CODE ENTER YOUR CODE _ _ _ keys to scroll through the letters/ DOWN numbers. Press to enter the SELEC desired value for each space in the code. Press when finished. ACCPT Teledyne Electronic Technologies 4-47 Analytical Instruments...
  • Page 96 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 4. Press to continue to the time/ CLOCK VALVES: ANALYZE T=25C - - - - SYSTEM SETUP - - - - date or scheduled Zero/Span menu.

  • Page 97: Setup: More Options

    - - - - M ORE SYSTEM SETUP - - - - filter period, displaying the mode during FILTR: SET TIM E AND DATE zeroing, and presenting the current ZEROB: SETUP SHOW BASE ZERO system configuration. FILTR ZEROB BYPAS Teledyne Electronic Technologies 4-49 Analytical Instruments...
  • Page 98 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 6. If you press , the display gives you FILTR VALVES: ANALYZE C=9:59 T=25C SET FILTER PERIOD the option of choosing the level of...
  • Page 99 Analyze mode Normal mode Analyze mode Zero mode TIME Figure 4-14. Typical Signal in Normal Mode Analyze mode Analyze mode Base mode Offset zero Zero mode TIME Figure 4-15. Typical Signal in Base Mode Teledyne Electronic Technologies 4-51 Analytical Instruments...
  • Page 100 Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Setup: H O Reservoir NOTE: Some Ultra Trace Oxygen Analyzers were built with a toggle switch mounted in the sensor compartment as shown in Figure 3-6. The...

  • Page 101: Setup: H2O Reservoir

    VALVES: RESERVOIR = ON returned to the previous screen. Press SELECT SWITCH TO TURN H2O RESERVOIR ON OR OFF to return to the previous menus. RPEAT: RESERVOIR WILL TURN ON AND OFF TEN TIMES RPEAT Teledyne Electronic Technologies 4-53 Analytical Instruments...

  • Page 102: Setup: Modem

    Setup: Modem You can remotely locate the analyzer and view and control analyzer function through an IBM-compatible PC using either TRACS (Teledyne Remote Analytical Control Software) or a command set using your own communica- tions software. The modem at the analyzer end of the operation can be prepared for use through this menu.

  • Page 103: Setup: Zero/Span Gas Source

    INTERNAL CALIBRATOR NOW IN USE screen prompts you to fill the calibrator with electrolyte, and returns you to the screen in step 2. If you press the system returns you to the screen in step 2. Teledyne Electronic Technologies 4-55 Analytical Instruments...

  • Page 104: Setup: Negative O2

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 6. To check your selection, press again, confirm your selection and then press twice to return to the Ana- lyze mode main menu.

  • Page 105: Range Mode

    3. The next screen returns you to the VALVES: ANALYZE C=9:59 T=25C FLOW = 150.0 CC/M IN Analyze mode menu. The last line 5.00 PPM 02 indicates the range selection and mode. AUTORANGE: 10 PPM STDBY SETUP RANGE ALRM R Teledyne Electronic Technologies 4-57 Analytical Instruments...

  • Page 106: Manual Range Function

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 Manual Range Function 1. After completing initial start-up, you VALVES: ANALYZE C=9:59 T=25C FLOW = 150.0 CC/M IN may select...

  • Page 107: Normal Shutdown

    4. Make changes in the background gas VALVES: OFF selection if required, and press SELECT THE BACKGROUND GAS ACCPT BACKGROUND GAS = NITROGEN to continue (quick start), or press for the initial start-up menu. DOW N ACCPT Teledyne Electronic Technologies 4-59 Analytical Instruments...

  • Page 108: High Current Output Mode

    Model 3060E Model 3060E Model 3060E Chapter 4 Chapter 4 Chapter 4 Model 3060E Model 3060E Chapter 4 Chapter 4 High Current Output Mode 10.00 blinks in High Current m ode VALVES: ANALYZE C=9:59 T=25C > 10 1. If FLOW = 49.5 CC/M IN 10.00...

  • Page 109: Routine Maintenance Checklist

    The electrolyte level detector mounted inside the Ultra Trace sensor continu- ously monitors the electrolyte level and triggers automatic addition of water to the sensor. The rate of addition is set close to the rate of evaporation of water Teledyne Electronic Technologies Analytical Instruments...

  • Page 110: Purging Distilled Water

    Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 from the electrolyte. If the rate of evaporation exceeds the rate of addition, causing the level to drop below the red marker, open MV3 one-half turn to increase the rate of addition, and repeat, if necessary.

  • Page 111: Replacing The Electrolyte In The Ultra Trace Sensor

    8. The analyzer will display the signal which will vary depending on the amount of dissolved oxygen in the electrolyte. The signal output will gradually decrease as the dissolved oxygen is removed by sparging the electrolyte. The down-time to PPB range should be about 10–24 hours. Teledyne Electronic Technologies Analytical Instruments...

