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Agilent Technologies 1260 Infinity II User Manual

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  • Page 1 Agilent InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Agilent Technologies...
  • Page 2 Use, duplication or disclosure of Software is subject to Agi- lent Technologies’ standard commercial license terms, and non-DOD Departments and Agencies of the U.S. Government will InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 3 In This Guide... In This Guide... This manual covers the Agilent InfinityLab LC Series 1260 Infinity II Binary Pump (G7112B). 1 Introduction This chapter gives an introduction to the module and an instrument overview. 2 Site Requirements and Specifications This chapter provides information about site requirements and specifications for the binary pump.
  • Page 4 This chapter provides detailed technical information about your binary pump. 12 LAN Configuration This chapter provides information on connecting the module to the Agilent ChemStation PC. 13 Appendix This chapter provides addition information on safety, legal and web. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 5: Table Of Contents

    When to Use a Vacuum Degasser When to Use the Active Seal Wash Option When to Use the Low Volume Mixer When to Remove Damper and Mixer How to Optimize the Compressibility Compensation Setting InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 6 Exchange the Seal Wash Cartridge Replace Leak Handling System Parts Exchange the Outlet Valve Installation of the Solvent Selection Valve Upgrade Kit Exchange the Solvent Selection Valve Replacing Module Firmware InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 7 Setting the 6-bit Configuration Switch Early Maintenance Feedback Instrument Layout 12 LAN Configuration What You Have to Do First TCP/IP parameter configuration Configuration Switches Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) Manual Configuration InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 8 Contents 13 Appendix General Safety Information Waste Electrical and Electronic Equipment (WEE) Directive Radio Interference Sound Emission Agilent Technologies on the Internet InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 9: Introduction

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Introduction Instrument and Operation Introduction to the Pump Principle of Operation Product Description Features Overview of the Hydraulic Path Leak and Waste Handling Leak Sensor Waste Concept This chapter gives an introduction to the module and an instrument overview.

  • Page 10: Instrument And Operation

    (optional) allows to form binary mixtures (isocratic or gradient) from one of two solvents per channel. Active seal wash (optional) is available for use with concentrated buffer solutions. Figure 1 Overview of the binary pump InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 11: Principle Of Operation

    A pressure sensor monitors the pump pressure. A purge valve with integrated PTFE frit is fitted to the pump outlet for convenient priming of the pumping system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 12 64. Bypassing the mixer while the damper remains in line is not a supported configuration and N O T E may lead to undesired behavior of the binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 13 Introduction Instrument and Operation Figure 3 The hydraulic path of the Binary Pump with bypassed damper and mixer For pump specifications, see “Performance Specifications” on page 30. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 14: Product Description

    Introduction Instrument and Operation Product Description The Agilent 1260 Infinity II Binary Pump is suited for LC applications using conventional or superficially porous particles columns, as well as STM column technology. Gradient formation is based on a high-pressure mixing principle.

  • Page 15: Overview Of The Hydraulic Path

    The solvent enters the pump heads close to the bottom limit and leaves it at its top. The outer diameter of the piston is smaller than InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 16 During the drawing stroke of the first piston, the second piston delivers the drawn volume into the system. For pump specifications, see “Performance Specifications” on page 30. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 17 Solvent compressibility calibrations acquired with a miscalibrated pump will work, but they are not transferable to other pumps. A correct pump elasticity calibration is an essential prerequisite for successful solvent compressibility calibrations. ➔ Calibrate the pump elasticity correctly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 18 Unfortunately, the influence of the temperature on compressibility is non-linear and cannot be calculated. The Agilent 1260 Infinity II Binary Pump features a multi point compressibility calibration. The compressibility of a solvent is determined at different pressures from 0 –...
  • Page 19 The stroke volume for the pump is by default set to AUTO mode. This means that the stroke is optimized for the flow rate in use. A change to larger stroke volumes is possible but not recommended. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 20: Leak And Waste Handling

    • from the Multisampler needle wash port • from the Sample Cooler or Sample Thermostat (condensate) • from the pump's Seal Wash Sensor (if applicable) • from the pump's Purge Valve or Multipurpose Valve InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 21 Introduction Leak and Waste Handling Figure 6 Infinity II Leak Waste Concept (Flex Bench installation) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 22 Introduction Leak and Waste Handling Figure 7 Infinity II Single Stack Leak Waste Concept (bench installation) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 23: Leak Sensor

    The solvent DMF (dimethyl formamide) leads to corrosion of the leak sensor. The material of the leak sensor, PVDF (polyvinylidene fluoride), is incompatible with DMF. ➔ Do not use DMF. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 24: Waste Concept

    1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports (5043-1221) for optimal and safe waste disposal. If you decide to use your own waste solution, make sure that the tubes don't immerse in the liquid. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 25: Site Requirements And Specifications

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information about site requirements and specifications for the binary pump. Agilent Technologies...

  • Page 26: Site Requirements

    ➔ Make sure the power connector of the instrument can be easily reached and unplugged. ➔ Provide sufficient space behind the power socket of the instrument to unplug the cable. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 27: Site Requirements

    Never use the power cords that Agilent Technologies supplies with this instrument for any other equipment. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. Absence of ground connection WA R N I N G The absence of ground connection can lead to electric shock or short circuit.
  • Page 28 ➔ If your module was shipped in cold weather, leave it in its box and allow it to warm slowly to room temperature to avoid condensation. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 29: Physical Specifications

    For storing the module Safety standards: Installation category II, Pollution degree 2 For indoor use only. IEC, EN, CSA, UL ISM Classification ISM Group 1 Class B According to CISPR 11 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 30: Performance Specifications

    Standard delay volume configuration: Delay volume measured with water at 600 – 900 µL, (includes 400 µL mixer), 1 mL/min (water/water with dependent on back pressure tracer) Low delay volume configuration:120 µL InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 31 Electronic records of maintenance and errors. Housing All materials are recyclable InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 32 Site Requirements and Specifications Performance Specifications InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 33: Using The Pump

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Using the Pump Magnets Turn on/off Status Indicators Best Practices Daily / Weekly tasks Power up / Shut-down the pump Prepare the pump How to deal with solvents Leak and Waste Handling...

  • Page 34: Magnets

    Using the Pump Magnets Magnets This stack exemplarily shows the magnets' positions in the modules. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 35: Turn On/Off

    Using the Pump Turn on/off Turn on/off Power switch: On Turn instrument On/Off with the control software. Power switch: Off InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 36 Using the Pump Turn on/off InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 37: Status Indicators

    5. Resident mode (blinking) - for example during update of main firmware. 6. Bootloader mode (fast blinking). Try to re-boot the module or try a cold-start. Then try a firmware update. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 38: Best Practices

    • Flush system with water to remove buffer. • Remove all samples from the sampler and store according to good laboratory practice. • Use recommended solvents to store the system. • Power off the system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 39: Prepare The Pump

    • Label bottles correctly with bottle content, and filling date / expiry date. • Use solvent inlet filters. • Reduce risk of algae growth: use brown bottles for aqueous solvents, avoid direct sunlight. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 40: Leak And Waste Handling

    N O T E has been shipped with the solvent cabinet, electronic copies are available in the Agilent Information Center or via the Internet. For details on correct installation, see separate installation documentation. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 41: Hints For Successful Use Of The Binary Pump

    • After changing the piston seals, apply the seal wear-in procedure (see “Seal Wear-in Procedure” on page 136). • Place the aqueous solvent on channel A and the organic solvent on channel B. The default compressibility settings are set accordingly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 42: Setting Up The Pump With The G4208A Instant Pilot

    Pilot G4208A User's Guide (G4208-90006). Details about setting up module specific parameters can be found in the Instant Pilot online help. The pump parameters are described in detail in “Overview” on page 43. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 43: Setting Up The Pump With The Instrument Control Interface

    Parameters described in following sections are offered by the instrument control interface and can usually be accessed through Agilent instrument control software. For details, please refer to manuals and online help of respective user interfaces. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 44: Setup Of Basic Pump Parameters

    • Display There are three ways to display the timetable: • in tabular form • as flow/pressure graph • as solvent percentage plot Values can only be changed in tabular view. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 45: Pump Control

    C AU T I O N This can result in a rapid and uncontrolled pressure increase. ➔ To prevent harm to the column, open the purge valve until the initialization is finished. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 46: Data Curves

    N O T E and flow are calculated from the method settings of the pump. For details, please refer to the online help or manual of your instrument control software. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 47: Bottle Filling

    If this option is checked, the pump will turn off before air is aspirated. However, off... the residual solvent volume has been calculated for 1 L solvent bottles and may be too small for large bottles or other vessels. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 48: Solvent Information

    Pump head (body) Pistons Sapphire Piston seals/wash seals PTFE, SST (reversed phase) or UHMW-PE, SST (normal phase) Pressure sensor Purge valve SST, gold, PTFE, ceramic Damping unit SST, gold Capillaries/fittings Tubings PTFE InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 49 PEEK capillaries keeps the flow path free of steel and ensures pressure stability to at least 600 bar. If in doubt, consult the available literature about the chemical compatibility of PEEK. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 50 It can be corroded by strong bases (e.g. hydroxide solutions > 10 %, diethylamine). It is not recommended for the use with fluoric acid and fluorides. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 51 For example, a 1 % solution of acetic acid in methanol will attack steel. • Solutions containing strong complexing agents (for example, EDTA, ethylene diamine tetra-acetic acid). • Mixtures of carbon tetrachloride with 2-propanol or THF. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 52 It can be corroded by complexing cyanides and concentrated acids like aqua regia. Zirconium Oxide (ZrO Zirconium Oxide is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 53 Sapphire, Ruby and Al -based ceramics Sapphire, ruby and ceramics based on aluminum oxide Al are inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 54: Algae Growth In Hplc Systems

    • Use the amber solvent bottle ( Solvent bottle, amber, 1000 mL (9301-6526)) supplied with the instrument for your aqueous mobile phase. • If possible add a few mg/l sodium azide or a few percent organic solvent to the aqueous mobile phase. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 55: Prevent Blocking Of Solvent Filters

    Observe appropriate safety procedures (for example, wear goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the solvent vendor, especially when toxic or hazardous solvents are used. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 56: Cleaning The Solvent Filters

    • Thoroughly flush the filter with HPLC-grade water (remove all nitric acid, some capillary columns can be damaged by nitric acid). • Replace the filter. Never use the system without solvent filter installed. N O T E InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 57: Normal Phase Applications

    Do not use normal phase valves in applications running with aqueous solutions. The N-Valves have been tested successfully in using hexane at pressures below 100 bar; heptane can be used as a substitute for neurotoxic hexane. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 58 Type N (G4204-60122) Outlet valves 1260 Infinity Outlet Valve Type 1290 Infinity Outlet Valve Type N/SFC (G1312-60167) N (G4220-60128) