Teledyne D series Installation And Operation Manual
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Teledyne D series Installation And Operation Manual

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D-Series Pumps
Installation and Operation Guide
Part #69-1243-969 of Assembly #60-1243-998
Copyright © 2013. All rights reserved, Teledyne Isco
Rev. F, July 2018

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  • Page 1 D-Series Pumps Installation and Operation Guide Part #69-1243-969 of Assembly #60-1243-998 Copyright © 2013. All rights reserved, Teledyne Isco Rev. F, July 2018...
  • Page 3 Teledyne ISCO recommends that you read this manual completely before placing the equipment in service. Although Teledyne ISCO designs reliability into all equipment, there is always the possibility of a malfunction. This manual may help in diagnosing and repairing the malfunction.
  • Page 5 D Series Syringe Pumps Warnings, Cautions, and Notices Warnings and Cautions The lightning flash and arrowhead within the triangle is a warning sign alerting you to “dangerous voltage” inside the product. The exclamation point within the triangle is a warning sign alerting you to important instructions in this manual.
  • Page 6 D Series Syringe Pumps Warnings, Cautions, and Notices Warnungen und Vorsichtshinweise Der gepfeilte Blitz im Dreieck ist ein Warnzeichen, das Sie vor „ “ gefährlichen Spannungen im Inneren des Produkts warnt. Das Ausrufezeichen in Dreieck ist ein Warnzeichen, das Sie darauf aufmerksam macht, daß...
  • Page 7 D Series Syringe Pumps Warnings, Cautions, and Notices “To prevent damaging the instrument or injuring yourself, it is absolutely necessary that you understand everything in English, above all, technical terms, before operating the instrument. Otherwise, it is necessary for you to receive complete instruction from someone qualified who understands both the instrument and English very well.”...
  • Page 8 D Series Syringe Pumps Warnings, Cautions, and Notices Laitteelle tai käyttäjälle aiheutuvien vahinkojen välttämiseksi on tärkeää, että käyttäjä hallitsee englannin kielen ja englantilaiset tekniset termit tai on saanut käyttöopastuksen englantia osaavalta henkilöltä. “Per evitare danni allo struménto od incidenti all’operatore, é...
  • Page 9 220, SFX 3560) be absolutely sure the built-in venting fan (a brushless motor) is operating properly. The Teledyne Isco D Series Syringe Pumps and the SFX units, use brush-type drive motors. Minor modifications to the pumps may render them safer, especially in the rare event of catastrophic piston seal failure.
  • Page 10 Remarque de sûreté concernant l’usage d’un fluide inflammable avec les pompes à seringue d’Isco Série ‘D’ et le système SFX. Le système SFX et pompes à seringue Teledyne Isco doivent être placées à l'intérieur d’une hotte chimique fonctionnelle, quand vous utilisez éthane C , ou tout autre gaz inflammable.
  • Page 11 D Series Syringe Pumps Warnings, Cautions, and Notices WARNING: PLEASE READ At the request of our Supercritical Fluid Extraction laboratory staff, we want our customers to be aware of the potential hazards involved with supercritical fluid extraction. Oxidizing gases, such as nitrous oxide, in contact with organic matrices or flammable modifiers, can detonate under certain conditions.
  • Page 12 In all cases, when using Teledyne Isco instrumentation, prudence and common sense must be used. WARNING: Pinch point.
  • Page 13 D Series Syringe Pumps Warnings, Cautions, and Notices AVIS: Éviter de répandre! Les liquides qui sont pompés dans cet instrument peuvent être cancérigènes, hasards biologiques, inflammables, ou radioactifs. Si vous devez utiliser ces liquides hasardeux, il est très recommandé que vous le faites à l'intérieur d'un environnement isolé...
  • Page 14 D Series Syringe Pumps Warnings, Cautions, and Notices Commonly Ordered Replacement Parts for the D Series Syringe Pumps Description Part Number Cylinder Seals General: 30D Seal Assembly 0-2068 bar 60-1249-128 30D Piston Assembly 0-2068 bar 60-1249-129 0-1379 bar 202-9096-08 65DM 0-689.5 bar...
  • Page 15 D Series Syringe Pumps Warnings, Cautions, and Notices Commonly Ordered Replacement Parts for the D Series Syringe Pumps Description Part Number 1000D Inlet/Outlet fittings:  " NPT Plug 209-0168-09   " NPT Connector to " tubing 209-1063-36 Stainless Steel Tubing: ...
  • Page 16 D Series Syringe Pumps Warnings, Cautions, and Notices -NOTICE- If you have ordered one of the following custom pumps from Teledyne Isco, technical specifications for tubing and fittings listed in this manual do not apply to your system. Contact the factory for details about your custom pump.

  • Page 17: Table Of Contents

    D Series Syringe Pumps Table of Contents Section 1 Introduction 1.1 About This Manual ..........1-1 1.2 Specifications .
  • Page 18 D Series Syringe Pumps Table of Contents 3.4.5 System Reset (Restore Default Settings) ......3-5 3.4.6 Display Contrast .
  • Page 19 D Series Syringe Pumps Table of Contents 4.3 Single-Pump Gradient Programming ........4-8 4.4 Dual Pump Concentration Gradient Programming .
  • Page 20 8.8 Serial Commands for the D Series Pump ....... 8-20...
  • Page 21 A.1.1 D Series Controller ........
  • Page 22 D Series Syringe Pumps Table of Contents 1-5 Pump controller key functions ........1-14 1-6 Pump controller rear panel connectors .
  • Page 23 9-14 D Series motor brush replacement ........
  • Page 24 1-14 Pump Front Panel ..........1-18 2-1 D Series Syringe Pump Accessory Packages ......2-3 2-2 Manual Refill Kits .
  • Page 25 D Series Syringe Pumps Table of Contents 7-6 Holding Registers ........... 7-7 8-1 External control connector serial pin connections .
  • Page 26 D Series Syringe Pumps Table of Contents xxii...

  • Page 27: About This Manual

    Section 9 Pump Maintenance, Troubleshooting, and Servicing Appendix A Replacement Parts 1.2 Specifications The technical specifications for the D Series Syringe Pumps are detailed in Tables 1-2 through 1-9. Note Underwriters Laboratories (UL) has certified all Series D Pumps with the exception of the 100 VAC versions.

  • Page 28: Flow Rate Range

    D Series Syringe Pumps Section 1 Introduction Table 1-1 30D Technical Specifications CYLINDER CAPACITY 30.42 ml POWER REQUIREMENTS 100 ± 10 VAC, 2.8 A maximum 117 ± 12 VAC, 2.4 A maximum Factory Set (Mains voltage line cord is a 234 ±...
  • Page 29 MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 30: 65Dm Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 31: 100Dm Technical Specifications

    2000 m NOTES: a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 32: 100Dx Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 33: D Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 34: D Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. Using water at 137.9 bar and a temperature controlled environment at 30°C. The analog output is an optional accessory.

  • Page 35: 500Hpx Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. A team lift is recommended when moving this instrument. Using water at 137.9 bar and a temperature controlled environment at 30°C.

  • Page 36: 1000D Technical Specifications

    MAXIMUM ALTITUDE 2000 m a. Underwriters Laboratories (UL) has certified all D Series Pumps with the exception of the 100 VAC versions. b. A team lift is recommended when moving this instrument. Using water at 137.9 bar and a temperature controlled environment at 30°C.

  • Page 37: Flow Rate Range

    D Series Syringe Pumps Section 1 Introduction 260D Flow Rate Range 100 125 150 175 200 225 250 275 300 325 350 375 400 425 450 475 500 Pressure (bar) 517.1 Flow Rate (ml/min) Max. Pressure (bar) 0.001 to 90 517.1...

  • Page 38: Hpx Flow Rate Range

    D Series Syringe Pumps Section 1 Introduction 500 HPx Flow Rate Range Pressure (bar) 344.7 Flow Rate (ml/min) Max. Pressure (bar) 0.001 to 340 344.7  340 to 408 (409.8 ml/min – flow rate) 4.985 Figure 1-3 500 HPx flow rate range...

  • Page 39: Unpacking

    P.O. Box 82531 Lincoln, NE 68501 USA immediately. Phone: (800) 228-4373 Compare the contents of the boxes with the enclosed packing (402) 464-0231 slip. If there are shortages, contact Teledyne Isco immediately. FAX: (402) 465-3022 E-mail: IscoInfo@teledyne.com 1-13...

  • Page 40: Controls And Indicators

    D Series Syringe Pumps Section 1 Introduction 1.4 Controls and The pump controller regulates all pumping functions. It is designed to sit on top of the pump base, but may be located else- Indicators where, according to safety and convenience. Programming and setup are performed using the keypad on the front panel.

  • Page 41: Pump Controller Key Functions

    D Series Syringe Pumps Section 1 Introduction Table 1-11 Pump Controller Key Functions Description ON/STANDBY Two-position toggle switch turns controller on and activates drive motor to maintain position. Standby disables the drive motor and halts the controlling processor. A, B, C, D Softkeys;...

  • Page 42: Pump Controller Rear Panel Connectors

    D Series Syringe Pumps Section 1 Introduction Figure 1-6 Pump controller rear panel connectors Table 1-12 Pump Controller Rear Panel Connectors Item No. on Connector Description Figure 1-6 PUMP D This connector is only used during multiple pump operation. The control cable from the rear panel of the fourth pump is attached to this connector.

  • Page 43: Pump Rear Panel Connectors

    D Series Syringe Pumps Section 1 Introduction 4-20mA OUTPUT Optional circuit provides 4-20mA current loop output and additional digital inputs and outputs. ANALOG OUTPUT Optional circuit provides flow rate and volume outputs. See Section 3.9. ELECTRIC VALVES Optional circuit provides motor drive for valve operation.

  • Page 44: Electrical Connections

    D Series Syringe Pumps Section 1 Introduction External Fuses * Limits pump current drawn from main power supply. Replace with same type: (“T” time delay fuses) 1 - 2.0 Amp for 100/117 volt operation 2 - 1.0 Amp for 234 volt operation For 500HPx Pumps: 1 - 7.5 Amp for 100 volt operation...

  • Page 45: Cabling

    D Series Syringe Pumps Section 1 Introduction CAUTION All connections between the pump and controller should be made BEFORE the pump is connected to mains power. 1. Connect the pressure transducer cable (which originates from the top of the pump cylinder) to the nine pin sub-D PRESSURE TRANSDUCER connector on the pump rear panel (Figure 1-7).

  • Page 46: Pump

    D Series Syringe Pumps Section 1 Introduction Hazloc pumps: 10 ft (3m) 68-1020-505 Extension cable for pump controller connect 50 ft (15.24m) 68-1020-506 D Series Pumps only: 10 ft (3m) 68-1020-210 50 ft (15.2m) 68-1020-214 RS232 Cable for computer serial control of a sin- gle controller.

  • Page 47: Preliminary Checkout

    D Series Syringe Pumps Section 1 Introduction Controller Pump Pressure Transducer connector Figure 1-10 Connecting the pump and controller CAUTION Never make any cable connections while the pump is powered 1.6 Preliminary Checkout After the electrical connections have been completed, follow this brief test of the pump’s operation:...

  • Page 48: Menu

    D Series Syringe Pumps Section 1 Introduction 3. Check the upper left corner of the controller screen. The current pump mode will appear in a two-letter abbrevia- tion, e.g. CF for constant flow. This will be followed by a lowercase letter indicating the current pump, e.g. “a” indi- cates that pump A is the current pump.

  • Page 49: Three Pump Stop Menu

    PUMP C PUMP A Figure 1-14 Four pump stop menu If you encountered any problems during the preliminary checkout, please contact the Teledyne Isco Service Department. The number is (800) 775-2965 or (402) 464-0231. Note In the event of an emergency, turn off the controller switch.
  • Page 50 D Series Syringe Pumps Section 1 Introduction 1-24...

  • Page 51: Section 2 Fluid System Connections And Accessories

    See Sections 2.4.1 and 2.4.2. 2.2 Fluid System All D Series pump models connect similarly, but with varying port sizes. Take care to follow the tips provided to ensure safety Connections and proper operation.

  • Page 52: Installation Tips

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Pressure transducer cap Nut & Plug Ferrule Pressure Transducer Port Port Nut & Collar Tubing to valve Plug Tubing to valve Figure 2-1 Liquid system plumbing connections (30D on Left) 2.2.2 Installation Tips...

  • Page 53: Accessory Packages

    1. Slide first the nut and then the ferrule over the tubing. 2. Push the tubing all the way into the port. 3. Hold the tubing in place and tighten the nut. Table 2-1 D Series Syringe Pump Accessory Packages Pump Model...

  • Page 54: Installing The Fittings (260D, 65Dm, And 100Dm/Dx Only)

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2.2.5 Installing the " Refer to Figure 2-1 Fittings (260D, 65DM,  1. Loosen the " nut on the adapter until it is held by a few and 100DM/DX only) threads.

  • Page 55: Draining Overflow

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2.2.6 Draining Overflow The drip tray outlet on the pump cylinder provides a means of  draining fluid from seal leakage. Use the " ID flexible tubing included with the accessory package to divert the leakage away from the pump.

  • Page 56: Drain Tube Installation And Wash Gland Connection

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories CAUTION The pressure in the wash gland and line should NEVER exceed the system pressure or the wash pressure limit as labeled on the pump. Units with a wash pressure limit label can be damaged if the pressure is exceeded.

  • Page 57: Cylinder Washing: Nitrogen Purge

    Section 2 Fluid System Connections and Accessories Note Wash gland options are available for the 500D syringe pump, with " wash tubes. Contact Teledyne Isco for more informa- tion. 2.2.8 Cylinder Washing: All pumps that do not have a wash gland are equipped with a Nitrogen Purge purge connector tube near the top of the pump body.

  • Page 58: Flushing Pumps With External Transducers

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2.2.9 Flushing Pumps with When changing pumped liquids in the Model 65D, 30D or other External Transducers models with external transducers, flush the pump to prevent cross-contamination or difficulties with incompatible fluids.

  • Page 59: Manual Outlet Valve Kit

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Note When connecting to pressurized sources in supercritical fluid applications, use the stainless steel tubing without a filter. An in-line filter is contained in the CO connection package (refer to Section 2.3.3).

  • Page 60: Co Cylinder Connection Package

    Figure 2-8 Outlet valve package connection 2.3.3 CO Cylinder For North American gas tank connections, the optional CO con- Connection Package nection package is available from Teledyne Isco. Table 2-4 CO Cylinder Connection Package 68-1247-043 Qty. Part Number Description ...

  • Page 61: In-Line Filter Package

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Reducing Inline filter PTFE connector washer Nipple frit assembly To CO To Valve Supply Inlet Figure 2-9 CO package installation 2.3.4 In-Line Filter Package The optional in-line filter package should be used when it is important to filter flow exiting the pump.

  • Page 62: Temperature And Pressure Controls

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2.4 Temperature and Some applications, such as those with very low flows, may require additional measures to maintain steady rates. Pressure Controls 2.4.1 Cylinder Insulating The optional insulating cover can reduce flow noise due to tem-...

  • Page 63: Temperature Control Jacket

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Notches in the cover provide openings for the inlet and outlet tubing, and for the cable to the pressure transducer. Installation 1. Install the back cover. 2. Route the cable around tubing through the appropriate tabs.

  • Page 64: Packages And Parts

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Table 2-6 Packages and Parts Item Description Part Number Temperature control jacket packages for: 65D, 65DM,100DM, 100DX, 260D 68-1247-047 68-1267-001 500D, 500HPx 68-1247-057 500SP 68-1247-115 1000D 60-5364-199 Temperature control jacket assembly:...
  • Page 65 D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 3. Run the pump until the display shows C YLINDER Note This will fill the pump with air to prevent spills later. 4. Toggle the S switch on the controller, turning off TANDBY the controller display.

  • Page 66: Removing The Cylinder Cap With Wrenches

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Cap assembly Wrenches Figure 2-15 Removing the cylinder cap with wrenches Removing the pump Refer to Figure 2-16 on the next page for the following steps. cylinder 1. Empty the cylinder.

  • Page 67: Temperature Control Jacket Installation

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories CAUTION Be careful not to damage the O-rings when pushing them over the threads of the cylinder. Cylinder cap O-ring Outlet connector port Pressure transducer cable Temperature control jacket...

  • Page 68: Back Pressure Regulation

    7. Reinstall tubing. 8. Reconnect the pump pressure transducer cable. 2.4.3 Back Pressure The back pressure regulator option from Teledyne Isco reduces Regulation flow noise and improves pump performance at pressures less than 3.5 bar. Two back pressure regulators are available: •...

  • Page 69: Seal Options

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories 2.5 Seal Options The pump contains four seals and a wear ring. Transducer seal – The transducer seal is gold-plated to press into minute gaps between the surfaces of the transducer flange and the shelf of the cylinder cap.

  • Page 70: Seal Selection Chart

    D Series Syringe Pumps Section 2 Fluid System Connections and Accessories Table 2-7 Seal Selection Chart Seal Type Seal 65D/DM 100DX/DM 260D 500D/ 1000D Pressure Description 500HPX GENERAL/SFE 0-689.5 Black, PTFE 202-9096-08 202-9090-75 202-9091-06 202-9091-56 upper seal CARBON graphite filled...

  • Page 71: Section 3 Basic Programming And Operation

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.1 Introduction This section will familiarize you with the D Series pump con- troller and describe operating the pump under each of the various modes: constant flow, constant pressure, dispense, and refill.

  • Page 72: Run Screens

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.2.3 Run Screens The run screen appears once a program has been loaded and the pump is running. The run screen, which is determined by your program selections, displays current information about pump operation. The fol- lowing sections explain the display line by line.

  • Page 73: Selecting Operating Parameters

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.2.4 Selecting Operating There are four ways to program the system from a menu screen. Parameters Menu Selection – The number keys are used to select from listed menu items.

  • Page 74: Pump Selection (If Multiple Pumps)

    D Series Syringe Pumps Section 3 Basic Programming and Operation Use numbers 1-4 to select the pressure units (ATM, BAR, PSI, kPa). The units selected will be displayed on the first line after PRESSURE UNITS=. Use numbers 5-8 (mL/MIN, mL/HR, µL/MIN, µL/HR) to set the flow rate units.

  • Page 75: Power Failure [Stop]

    D Series Syringe Pumps Section 3 Basic Programming and Operation Unless otherwise specified, the pump will refill to full cylinder capacity. To specify a smaller refill volume, press 2 and enter the desired volume. Press 5 to toggle this feature off or on for each pump.

  • Page 76: Serial Option

    Use softkey B, NEXT ID#, to scroll through the available ID numbers. These are 1-7. Six is the default, as this is the unit identifier for the Teledyne Isco LabView™ software. For a complete discussion of serial control, refer to Section 8 in this manual.

  • Page 77: Valve

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.5.6 Valve This feature identifies the type of valves (passive, active (air), active ball (air), or electric) being used for the flow operation. Valves are set to “active” by default. If “active valve,” “active ball valve,”...

  • Page 78: Menu Three

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.6 Menu Three Menu 3 provides programming options for poor fills, diagnostics, pressure calibration, alternative pressure inputs, pressure control setting, and pressure setpoint tolerance. To save all settings and return to the main menu, press...

  • Page 79: Diff. Modes

    D Series Syringe Pumps Section 3 Basic Programming and Operation Press C A, C B, C C, or C D to select the correct pump, enter the calibration number, and press ENTER 3.6.4 Diff. Modes This feature allows the use of other analog inputs for pressure input to the pump.

  • Page 80: Front Panel Keys

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.8 Front Panel Keys In addition to the menu options, certain functions and modes are selectable from the front panel keyboard. 3.8.1 CONST PRESS and These keys place the system in constant pressure mode or con- CONST FLOW stant flow mode, respectively.

  • Page 81: Limits Menu

    D Series Syringe Pumps Section 3 Basic Programming and Operation To set the limits 1. Press LIMITS. To display the Limits menu, enter the num- ber of the limit you wish to program. One of five limit set- point menus will appear: MAX PRESS, MIN PRESS, MAX FLOW, MIN FLOW, or FLOW LIMIT.

  • Page 82: Rapid Press

    D Series Syringe Pumps Section 3 Basic Programming and Operation These features are set using the softkeys A - C, which toggle the feature on and off. Note The Max Press (maximum pressure) display on and alarm on options cannot be disabled.

  • Page 83: Disp

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3. The controller will display maximum flow rate and target pressure setting. If these values are correct, press D to con- tinue rapid pressurization. 4. If you know approximately what the pressure will be when the system is stable, enter this value as a target pressure.

  • Page 84: Multi-Pump Operation

    Sets the NCV feature On/Off. See Section 5.6.4. 3.9.2 Independent Control A D Series syringe pump controller can run four syringe pumps of up to Four Separate independently of each other in either constant pressure, constant Pumps flow mode, dispense mode, or any combination of the three.

  • Page 85: Operating Modes

    D Series Syringe Pumps Section 3 Basic Programming and Operation 2. Press softkey A, MORE. 3. Press number 4, MULTI PUMP. The multi-pump menu will appear. 4. Press number 1 for pumps A or B, press number 2 for pumps C or D.

  • Page 86: Constant Flow

    D Series Syringe Pumps Section 3 Basic Programming and Operation The constant pressure mode is used when the application of fixed pressure throughout the pumping operation is required. The pump will maintain the desired pressure by positive or negative displacement of the piston.

  • Page 87: Dispense Mode

    D Series Syringe Pumps Section 3 Basic Programming and Operation wish to define parameters for pump B, C, or D press soft- key D, select pump, and then press softkey A, B, C, or D to select pump A, B, C, or D respectively.

  • Page 88: External Control

    D Series Syringe Pumps Section 3 Basic Programming and Operation To specify the volume of the batch delivered, press (C), VOLUME enter the desired volume using the number keys, and press ENTER To dispense the batch, press . The sequence runs once, then stops.

  • Page 89: Preparation

    D Series Syringe Pumps Section 3 Basic Programming and Operation 3.12.2 Preparation Before programming the controller to accept the analog signal, you must know the maximum flow rate (constant flow) or the maximum pressure (constant pressure). Note The high and low limits you enter cannot exceed the pump specifications: Normal input = 10V.

  • Page 90: Calculation Examples

    D Series Syringe Pumps Section 3 Basic Programming and Operation FULL SCALE INPUT RANGE < XX.XXX VOLTS SET RANGE EXTERNAL REFILL PREVIOUS Figure 3-12 External control for refill menu To set the full-scale value (maximum 11.5 volts), press SET RANGE...

  • Page 91: Remote Run/Stop

    Figure 3-13 Button sequence for external control setup 3.13 Remote RUN/STOP The D series syringe pump RUN/STOP function can be exter- nally controlled by a switch contact closure or TTL input. The input voltage is 5 volts and is internally pulled high (RUN). The...

  • Page 92: Analog Flow Rate And Volume Output Options

    D Series Syringe Pumps Section 3 Basic Programming and Operation If two pumps are used with the controller, the second control wire should be connected to terminal 2, under DIGITAL INPUT. If three pumps are used with the controller, the third control wire should be connected to terminal 3, under DIGITAL INPUT.

  • Page 93: Current Loop Output

    D Series Syringe Pumps Section 3 Basic Programming and Operation 5V and the preferred output scale is 1 volt per 10 ml/min, is set at 50 ml/min. cannot exceed the pump FLOW MAX FLOW specification. A controller running one to two pumps can also output cylinder volume on the remaining outputs.

  • Page 94: Analog Output Signal/Sub-D Pins For 4-20Ma

    D Series Syringe Pumps Section 3 Basic Programming and Operation be purchased to output data for one or two more pumps. Refer to Table 3-3 for connections for the 4-20mA and 0-10v 12 channel outputs. Note Connections to the controller DB-25 are the same as shown in figure 3-14.

  • Page 95: Analog Output Signal/Sub-D Pins For 0-10 Vdc

    D Series Syringe Pumps Section 3 Basic Programming and Operation Table 3-4 Analog Output Signal/Sub-D Pins for 0-10 VDC Pin # Channel Data Type/Pump Pump A Flow Rate Pump A Flow Rate (Signal Return) Pump A Pressure Pump A Pressure (Signal Return)
  • Page 96 D Series Syringe Pumps Section 3 Basic Programming and Operation 3-26...

  • Page 97: Section 4 Gradient Pumping For Pressure, Flow, And Concentration Modes

    All Teledyne Isco syringe pump models can be used in gradient mode. The model 65D requires special hardware for this. Call the factory for complete information.

  • Page 98: Connecting The System

    When making fluid connections that use ferrules, be sure to use the ferrules supplied for that pump by Teledyne Isco. Push the tubing completely into the connector and finger-tighten. Then tighten with a wrench to clamp the ferrules onto the tubing.
  • Page 99 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes A g r a d i e n t p u m p i n g s y s t e m i n c l u d e s...

  • Page 100: Inlet Connections

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4.2.1 Inlet Connections Kit components and connections are shown in Figure 4-1. 1. Mount the inlet valve on the pump housing with the spacer block and screws provided.

  • Page 101: Outlet Connections

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4.2.2 Outlet Connections Kit components and connections are shown in Figure 4-2. 1. Mount the two-way outlet valve on the side of the pump housing opposite the refill valve, with the spacer block and screws provided.

  • Page 102: Dual Gradient System Connections

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4.2.3 Dual Gradient System Connection of the dual gradient system requires two refill valve Connections kits and the gradient mixer package, as discussed in the intro- duction on Page 4-1.

  • Page 103: Inlet Valves (A & C) Are From Refill Valve Kits)

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes OUTLET 1/8” OD X 0.069”ID INLET SST TUBING OUTLET (from INLET refill kit) VALVE A (from refill kit) 1/8” TO 1/16” 1/8” OD X 0.085”ID REDUCER...

  • Page 104: Single-Pump Gradient Programming

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4.3 Single-Pump Gradient A single-pump gradient program is based on either pressure or flow, and controlled by either time duration (in minutes) or rate Programming of change (units per minute).
  • Page 105 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes FILE# 1 STEP# 1 STORE TO EXIT 1. INIT = 0PSI 3. RATE = 0:00PSI/MIN 2. FINAL = 0PSI 4. DURATION = 1.0MIN INSERT DELETE FILE# 1...

  • Page 106: Dual Pump Concentration Gradient Programming

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4.4 Dual Pump Two-pump concentration gradients enable proportionate use of two different fluids that combine at the mixer (refer to Concentration Figures 4-3 and 4-4). Gradient Programming This type of pumping uses flow mode (FG) only.
  • Page 107 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes ENTER FLOWRATE 0.00000 XX.00000 FLOWRATE PREVIOUS 5. To proceed to the programming screen, press STEP FWD (B). The programming screen will appear, with the file number and step number at the top of the screen.

  • Page 108: Review, Revise, & Hold Options

    D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes The flow rates and ramp rate for Pump A in each step will be in direct opposite proportion to the values set for Pump B (INIT%B, FIN%B, and RATE).
  • Page 109 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes GRADIENT ACTION=HOLD FINAL VALUE NEXT_ACTION PREVIOUS To scroll through the four options, press NEXT_ACTION (A). When you have reached the desired option, press PREVIOUS (D) to save and exit.
  • Page 110 D Series Syringe Pumps Section 4 Gradient Pumping for Pressure, Flow, and Concentration Modes 4-14...

  • Page 111: Section 5 Continuous Flow Introduction, Installation, & Operation

    Section 5 Continuous Flow Introduction, Installation, & Operation 5.1 Introduction A D Series continuous flow pumping system consists of two syringe pumps and a valve accessory package regulated by one controller. This system allows you to continuously deliver liq- uefied gas or liquid under constant flow or constant pressure mode.

  • Page 112: Check Valve Technical Specifications

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation fittings already attached. The only connections you have to make are between the pump tubing and the double check valve housings and between the outlet and inlet tubing and the tees.

  • Page 113: Inlet Tubing

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation  " nuts and ferrules to attach to the double check valve housings. 4. Attach the inlet tubing assembly. The tubing you use depends upon whether or not your source is pressurized.

  • Page 114: Check Valve Package Installation: 65Dm/100D/265D/500D Pumps

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Figure 5-1 Check valve package installation: 65DM/100D/265D/500D pumps...

  • Page 115: Continuous Flow Check Valve Package For 100D/260D /500D, Part #68-1247-059

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Table 5-2 Continuous Flow Check Valve Package for 100D/260D /500D, part #68-1247-059 Qty. Part Number Description  3 loose 209-0169-41 " ferrule  3 loose 209-0169-27 " nut ...

  • Page 116: Continuous Flow Check Valve Package For 1000D, Part #68-1247-128

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Outlet Tee 1/4” 1000D Connector (2) Plug Check Valve, 1/4 " Conn (4) Plug Inlet Tee Figure 5-2 Check valve package installation: 1000D pump Table 5-3 Continuous Flow Check Valve Package for 1000D, part #68-1247-128 Qty.

  • Page 117: Continuous Flow Air Valves

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation 5.3 Continuous Flow Air Air valves generally open and close faster and are less prone to error and component wear, making them suitable for industrial Valves use and other applications where the system will be constantly running;...
  • Page 118 D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation DANGER RISK OF INJURY. THE PRESSURE PRODUCED COULD BE 700 BAR. PLEASE UTILIZE APPROPRIATE TUBING AND CONNECTIONS NOTED IN THE MANUAL. 3. Loosely attach the tubing lengths from the valve assembly to the pumps.

  • Page 119: Air Valve Installation For 65Dm, 100Dm/Dx, 260D, And 500D Pumps

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Optional reducing Optional reducing fitting (for ” fitting (for ” Outlet Outlet ” nut and ferrule ” nut and ferrule (100/260D), or male (100/260D), or male ” ”...

  • Page 120: Air Valve Installation For 500Hpx Pumps

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Outlet Pre-swaged 3/8" male connector tubing Mounting plate Inlet (customer reservoir) Air supply #4 Panhead screws (4) Wire pair conversion table for A-B Pump Pair and C-D Pump Pair...

  • Page 121: Air Valve Installation For 1000D Pump

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Outlet Mounting plate Pressure transducer cap Cylinder head Valve (2) Tee fitting (2) Air tubing Actuator to vale Check valve upply Inlet from eservoir Control Panel Rear W i r e p a i r c o n -...

  • Page 122: Air Valve Installation For 65D Pump

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation TOP VIEW Outlet Pressure transducer (2) Cylinder head (2) Valve (2) Tee fitting (2) Air tubing to valve Actuator Check valve Inlet from reservoir Control Panel Rear Wire pair conversion table for A-B Pump Pair and C-D Pump Pair...

  • Page 123: Continuous Flow Electric Valves

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation 5.4 Continuous Flow Electric valves, which provide the best positive valve closure, are most commonly used in liquefied gas applications. Electric valves Electric Valves require the pump controller to be equipped with the valve driver board.

  • Page 124: Dual Electric Valve Installation

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation 5.4.2 Dual Electric Valve To install the electric valve package (refer to Figure 5-7 on the Installation following page): 1. Position the valve bases 1.3 cm apart. 2. Use the plugs to stopper the ports that will not be con- nected.

  • Page 125: Electric Valve Installation

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Figure 5-7 Electric valve installation 5-15...

  • Page 126: User Supplied Valves

    • Check valves Do not use spring-loaded check valves if refilling at atmospheric pressure; the pump seals are not designed to draw against a vacuum. The balls in Teledyne Isco check valves are closed by gravity. • Powered valves These are electrically triggered from the pump controller and could be air or electrically actuated.

  • Page 127: Continuous Flow Mode

    You must operate the two pumps manually for initial setup, i.e. refill and purging of air. If the Teledyne Isco air valve package is used, the air valves are switched through ACCESS CTRL. When air valves are used, lights on the air valve actuator indicate which valves are open.

  • Page 128: Constant Flow Mode

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation CHECK VALVES MORE ELECTRIC ELECTRIC PREVIOUS Press 3x to return VALVE to run screen Figure 5-8 Keystrokes to specify valve type Note In older controller versions, only buttons 1 (...

  • Page 129: Constant Pressure Mode

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation CONTIN CONST FLOW ‘1’ will blink MORE PREVIOUS Starts Press 3x to operation return to run MULTI PUMP screen 1. AB Pumps 2. CD Pumps Figure 5-10 Keystrokes to set up constant flow 5.6.3 Constant Pressure...

  • Page 130: No Check Valve

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation 5.6.4 No Check Valve To limit fluid backflow from the pump to the supply reservoir one of two approaches is generally used. Either a check valve is installed in the supply line or the N...

  • Page 131: To Run Or Stop

    D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation 5.6.5 To Run or Stop This menu setting allows the operator to run or stop both pairs of pumps simultaneous. REVIOUS Press 3x to return to run screen...
  • Page 132 D Series Syringe Pumps Section 5 Continuous Flow Introduction, Installation, & Operation Liquefied Gases Checklist: 1. Open the valves to atmosphere by pressing , then ACC CTRL selecting each valve to open. 2. Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero.

  • Page 133: Section 6 Modifier Addition

    D Series Syringe Pumps Section 6 Modifier Addition 6.1 Overview Pumping systems using a modifier (usually a solvent) may have different configurations, depending on the application, including: • Two separate pumps delivering a mixture of super- critical fluid and modifier to one or more user-provided extractors.

  • Page 134: Modifier Addition Kit Installation (Two-Pump Configuration)

    D Series Syringe Pumps Section 6 Modifier Addition Note Tighten fittings just enough to hold tubing in place. Final tight- ening will be done after all tubing and fittings are connected. The following installation steps refer to Figure 6-1 (independent pumps) or Figure 6-2 (continuous flow system).

  • Page 135: Modifier Addition Kit For Two Pumps (Part #68-1247-079)

    D Series Syringe Pumps Section 6 Modifier Addition Table 6-1 Modifier Addition Kit for Two Pumps (part #68-1247-079) Description Part Number Description Part Number Description Part Number  Tee union fitting 209-0169-47 ” nut (4) 209-0169-27 Check valve cartridge 209-0161-80 ...

  • Page 136: Modifier Mode Setup

    D Series Syringe Pumps Section 6 Modifier Addition Table 6-2 contains modifier addition components for connecting to a continuous flow system. Table 6-2 Modifier Addition Components for Continuous Flow System Description Part Number  Tee union fitting ” 209-0169-47 Check valve cartridge...

  • Page 137: Two Pump Operation

    D Series Syringe Pumps Section 6 Modifier Addition 5. Open the inlet valves of each pump. 6. Run both pumps empty. 7. Zero the pressure on each pump. 8. Reconnect the pump A inlet tubing to the inlet valve. To fill pump B with 1.

  • Page 138: Programming

    D Series Syringe Pumps Section 6 Modifier Addition Once pump A has reached the set pressure, the controller will enter a hold mode and wait for a pressure drop. The start of EQUILIBRATION is signaled by opening the extractor inlet, or pressing RUN.

  • Page 139: Mininum Modifier Pressure Setting

    D Series Syringe Pumps Section 6 Modifier Addition 6.2.1 Mininum Modifier The default setting for the minimum modifier pump pressure is Pressure Setting 50PSI. This can be changed to a value appropriate for the type of modifier being used. If there is no need to change minimum pressure, press PRE- (D) three times to return to the main menu.

  • Page 140: Refilling

    D Series Syringe Pumps Section 6 Modifier Addition 8. Open the outlet valves of both pumps if they are not open. 9. Press RUN. 10. When the pressure for Pump A is established, the message “HOLD: PRESS RUN” will be displayed.
  • Page 141 D Series Syringe Pumps Section 6 Modifier Addition 11. Immediately open the extractant outlet valve(s). Note Flow MUST be established through the system at or before the time EQUILIBRATE is displayed. To properly equilibrate the pumps, they must be delivering fluid.
  • Page 142 D Series Syringe Pumps Section 6 Modifier Addition 6-10...

  • Page 143: Section 7 Modbus Configuration

    Modbus Application Protocol Vol. 1 Modbus Over Serial Line Vol. 1 Modbus Messaging on TCP/IP. The Isco D Series Syringe pump controller supports the Modbus RTU and Modbus TCP/IP protocols. 7.1.1 Modbus RTU The Modbus RTU protocol implementation uses a 2-wire RS-485 connection.

  • Page 144: Modbus Tcp/Ip

    D Series Syringe Pumps Section 7 Modbus Configuration 7.1.2 Modbus TCP/IP The modbus TCP/IP protocol implementation uses an ethernet connection. The ethernet connections are located on the optional DB25 connector labeled USB/Ethernet. Use optional cable (PN 60-1244-488) and coupler (PN 14-9905-200) to connect to your Ethernet.

  • Page 145: Supported Modbus Function Codes

    D Series Syringe Pumps Section 7 Modbus Configuration Table 7-2 Modbus RTU Configuration Options Even 1 Stop Bit, Odd 1 Stop Bit, Communication parameters Parity None 1 Stop Bit, None 2 Stop (Default Even 1 Stop Bit) Word order for 32-bit integers...

  • Page 146: Coils

    D Series Syringe Pumps Section 7 Modbus Configuration Table 7-5 Coils Register Address Type Size Description 00001 1 BIT 0: Stop Pump A 1: Run Pump A 00002 1 BIT 0: Stop Pump B 1: Run Pump B 00003 1 BIT...
  • Page 147 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-5 Coils (Continued) Register Address Type Size Description 00038 1 BIT 1: Pump C is Equilibrating 00039 1 BIT 1: Pump D is Equilibrating 00040 1 BIT 1: Pump A is in Hold (clock stopped)
  • Page 148 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-5 Coils (Continued) Register Address Type Size Description 00078 1 BIT 0: DIGITAL OUTPUT BIT 8 HIGH 1: DIGITAL OUTPUT BIT 8 LOW 0: Disable Dispense Mode A 1: Enable Dispense Mode A Only configure if in Constant Flow...

  • Page 149: Holding Registers

    D Series Syringe Pumps Section 7 Modbus Configuration Table 7-5 Coils (Continued) Register Address Type Size Description 00115 1 BIT 1: Motor failure Pump A 00116 1 BIT 0: Transducer of Pump B not connected 1: Transducer of Pump B connected...
  • Page 150 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-6 Holding Registers (Continued) Read/ # of Register Address Type Description Units Write Registers Pressure set-point for multi-pump pair AB in 40009 FLOAT ATM; BAR; kPa; PSI See NOTE 1. Continuous Flow Constant Pressure mode.
  • Page 151 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-6 Holding Registers (Continued) Read/ # of Register Address Type Description Units Write Registers Maximum flow limit in Constant Pressure 40071 FLOAT ml/min; ml/hr; ul/min; ul/hr See NOTE 2. mode for Pump D.
  • Page 152 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-6 Holding Registers (Continued) Read/ # of Register Address Type Description Units Write Registers Volume that Pump C will be refill to if AUTO 40129 FLOAT milliliters FILL TO C is ON.
  • Page 153 D Series Syringe Pumps Section 7 Modbus Configuration Table 7-6 Holding Registers (Continued) Read/ # of Register Address Type Description Units Write Registers 40211 FLOAT Absolute maximum flow rate for Pump B. ml/min; ml/hr; ul/min; ul/hr See NOTE 2. 40213 FLOAT Absolute maximum refill rate for Pump B.
  • Page 154 D Series Syringe Pumps Section 7 Modbus Configuration 7-12...

  • Page 155: Section 8 Serial Interface

    D Series Syringe Pumps Section 8 Serial Interface 8.1 Overview The Teledyne Isco D Series pump can be remotely controlled by a computer through a built-in RS-232-C serial or USB interface. This function is supported by the Teledyne Isco LabView™...

  • Page 156: Network Control And Communication

    Possible baud rates are 1200 and 19200. Other baud rates of 300, 1200, 2400, 4800, 9600, 19200, 38400, 57600, and 115200 are supported by the D Series pumps but are not part of the Teledyne Isco defined communications standard.

  • Page 157: Usb Interface

    The computer is always con- Control nected from the serial port to the serial port(s) of the D Series controller(s) it is controlling. Each controller is connected to its pumps in the normal fashion, i.e. the pump control cables are attached to the pump A, B, and C connectors on the rear panel of the pump controller.

  • Page 158: Two Controllers (Compiler Required)

    D Series Syringe Pumps Section 8 Serial Interface Null Modem Cable part #480-7996-00 Figure 8-1 Serial network connection example - Single connection With this configuration, your sample program is capable of: • Constant flow • Constant pressure • Gradient 8.4.2 Two Controllers To connect two controllers in the network, use the ‘Y’...

  • Page 159: Serial Control Check List

    D Series Syringe Pumps Section 8 Serial Interface 8.5 Serial Control Check In order to build and operate a custom program for Isco syringe pumps, you must have the following: List 1. Sample program (Isco LabView toolkit)* 2. LabView Compiler (purchased separately) 3.

  • Page 160: Verify Operation

    DASNET communications protocol. This protocol allows a number of instruments to be controlled from a single RS-232-C serial port. Up to seven D Series controllers may share a single serial data channel, with each controller only accepting commands that are meant for it.

  • Page 161: Universal Driver From Teledyne Isco

    TB06 Basic Operation of LabView Toolkit. A copy of the driver can be found on the CD included in the back of your D Series pump user manual. It can also be downloaded from: http://www.isco.com/products/appnotes.asp?PL=105. Open the Software Utilities folder and select Universal D-Series Pump driver to download the utility to a zip folder.

  • Page 162: Conversion Of Pump Commands To Dasnet Frames

    D Series Syringe Pumps Section 8 Serial Interface Table 8-3 Example of BASIC program to demonstrate conversion of pump commands to DASNET frames 1 CLS : Z$ = "": PRINT "INPUT ALL ENTRIES IN CAPITAL LETTERS" 5 INPUT "INPUT UNIT ID >> ", UNITNUM’GET UNIT NUMBER 30 REM OPEN COM PORT SET FOR COM2 EDIT TO COM1 IF NEED 40 OPEN "COM2:1200,N,8,1,ASC"...

  • Page 163: Conversion Of Pump Commands To Dasnet Frames

    D Series Syringe Pumps Section 8 Serial Interface Table 8-4 Example of C program to demonstrate conversion of pump commands to DASNET frames #include<stdio.h> #include<conio.h> #include "b:comm.c" /* edit to path needed */ /* a ’C’ example of DASNET serial control */ int conv_das();...

  • Page 164: Of Pump Commands To Dasnet Frames

    D Series Syringe Pumps Section 8 Serial Interface Table 8-5 Example of a Visual C++ program to demonstrate conversion of pump commands to DASNET frames // visual C++ version 10.0 // Dasnet.cpp : Defines the entry point for the console application.
  • Page 165 D Series Syringe Pumps Section 8 Serial Interface Table 8-5 Example of a Visual C++ program to demonstrate conversion of pump commands to DASNET frames (Continued) CloseHandle(hCom); printf("Comm intr released\n"); void conv_das(char *in, char *out) unsigned sum; char *c_ptr; c_ptr=out;...
  • Page 166 D Series Syringe Pumps Section 8 Serial Interface Table 8-5 Example of a Visual C++ program to demonstrate conversion of pump commands to DASNET frames (Continued) int count=0; n=strlen(out); // start of packet if(!WriteFile(hCom, "\r", 1, &dwBytesRead, NULL)) //error occurred. Report to user.
  • Page 167 D Series Syringe Pumps Section 8 Serial Interface Table 8-5 Example of a Visual C++ program to demonstrate conversion of pump commands to DASNET frames (Continued) Sleep(2000); exit(1); switch(speed) case 19200: dcbSerialParams.BaudRate=CBR_19200; break; case 38400: dcbSerialParams.BaudRate=CBR_38400; break; case 57600: dcbSerialParams.BaudRate=CBR_57600;...
  • Page 168 D Series Syringe Pumps Section 8 Serial Interface Table 8-5 Example of a Visual C++ program to demonstrate conversion of pump commands to DASNET frames (Continued) char buf[2]; buf[0]=0; /* get char if there if(!ReadFile(hCom, buf, 1, &dwBytesRead, NULL)) //error occurred. Report to user.
  • Page 169 D Series Syringe Pumps Section 8 Serial Interface • Acknowledgment is one character to indicate the success of the previous transmission. There are three possibilities: (1) E means error, resend the message immediately (E is sent by the network controller only.
  • Page 170 D Series Syringe Pumps Section 8 Serial Interface Decimal Format Using Step 1: 559 = 82 + 51 + 48 + 52 + 83 + 84 + 79 + 80 MODULO  2R47 Step 2: 47 = 559 · · 256 ...
  • Page 171 D Series Syringe Pumps Section 8 Serial Interface All the parameters are as previously described except message destination. Message destination is the 1-digit identification number of the unit that the message is sent to. An example of a typical data exchange is summarized below. For illustration, we will assume the network consists of a computer serving as a combination network controller and master.
  • Page 172 D Series Syringe Pumps Section 8 Serial Interface this example, the master and the network controller are a single unit. If they were separate units, the master would send the inquiry to the network controller; then the network controller would send the message to the slave unit the next time it is polled.
  • Page 173 Commands must be in uppercase letters. The network definition allows multiple commands in a message field when delimited by semicolons, but the D Series controller is limited to single commands. It will respond with a PROBLEM=INVALID COMMAND message.

  • Page 174: Serial Commands For The D Series Pump

    D Series Syringe Pumps Section 8 Serial Interface 8.8 Serial Commands for Table 8-6 is a list of the serial commands recognized by the pump. These commands are the message part of the DASNET the D Series Pump protocol. The operand always follows the equals sign. The REMOTE command must be sent once, before any command that changes the operation of the pump will be accepted.
  • Page 175 D Series Syringe Pumps Section 8 Serial Interface Table 8-6 Serial Commands (Continued) Command Description DIG CONTROL Returns the status of the digital output control bits as either REMOTE (R) or INTER- NAL (I). The return message format is DIG CONTROL=xxxxxx, where “x” is either “R”...
  • Page 176 D Series Syringe Pumps Section 8 Serial Interface Table 8-6 Serial Commands (Continued) Command Description INDEPENDENT Put pumps in Independent mode. INDEPENDENTCD IPUMPA=1, IPUMPA=0 Turns the pressure integral control On and Off for the pump indicated. IPUMPB=1, IPUMPB=0 1 = ON...
  • Page 177 D Series Syringe Pumps Section 8 Serial Interface Table 8-6 Serial Commands (Continued) Command Description MAXPRESSA Returns the maximum pressure setpoint. MAXPRESSB MAXPRESSC MAXPRESSD MFLOWA=# Enter # to designate the maximum flow limit in constant pressure mode. MFLOWB=# MFLOWC=# MFLOWD=# MFLOWA Returns the maximum flow limit setpoint.
  • Page 178 D Series Syringe Pumps Section 8 Serial Interface Table 8-6 Serial Commands (Continued) Command Description PRESSCNTRLDIFF1 Sets the pressure control input to Analog input 1, with a pressure range of 50 psi. PRESSCNTRLDIFF1=XXXXX Sets the pressure control input to Analog input 1 and sets the pressure range. The range is 1 to 5000.

  • Page 179: Get Status Command

    D Series Syringe Pumps Section 8 Serial Interface Table 8-6 Serial Commands (Continued) Command Description SETPRESSA Returns the pressure setpoint. SETPRESSB SETPRESSC SETPRESSD STATUSA Returns with status of pump. May be any combination of responses listed below. STATUSB STATUSC STATUSD...

  • Page 180: Get Status String "G" Command

    D Series Syringe Pumps Section 8 Serial Interface R046=37510,-00128, 01017, 06981, 05743, 00421, 00442, 00449,11111000,CS Pressure Pump A Pressure Pump B Digital Inputs 1—8 Pressure Pump C 1 = High Units = (psi*5) 0 = Low Resolution = 0.2 psi ALOG1 —...

  • Page 181: Get All Status String "G&" Command

    D Series Syringe Pumps Section 8 Serial Interface Figure 8-5 Get All Status String “G&” Command 8-27...

  • Page 182: Get All Status Strings From Four Pump Operation "G&2" Command

    D Series Syringe Pumps Section 8 Serial Interface Figure 8-6 Get all status strings from four pump operation “G&2” Command 8-28...

  • Page 183: Gradient Download Command

    D Series Syringe Pumps Section 8 Serial Interface 8.8.2 Gradient Download This command downloads a step from the D Series pump to the Command PC. This command will respond with “PROBLEM=INVALID COMMAND” if the file or step does not exist. If the file and step is valid, the controller will respond as shown in Figures 8-7 and 8-8.

  • Page 184: Gradient Download Commands - Two Pump Flow Gradient

    D Series Syringe Pumps Section 8 Serial Interface Step Number 01 LGUL,F:xx,S:01,FL:xxx.xxxx,IB%:xx.xx,FB%:xx.xx,D:xxxx.x, Gradient Duration Range = (0000.1 – 9999.0 minutes) Final %B Range = (00.00 – 100.0) Initial %B Range = (00.00 – 100.0) Gradient Total Flow Rate Units = milliliters/minute Range = (000.0000 –...

  • Page 185: Gradient Upload Commands - Single Pump Flow Gradient

    D Series Syringe Pumps Section 8 Serial Interface Step Number 01: LGUL,F:xx,S:01,FL:xxx.xxxx,I %:xx.xx,F %:xx.xx,D:xxxx.x, Gradient Duration Range = (0000.1 – 9999.0 minutes) Final Gradient Percentage Range = (00.00 – 100.0) Initial Gradient Percentage Range = (00.00 – 100.0) Gradient Total Flow Rate Units = milliliters/minute Range = (000.0000 –...

  • Page 186: Gradient Upload Commands - Two Pump Flow Gradient

    D Series Syringe Pumps Section 8 Serial Interface Step Number 01 LGUL,F:xx,S:01,FL:xxx.xxxx,IB%:xx.xx,FB%:xx.xx,D:xxxx.x, Gradient Duration Range = (0000.1 – 9999.0 minutes) Final %B Range = (00.00 – 100.0) Initial %B Range = (00.00 – 100.0) Gradient Total Flow Rate Units = milliliters/minute Range = (000.0000 –...

  • Page 187: Range Command

    D Series Syringe Pumps Section 8 Serial Interface LGUL,F:xx,S:xx,I:xxxxx,F:xxxxx,D:xxxx.x, Pressure Duration Range = 0000.1 – 9999.0 minutes Final Pressure Range = 00010 – Maximum Units = psi Initial Pressure Range = 00010 – Maximum Units = psi Step Number (01 – 99) File (01 –...

  • Page 188: Error Messages

    D Series Syringe Pumps Section 8 Serial Interface 8.8.5 Error Messages If an error occurs in a message, one of the following responses w i l l b e s e n t . T h e f o r m a t o f a n e r r o r m e s s a g e i s “PROBLEM=_____.”...

  • Page 189: Section 9 Pump Maintenance, Troubleshooting, And Servicing

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing DANGER RISK OF ELECTRIC SHOCK - DISCONNECT THE ELECTRIC POWER BEFORE SERVICING. ONLY TRAINED SERVICE PERSONNEL MAY REMOVE THE CASE TOP. DANGER RISQUE DE CHOC ÉLECTRIQUE. COUPER L´ALIMENTATION AVANT LA RÉPARATION.

  • Page 190: Service Department

    · Do not return the pump without first providing written guarantee that it has been decontaminated of hazardous or potentially lethal materials. · Teledyne Isco reserves the right to refuse shipment if no decontamination assurance has been provided prior to shipment. Failure to decontaminate a pump may result in legal action taken by state or federal authorities.

  • Page 191: Maintenance Kits

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.2 Maintenance Kits Maintenance kits are available for all pump models, for use in many maintenance and servicing tasks. Table 9-1 summarizes major kit components. Table 9-2 contains part numbers for each kit.

  • Page 192: General Cleaning

    The 500HPx contains an inlet fan to cool the motors. Teledyne Isco recommends inspecting and cleaning, if necessary, the inlet fan filter on the 500HPx every six months.
  • Page 193 D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 4. Release the key and turn the controller CLEAR ENTRY switch back to STANDBY 5. Turn the controller switch back to , and perform the Basic Reset, as described above.

  • Page 194: Diagnostic Menu

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.5 Diagnostic Menu The syringe pump controller can run a number of system tests that are initialized using the keypad. MORE MORE DIAGNOSTIC MENU 1. LCD TEST 4. KEYPAD TEST 2.

  • Page 195: Keypad Test

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.5.3 KEYPAD TEST The screen will briefly display the name of each key pressed. Press (D) to return to the diagnostic menu. EXIT 9.5.4 MOTOR Tests the digital position controls.

  • Page 196: Serial Test

    If the unit passes the internal port test, next perform the I/O test. Use a null-modem cable (available from Teledyne Isco, part #480-7996-00) to connect the 9-pin serial output port of a com- puter to the RS-232-C port, as shown on the following page.

  • Page 197: Removing The Case Top

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Open a terminal emulator program such as HyperTerminal (©Hilgraeve, Inc. Monroe, MI). The factory default port settings are: BPS - 9600. Baud rate should match controller setting (refer to Section 8.2)

  • Page 198: Pump Case Top Removal

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Figure 9-6 Controller case top screws (2 of 4 shown) 9.6.2 Pump Case Top Some maintenance and troubleshooting procedures require Removal accessing the pump module interior. Remove the four screws holding the case top in place (two screws on each side).

  • Page 199: Test Points

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.7 Test Points The following sections contain tables listing the most commonly used test points and their voltages. Refer to the controller sche- matic and the pump schematic (available online on our Web site).

  • Page 200: Lubrication

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.8 Lubrication The pump is a precision engineered instrument that must be lubricated every two years or every 6,000 strokes (whichever comes first) to ensure proper service life. The pump has an easy-to-access lube wheel that keeps the main gears lubricated during operation.

  • Page 201: Seal Cleaning And Replacement

    4. Unscrew the cylinder using either a strap wrench or the clamp and wrench in the Teledyne Isco wrench package (60-1247-130 for 65D and 65DM, 60-1247-067 for 100DM, 100DX, and 260D; 68-1247-068 for 500D; 60-1247-145 for 500HPx;...

  • Page 202: Piston Seal (Excludes 30D)

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 5. Once the cylinder has been unscrewed, lift it straight up and off the piston and the push tube. CAUTION Do not tilt the cylinder while removing it. Seal damage can result.

  • Page 203: All Other Piston Seals

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 5. Install the cylinder over the piston assembly, again, and screw onto the mounting block. 6. Leak test the pump. Model 1000D - Refer to Replacement Parts Listing 60-1242-347...

  • Page 204: Piston Wrench Tools

    Isco wrench package in the round hole on the side of the piston. Teledyne Isco has piston wrench tools, which are also included in the wrench packages for each model of pump. Refer to Table 9-3 on the following page.

  • Page 205: Wear Ring Cleaning And Replacement

    Although the wear ring does not routinely need to be replaced, occasionally it becomes worn or damaged, depending on how the and Replacement pump has been used. Teledyne Isco recommends that when replacing the seal or cleaning the piston, check the wear ring for any signs of deterioration.

  • Page 206: Liquid Solvent Changeover And Flushing

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 7. Cycle the pump between REFILL and RUN a few times, opening and closing the appropriate valves at the proper time to purge any remaining gas from the pump. Use about 10 - 20 mls per stroke to purge.

  • Page 207: Shear Key

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing In the event of a shear key failure, the pump will sound as though it is turning, but the piston will not move up the cylinder. When this occurs, the pump motor will not stop automatically.

  • Page 208: Replacement Using Installation Tool

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Spacer Ball Screw Access Plate Cotter Pin Castle Nut Figure 9-10 Accessing the shear key Shear Key shear key for shear key for all 65DM other models Locking Pin Figure 9-11 Shear key replacement 9.12.2 Replacement Using...

  • Page 209: Replacement Without Installation Tool

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 1. Insert tool into ball screw so that the slot on ball screw and tool are lined up, then lock with locking pin. 2. Rotate the ball screw until the broken halves of shear key are realigned (Figure 9-11).

  • Page 210: Completion Of Shear Key Replacement

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Figure 9-12 30D and 65DM Bearing set Note that the 30D and 65DM spacer is shaped differently from that of the other pumps, and must be properly oriented during reinstallation, Figure 9-13.

  • Page 211: Motor Brushes

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing b. For all other models, torque to 250 in-lbs (28 N-m). 3. Loosen the nut until it can be turned by hand. Tighten the nut finger tight. 4. Torque the castle nut to 100 in-lbs.

  • Page 212: D Series Motor Brush Replacement

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Quick Disconnect / Motor Brush Retainer (one of two) Figure 9-14 D Series motor brush replacement Note Parts for Configuration 1 and Configuration 2 are not inter- changeable. Figure 9-15 Location of motor brushes A new brush is 1.1 cm long.

  • Page 213: Motor Brush Disassembly

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 1. Unscrew the brush retainer from the motor using a straight edge screwdriver. 2. Pull the brush out of the slot and measure its length. If it is nearing 0.4 cm, replace both brushes.

  • Page 214: Hpx Motor Brush Replacement

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.13.2 HPx Motor Brush This section goes through the various steps needed to replace the Replacement HPx motor brush. The following tools are required: • #2 Phillips screwdriver • Flat-blade screwdriver •...

  • Page 215: Two Pin Connector

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 4. Unplug the two pin connector (Figure 9-21). Figure 9-21 two pin connector 5. Unplug connector from the encoder by carefully pulling down on the connector. Figure 9-22 Encoder...

  • Page 216: Location Of Screws And Washers Holding The Motor In Place

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 6. Remove the three screws and three flat washers that hold the motor plate onto the bearing plate. Two of the screws are on top and the third screw is down below the fan (Fig- ure 9-23).

  • Page 217: Support Plate

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Support Plate Figure 9-25 Support plate Note Make a note of the position of the two orange and two black wires connected to the motors. Marking them “Top” and “Bot- tom”...

  • Page 218: Set Screws Holding The Two Negative Brushes

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 10. Leaving the wires connected to the terminals, use a flat-blade screwdriver and remove the set screws holding the two Negative (-) brushes (black wires) into the motors. Set Screws Figure 9-28 Set screws holding the two negative brushes 11.

  • Page 219: Connector Connected To The Brush

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 12. Connect the bottom black wire to the new brush and insert the new brush into the motor using the connector as lever- age to guide brush into the motor. Hold the connector so the brush is fully engaged into the motor (Figure 9-30)then reinstall the set screw that holds brush in place.

  • Page 220: Loosen The Connector

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Figure 9-32 Loosen the connector 15. Connect the bottom orange wire to the new brush and insert the new brush into the motor using the connector as leverage to guide brush into the motor. Hold the connector so the brush is fully engaged into the motor (Figure 9-33) then reinstall the set screw that holds brush in place.

  • Page 221: Location Of Locating Pins

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Locating Pin Figure 9-34 Location of locating pins 3. Once the motor plate is located properly over the two locat- ing pins install the three screws and three flat washers to hold motor in place and tighten the screws (Figure 9-23).

  • Page 222: Motor Plate And Bearing Plate

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Make sure the ferrite beads are not pinched in these areas Figure 9-35 Motor plate and bearing plate 8. Once it has been determined that all wires are clear of...

  • Page 223: Calibrations

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing on the shaft carefully pry up on the capacitor until it no longer makes contact. No contact allowed between the capacitor and the motor shaft Figure 9-37 Capacitor and motor shaft 9.14 Calibrations...
  • Page 224 D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 1. Disconnect the instrument from mains power. 2. Disconnect the pressure transducer cable from the pump, and remove the tubing from the inlet and outlet ports. 3. Loosen the four cover screws and remove the front and rear covers of the pump.

  • Page 225: Limit Sensor Replacement

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Figure 9-38 Limit sensor replacement Figure 9-39 Installing the plastic mounts 9-37...
  • Page 226 8. (Not 30D) Be sure that the cylinder is unscrewed several turns. If you need to use a wrench, we recommend a strap wrench or wrenches in the Teledyne Isco wrench package (P/N 68-1247-067 for 100DM, 100DX, an d 260D; P/N 68-1247-068 for 500D;...

  • Page 227: Limit Sensor Calibration (Excludes 30D)

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9.14.4 Limit Sensor Once the new limit sensor assembly is installed, the sensors Calibration must be calibrated. Before calibrating the limit sensors, be sure (Excludes 30D) the cylinder is unscrewed several turns. Follow steps 8-10 in the previous section (9.14.3).

  • Page 228: Limit Sensor Calibration

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 24. Install the covers. 9.14.5 30D Limit Sensor The following steps are for the 30D limit sensor calibration: Calibration 1. Disconnect the mains power and the transducer cable from the cylinder cap.

  • Page 229: Electric Valve Motor Calibration

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 25. If the clearance is not between 0.025” and 0.050” (0.6-1.3 mm), loosen the screw holding the interrupter and move the interrupter S . Repeat steps 22-25. LIGHTLY 26. Set both the R...

  • Page 230: Electric Valve Motor Voltage

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing Calibration Voltage Value Figure 9-40 Electric valve motor voltage 2. Inside the controller, attach the leads of a voltmeter across resistor R204 on the electric valve interface board. 3. Press ) >...

  • Page 231: Electric Valve Motor Adjustment

    D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing B Out A In A Out B In A Out B Out B In A In Figure 9-41 Electric valve motor adjustment 9-43...
  • Page 232 D Series Syringe Pumps Section 9 Pump Maintenance, Troubleshooting, and Servicing 9-44...

  • Page 233: Appendix A Replacement Parts

    Replacement parts are called out in the following illustrations. Refer to the call-out in the adjacent table to determine the part number for the item. Replacement parts can be purchased by contacting Teledyne Isco’s Customer Service Department. Teledyne Isco Customer Service Department P.O.

  • Page 234: D Series Controller

    D Series Syringe Pumps Appendix A Replacement Parts A.1.1 D Series Controller...
  • Page 235 D Series Syringe Pumps Appendix A Replacement Parts...
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  • Page 237: 1000D Pump

    D Series Syringe Pumps Appendix A Replacement Parts A.1.2 1000D Pump...
  • Page 238 D Series Syringe Pumps Appendix A Replacement Parts...
  • Page 239 D Series Syringe Pumps Appendix A Replacement Parts...
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  • Page 241: Dx Pump

    D Series Syringe Pumps Appendix A Replacement Parts A.1.3 500D/DX Pump...
  • Page 242 D Series Syringe Pumps Appendix A Replacement Parts A-10...
  • Page 243 D Series Syringe Pumps Appendix A Replacement Parts A-11...
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  • Page 245: 500Hpx Pump

    D Series Syringe Pumps Appendix A Replacement Parts A.1.4 500HPx Pump A-13...
  • Page 246 D Series Syringe Pumps Appendix A Replacement Parts A-14...
  • Page 247 D Series Syringe Pumps Appendix A Replacement Parts A-15...

  • Page 248: 100Dm/Dx And 260D Pumps

    D Series Syringe Pumps Appendix A Replacement Parts A.1.5 100DM/DX and 260D Pumps A-16...
  • Page 249 D Series Syringe Pumps Appendix A Replacement Parts A-17...
  • Page 250 D Series Syringe Pumps Appendix A Replacement Parts A-18...
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  • Page 252: Pump

    D Series Syringe Pumps Appendix A Replacement Parts A.1.6 65D Pump A-20...
  • Page 253 D Series Syringe Pumps Appendix A Replacement Parts A-21...
  • Page 254 D Series Syringe Pumps Appendix A Replacement Parts A-22...
  • Page 255 D Series Syringe Pumps Appendix A Replacement Parts A-23...
  • Page 256 D Series Syringe Pumps Appendix A Replacement Parts A-24...
  • Page 257 D Series Syringe Pumps Appendix A Replacement Parts A-25...
  • Page 258 D Series Syringe Pumps Appendix A Replacement Parts A-26...
  • Page 259 D Series Syringe Pumps Appendix A Replacement Parts A-27...
  • Page 260 D Series Syringe Pumps Appendix A Replacement Parts A-28...
  • Page 261 D Series Syringe Pumps Appendix A Replacement Parts A-29...
  • Page 262 D Series Syringe Pumps Appendix A Replacement Parts A-30...
  • Page 263 D Series Syringe Pumps Appendix A Replacement Parts A-31...
  • Page 264 D Series Syringe Pumps Appendix A Replacement Parts This page intentionally blank A-32...

  • Page 265: 65Dm

    D Series Syringe Pumps Appendix A Replacement Parts A.1.7 65DM A-33...
  • Page 266 D Series Syringe Pumps Appendix A Replacement Parts A-34...
  • Page 267 D Series Syringe Pumps Appendix A Replacement Parts A-35...
  • Page 268 D Series Syringe Pumps Appendix A Replacement Parts A-36...
  • Page 269 D Series Syringe Pumps Appendix A Replacement Parts A-37...
  • Page 270 D Series Syringe Pumps Appendix A Replacement Parts A-38...
  • Page 271 D Series Syringe Pumps Appendix A Replacement Parts A-39...
  • Page 272 D Series Syringe Pumps Appendix A Replacement Parts A-40...
  • Page 273 D Series Syringe Pumps Appendix A Replacement Parts A-41...
  • Page 274 D Series Syringe Pumps Appendix A Replacement Parts A-42...
  • Page 275 D Series Syringe Pumps Appendix A Replacement Parts A-43...
  • Page 276 D Series Syringe Pumps Appendix A Replacement Parts A-44...
  • Page 277 D Series Syringe Pumps Appendix A Replacement Parts A-45...
  • Page 278 D Series Syringe Pumps Appendix A Replacement Parts A-46...

  • Page 279: Power Circuit Board

    D Series Syringe Pumps Appendix A Replacement Parts A.1.8 Power Circuit Board A-47...
  • Page 280 D Series Syringe Pumps Appendix A Replacement Parts A-48...
  • Page 281 D Series Syringe Pumps Appendix A Replacement Parts A-49...
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  • Page 283: Analog Output Circuit Board

    D Series Syringe Pumps Appendix A Replacement Parts A.1.9 Analog Output Circuit Board A-51...
  • Page 284 D Series Syringe Pumps Appendix A Replacement Parts A-52...

  • Page 285: Interface Circuit Board

    D Series Syringe Pumps Appendix A Replacement Parts A.1.10 Interface Circuit Board A-53...
  • Page 286 D Series Syringe Pumps Appendix A Replacement Parts A-54...

  • Page 287: Dual Electric Valve Package

    D Series Syringe Pumps Appendix A Replacement Parts A.1.11 Dual Electric Valve Package A-55...
  • Page 288 D Series Syringe Pumps Appendix A Replacement Parts A-56...

  • Page 289: Single Electric Valve Package

    D Series Syringe Pumps Appendix A Replacement Parts A.1.12 Single Electric Valve Package A-57...
  • Page 290 D Series Syringe Pumps Appendix A Replacement Parts A-58...

  • Page 291: Sst Dual Air Valve Package For 100/260D/500D

    D Series Syringe Pumps Appendix A Replacement Parts A.1.13 SST Dual Air Valve Package for 100/260D/500D 65DM, 100DM/DX, 260D, & 500D AIR VALVE PACKAGE Note This valve system is for use with 65DM, 100D, 100DX, 260D, and 500D pumps. This air valve will n o t w o r k w i t h 6 5 D pumps.
  • Page 292 D Series Syringe Pumps Appendix A Replacement Parts A-60...

  • Page 293: Sst Dual Air Valve Package For 1000D

    D Series Syringe Pumps Appendix A Replacement Parts A.1.14 SST Dual Air Valve Package for 1000D A-61...
  • Page 294 D Series Syringe Pumps Appendix A Replacement Parts A-62...

  • Page 295: Single Air Valve Package

    D Series Syringe Pumps Appendix A Replacement Parts A.1.15 Single Air Valve Package A-63...
  • Page 296 D Series Syringe Pumps Appendix A Replacement Parts A-64...

  • Page 297: Dual Air Valve Package For 500Hpx

    D Series Syringe Pumps Appendix A Replacement Parts A.1.16 Dual Air Valve Package for 500HPx A-65...
  • Page 298 D Series Syringe Pumps Appendix A Replacement Parts A-66...

  • Page 299: Dual Check Valve Package For 100/260/500D

    D Series Syringe Pumps Appendix A Replacement Parts A.1.17 Dual Check Valve Package for 100/260/500D A-67...
  • Page 300 D Series Syringe Pumps Appendix A Replacement Parts A-68...

  • Page 301: Dual Check Valve Package For 1000D

    D Series Syringe Pumps Appendix A Replacement Parts A.1.18 Dual Check Valve Package for 1000D A-69...
  • Page 302 D Series Syringe Pumps Appendix A Replacement Parts A-70...

  • Page 303: Single Check Valve Package

    D Series Syringe Pumps Appendix A Replacement Parts A.1.19 Single Check Valve Package A-71...
  • Page 304 D Series Syringe Pumps Appendix A Replacement Parts A-72...
  • Page 305 D Series Syringe Pumps Appendix A Replacement Parts A-73...
  • Page 306 D Series Syringe Pumps Appendix A Replacement Parts A-74...

  • Page 307: Appendix B Continuous Flow Introduction, Installation, And Opera- Tion For 30D

    Appendix B Continuous Flow Introduction, Instal- lation, and Operation for 30D B.1 Introduction A D Series continuous flow pumping system consists of two syringe pumps and a valve accessory package regulated by one controller. This system allows you to continuously deliver liq- uefied gas or liquid under constant flow or constant pressure mode.

  • Page 308: Dual Air Valve Installation

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D Table B-1 Continuous Flow Technical Specifications-Air Valves: Pressure fluctuation 34.5 bar at system backpressures from 500 psi (34.5 bar) at switch over to the single pump maximum.

  • Page 309: Air Valve Installation For 30D Pump

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D Outlet Tee Inlet Tee Inlet Filter Air Inlet Tubing Wire Pair ConversionTable for A-B Pump Pair A-B Pump Digital +15 Wires Wire Pair Output Figure B-1 Air valve installation for 30D pump...

  • Page 310: Continuous Flow Electric Valves

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.3 Continuous Flow Electric valves, which provide the best positive valve closure, are Electric Valves most commonly used in liquefied gas applications. Electric valves require the pump controller to be equipped with the valve driver board.

  • Page 311: Dual Electric Valve Installation

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.3.2 Dual Electric Valve To install the electric valve package (refer to Figure B-2 on the Installation following page): 1. Position the valve bases 1.3 cm apart.

  • Page 312: Electric Valve Installation

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D Inlet Tubing with filter DB-25 Connector to controller “electric valve” connector Figure B-2 Electric valve installation...

  • Page 313: User Supplied Valves

    B.4 User Supplied Valves Users may also choose to supply their own valves. The following information is necessary to choose the appropriate valves to work with Teledyne Isco Continuous Flow software. • Check valves Do not use spring-loaded check valves if refilling at atmospheric pressure;...

  • Page 314: Continuous Flow Mode

    You must operate the two pumps manually for initial setup, i.e. refill and purging of air. If the Teledyne Isco air valve package is used, the air valves are switched through ACCESS CTRL. When air valves are used, lights on the air valve actuator indicate which valves are open.

  • Page 315: Defining Operation

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.5.1 Defining Operation Select Pump – This menu allows you to select any pump to display its run screen (program and operation data) and to make program changes.

  • Page 316: Constant Flow Mode

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.5.2 Constant Flow Mode Continuous flow mode is found under the multi-pump options on Menu 2. Once you have accessed the multi-pump options, you may select Constant Flow mode or Constant Pressure mode.

  • Page 317: No Check Valve

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.5.4 No Check Valve To limit fluid backflow from the pump to the supply reservoir one of two approaches is generally used. Either a check valve is...

  • Page 318: To Run Or Stop

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.5.5 To Run or Stop This menu setting allows the operator to run or stop both pairs of pumps simultaneous. REVIOUS Press 3x to return to run screen...
  • Page 319 D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D Liquefied Gases Checklist: 1. Open the valves to atmosphere by pressing , then ACC CTRL selecting each valve to open. 2. Zero the pressure in each pump by pressing ZERO PRESS and selecting each pump to zero.

  • Page 320: Replacement Parts List

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.6 Replacement Parts List B.6.1 30D Pump B-14...
  • Page 321 D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B-15...
  • Page 322 D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B-16...

  • Page 323: Air Valve

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.6.2 30D Air Valve B-17...
  • Page 324 D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B-18...

  • Page 325: Electric Air Valve

    D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B.6.3 30D Electric Air Valve B-19...
  • Page 326 D Series Syringe Pumps Appendix B Continuous Flow Introduction, Installation, and Operation for 30D B-20...
  • Page 327 D Series Syringe Pumps Index D Series Syringe Pumps Index Acc ctrl key, 3-13 Electric valve package, 5-13, B-4 Accessories Electrical connections, 1-18 analog output option, 3-22 analog control, 3-18 back pressure regulation, 2-18 controller, 1-16 cylinder connection package, 2-9...
  • Page 328 D Series Syringe Pumps Index general cleaning, 9-18 lubrication, 9-12 Safety, 1-i–1-ix motor brush replacement, 9-23 Seals power supply voltages, 9-11 break-in procedure, 9-14 removing the case top, 9-9 cleaning and replacement, 9-13 replacement parts, A-2–A-54 Serial control seal cleaning and replacement, 9-13...
  • Page 329 Compliance Statements NOTICE Disregard the following “Declaration of Conformity” and Radio Interference Statement” if your instrument does not have a CE label on its rear panel Radio Interference Statement This equipment has been tested and found to comply with the limits for a class A digital device, pursuant to Part 15 of the FCC Rules.
  • Page 331 Mailing Address: P.O. Box 82531, Lincoln, NE 68501 Equipment Type/Environment: Laboratory Equipment for Light Industrial/Commercial Environments Trade Name/Model No: Series D Series Controller/Pump Controller Year of Issue: 2014 Standards to which Conformity is Declared: EN 61326-1:2006 EMC Requirements for Electrical Equipment for...
  • Page 333 The EMC Directive 2006/95/EEC The Low Voltage Directive 2012/19/EU WEEE Directive Manufacturer's Name: Teledyne Isco Manufacturer's Address: 4700 Superior, Lincoln, Nebraska 68504 USA Mailing Address: P.O. Box 82531, Lincoln, NE 68501 Equipment Type/Environment: Laboratory Equipment for Light Industrial/Commercial Environments Trade Name/Model No:...
  • Page 337 Name and amount of Hazardous Substances or Elements in the product Hazardous Substances or Elements Component Name (Pb) (Hg) (Cd) (Cr(VI)) (PBB) (PBDE) Circuit Boards LCD Display Capacitor Wiring Internal Cables External Cables Line Cord Transformer Front Panel Label Keypad DC Motor Name and amount of Hazardous Substances or Elements in the product...
  • Page 339 The warrantor is Teledyne Isco, 4700 Superior, Lincoln, NE 68504, U.S.A. *This warranty applies to the USA and countries where Teledyne Isco does not have an authorized dealer. Customers in countries outside the USA, where Teledyne Isco has an authorized dealer, should contact their Teledyne Isco dealer for warranty service.
  • Page 341 9-36 Installing the deflector shield ........9-34 9-37 Capacitor and motor shaft .
  • Page 343 1-14 Pump Front Panel ..........1-18 2-1 D Series Syringe Pump Accessory Packages ......2-3 2-2 Manual Refill Kits .

  • Page 344: B-1 Continuous Flow Technical Specifications-Air Valves:

    B-1 Continuous Flow Technical Specifications-Air Valves: ..... B-2 B-2 Continuous Flow Technical Specifications-Electric Valves: ....B-4 B-3 Accessory Control Digital Outputs .

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