  • Page 112: Scrubber Maintenance

    The oxygen scrubber is a replaceable (P/N C58750) or rechargeable compo- nent. With normal use, the scrubber usually lasts for several years. The scrubber is designed specifically for the Model 3060E. If oxygen readings drift or the analyzer will not zero, the scrubber may need replacing or recharging. Contact the factory for recharging the scrubber.

  • Page 113: Troubleshooting Tables

    CHECK SENSOR CHECK ELECTRICAL CABLE CONNECTIONS CONNECTIONS CHECK ELECTROLYTE FROM REAR OF CONTROL LEVELS IN ULTRA MODULE TO OUTPUT TRACE SENSOR TERMINALS CALL FAILURE PROCEED SERVICE CORRECTED Table 5-1. No Signal to Display/No Analog Output Signal Teledyne Electronic Technologies Analytical Instruments...
  • Page 114 Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 NOISE OR SPIKES ON SIGNAL OUTPUTS CHECK ANODE AND CATHODE TERMINALS ARE FIRMLY SECURED REDUCE SPARGE RATE NOISE PROCEED REDUCED...
  • Page 115 FROM LOW (4-5 STREAMS OF BUBBLES) TO MEDIUM (10-20 STREAMS OF BUBBLES) CHANGE ELECTROLYTE WITH PREPURGED ELECTROLYTE REPLACE ANODE ACCEPTABLE CALL PROCEED BACKGROUND SERVICE SIGNAL Table 5-3. Background Signal Greater than the Maximum Correctable Value Teledyne Electronic Technologies Analytical Instruments...
  • Page 116 Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 SLOW RESPONSE/ RECOVERY TIM E CHECK BYPASS FLOW (1 LITER/M IN) REPLACE ACCEPTABLE PROCEED SENSOR RESPONSE TIM E ACCEPTABLE RESPONSE...
  • Page 117 IF RESISTANCE IS MORE AT 25 C THAN 1K OFF FROM THE EXPECTED VALUE PRESS THE START KEY TO RESET THE ANALYZER TO THE FACTORY SETTINGS CALL FAILURE PROCEED SERVICE CORRECTED Table 5-5. Temperature Failure Teledyne Electronic Technologies Analytical Instruments...
  • Page 118 Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 FLOW FAILURE <20cc/min 150cc/MIN OPTIMUM CHECK AIR SUPPLY PRESSURE (75-80 PSIG) CHECK SAMPLE SPAN GAS PRESSURE (10-30 PSIG) PRESS THE START KEY...
  • Page 119 CURRENT FAILURE CHECK FOR CALIBRATOR ELECTROLYTE CHECK THAT CALIBRATOR WICK IS CENTERED CHECK CALIBRATOR CONNECTIONS & CABLES PRESS ACK TO RETURN TO ANALYZE MODE FAILURE CALL CORRECTED SERVICE PROCEED Table 5-7. Calibration Current Failure Teledyne Electronic Technologies 5-11 Analytical Instruments...

  • Page 120: Analytical Instruments

    Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 HIGH CURRENT FAILURE (>30ppm) CHECK FOR AIR LEAKS IN SAMPLE LINE PRESS START KEY TO RESET THE ANALYZER TO FACTORY...
  • Page 121 Ultra race Oxyg race Oxygen Anal en Anal en Analyz SENSOR W EAK CONDITION SENSOR (SECTION 4.3.6.1) RECALIBRATE ANALYZER (SECTION 4.3.7 OR 4.3.7.1) CALIBRATION REPLACE PROCEED SUCCESSFUL SENSOR Table 5-9. Sensor Too Weak Error Teledyne Electronic Technologies 5-13 Analytical Instruments...
  • Page 122 Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 SENSOR STRONG VERIFY SPAN GAS CERTIFICATION PURGE THE SPAN CHECK EXTERNAL SPAN INTERNAL SPAN GAS LINE; USE A CALIBRATION VERIFY FLOW...
  • Page 123 WET THE ENTIRE CALIBRATOR WICK WITH CALIBRATION ELECTROLYTE MOUNT THE CALIBRATOR ASSEMBLY RECALIBRATE ANALYZER (SECTION 4.3.7 OR 4.3.7.1) REPLACE CALIBRATOR SPAN GAS PROCEED GENERATED REPLACE ELECTROLYTE Table 5-11. No Span Gas From Internal Calibrator Teledyne Electronic Technologies 5-15 Analytical Instruments...
  • Page 124 Model 3060E Model 3060E Model 3060E Chapter 5 Chapter 5 Chapter 5 Model 3060E Model 3060E Chapter 5 Chapter 5 Teledyne Electronic Technologies 5-16 Analytical Instruments...

  • Page 125: Quick Reference

    Overview This Quick Reference section is designed to provide the essential steps and key sequences for each mode of operation of the Model 3060E Analyzer. It should be considered a companion to the more detailed explanation of operation found in Section 4 of this manual.
  • Page 126 Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Use COLD START when: • The Instrument is turned on for the first time. • A new authorization code is desired.
  • Page 127 2 minutes to check the oxygen level. If the oxygen concentration falls below 30 PPM, normal operation will resume. • If the measured oxygen level remains above 30 PPM for 60 minutes, the unit will automatically shut down. Teledyne Electronic Technologies Analytical Instruments...

  • Page 128: Cold Start

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Cold Start COLD START From the ANALYZE MODE BY POWERING DOWN Turn power off. Wait 10 seconds Hold down red key on panel...

  • Page 129: Full Start

    PURGE FROM SPAN (30 MIN CHECK FLOW RATE SLOWLY OPEN MV1 SAMPLE GAS LINE PURGE (30 MIN) ZERO LINE PURGE CALIBRATOR PURGE (30 MIN) SAMPLE LINE REPURGED (5 MIN) ENTER ANALYZE MODE Figure 6-2. Full Start Teledyne Electronic Technologies Analytical Instruments...

  • Page 130: Quick Start

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Quick Start QUICK FULL NOTE: Pressing ESC brings you back to previous screen. SELECT BACKGROUND ACCPT CONNECT SAMPLE CLOSE SPAN GAS...

  • Page 131: Span Calibration Using External Gas Source

    TIME REMAINING. PRESSING ANY OTHER KEY BUT ACK WILL ABORT OUT OF AUTO SETTLING CALIBRATION PROCESS COMPLETED. PRESS ACK TO RETURN TO ANALYZE MODE STDBY SETUP RANGE ALRMR Figure 6-4. Calibration/Span Calibration with External Source Teledyne Electronic Technologies Analytical Instruments...

  • Page 132: Span Calibration Using Internal Calibrator

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Span Calibration Using Internal Calibrator STDBY SETUP RANGE ALRMR SPAN NOTE: Pressing ESC brings you CHOOSE A CALIBRATION back to previous screen.

  • Page 133: Zero Calibration

    Refer to Sections 3.3.1 and 4.3.7.2 for more details AFTER AUTO SETTLING, THE SYSTEM WILL AUTOMATICALLY RETURN TO THE ANALYZE MODE CALIBRATION PROCESS COMPLETED PRESS ACK TO RETURN TO ANALYZE MODE Figure 6-6. Calibration/Zero Calibration Teledyne Electronic Technologies Analytical Instruments...

  • Page 134: Setting The Password

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Setting the Password STDBY SETUP RANGE ALRMR NOTE: Pressing ESC brings you back to previous screen. SYSTM USE UP AND DOWN KEYS...

  • Page 135: Setting The Alarms

    ALARM YOU SET ACCPT REFER TO SECTION 4.3.8.2 FOR DISCUSSION OF EACH PARAMETER: ALARMS ARE NOW SET PRESSING ESC TWICE RETURNS YOU TO THE ANALYZE MODE STDBY SETUP RANGE ALRMS Figure 6-8. Setup/Setting the Alarms Teledyne Electronic Technologies 6-11 Analytical Instruments...

  • Page 136: Auto Settling

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Auto Settling STDBY SETUP RANGE ALRMR NOTE: Pressing ESC brings you USE UP AND DOWN KEYS SYSTM TO SCROLL THROUGH THE back to previous screen.

  • Page 137: Scheduled Zero And Scheduled Span

    DOWN DOWN SET TIME FOR SET TIME FOR NEXT ZERO NEXT SPAN ACCPT ACCPT ACCPT PRESSING ESC TWICE RETURNS YOU TO ANALYZE MODE STDBY SETUP RANGE ALRMR Figure 6-10. Setup/Clock-Scheduled Zero and Scheduled Span Teledyne Electronic Technologies 6-13 Analytical Instruments...

  • Page 138: Filtering, Zero Display, Bypass And Reservoir

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Filtering, Zero Display, Bypass and Reservoir STDBY SETUP RANGE ALRMR USE UP AND DOWN KEYS SYSTM NOTE: Pressing ESC brings you TO SCROLL THROUGH THE back to previous screen.

  • Page 139: Modem

    STDBY SETUP RANGE ALRMR MODEM MODEM MONTR ESTABLISHES A PC THIS OPTION INITIATES TO ANALYZER LINK A MODEM SEARCH THROUGH A NULL MODEM CABLE STDBY SETUP RANGE ALRMR Figure 6-12. Setup/Modem Teledyne Electronic Technologies 6-15 Analytical Instruments...

  • Page 140: Setup: Zero And Span Gas Source

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Setup: Zero and Span Gas Source NOTE: Pressing ESC brings you back to previous screen. STDBY SETUP RANGE ALRMR SELECT BETWEEN ZERO OR SPAN...

  • Page 141: Negative Oxygen Display

    NEG02 back to previous screen. THIS OPTION ENABLES THIS OPTION DISABLES NEGATIVE OXYGEN NEGATIVE OXYGEN READINGS READINGS PRESS ESC TWICE TO RETURN TO ANALYZE MODE STDBY SETUP RANGE ALRMR Figure 6-14. Setup/Negative Oxygen Display Teledyne Electronic Technologies 6-17 Analytical Instruments...

  • Page 142: Auto And Fixed Range

    Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Auto and Fixed Range NOTE: Pressing ESC brings you back to previous screen. STDBY SETUP RANGE ALRMR SELECT BETWEEN AUTO OR FIXED RANGE...

  • Page 143: Standby: Normal Shutdown

    SHUTDOWN, TURN POWER SWITCH OFF START USE UP/DOWN AND SELEC KEYS TO CHANGE THE BACKGROUND GAS PRESSING ESC BRINGS YOU TO QUICK START MENU FULL QUICK Figure 6-16. Standby/Normal Shutdown Teledyne Electronic Technologies 6-19 Analytical Instruments...
  • Page 144 Model 3060E Model 3060E Model 3060E Chapter 6 Chapter 6 Chapter 6 Model 3060E Model 3060E Chapter 6 Chapter 6 Teledyne Electronic Technologies 6-20 Analytical Instruments...

  • Page 145: Appendix

    Zero: Integral scrubber makes O -free zero gas Span: Integral Faradaic calibrator makes a known span gas. If preferred, a span gas inlet port is provided to accommodate a certified span gas Specifications subject to change without notice. Teledyne Electronic Technologies Analytical Instruments...

  • Page 146: Spare Parts List

    IMPORTANT: Orders for replacement parts should include the model number, serial number and range of the analyzer for which the parts are intended. Orders should be sent to: Teledyne Electronic Technologies/Analytical Instruments 16830 Chestnut Street City of Industry, CA 91749-1580...

  • Page 147: Drawing List

    Final Assembly D-59713 Schematic, Analog input main PCB D-50824 Schematic, Analog input daughterboard B-50721 Schematic, Signal terminal PCB D-59130 Schematic, Valve control PCB, top D-59133 Schematic, Valve control PCB, bottom D-50609 Schematic, LED display PCB Teledyne Electronic Technologies Analytical Instruments...

  • Page 148: Material Safety Data Sheets

    Product Name: Product Name: Product Name: Product Name: Ultra Trace Sensor Electrolyte/Open Cathode Cell Manufacturer: Manufacturer: Manufacturer: Manufacturer: Manufacturer: Teledyne Electronic Technologies Analytical Instruments Address: Address: Address: 16830 Chestnut Street, City of Industry, CA 91749 Address: Address: Phone: Phone: Phone:...
  • Page 149 Carcinogenity: Carcinogenity: Carcinogenity: Carcinogenity: Carcinogenity: NTP Annual Report on Carcinogens: Not listed LARC Monographs: Not listed OSHA: Not listed Other health hazards: Other health hazards: Other health hazards: Other health hazards: Other health hazards: Teledyne Electronic Technologies MSDS-2 Analytical Instruments...
  • Page 150 NOTE: The above information is derived from the MSDS provided by the manu- facturer. The information is believed to be correct but does not purport to be all inclusive and shall be used only as a guide. Teledyne Electronic Technologies/Analytical Instruments shall not be held liable for any dam- age resulting from handling or from contact with the above product.
  • Page 151 Product Name: Product Name: Product Name: Product Name: Product Name: Calibration Electrolyte Manufacturer: Manufacturer: Manufacturer: Manufacturer: Manufacturer: Teledyne Electronic Technologies Analytical Instruments Address: Address: Address: 16830 Chestnut Street, City of Industry, CA 91749 Address: Address: Phone: Phone: Phone: (818) 961-9221...
  • Page 152 Not known. aggravated by exposure: aggravated by exposure: Carcinogenity: Carcinogenity: Carcinogenity: Carcinogenity: Carcinogenity: NTP Annual Report on Carcinogens: Not listed LARC Monographs: Not listed OSHA: Not listed Teledyne Electronic Technologies MSDS-5 Analytical Instruments...
  • Page 153 NOTE: The above information is derived from the MSDS provided by the manu- facturer. The information is believed to be correct but does not purport to be all inclusive and shall be used only as a guide. Teledyne Electronic Technologies/Analytical Instruments shall not be held liable for any dam- age resulting from handling or from contact with the above product.

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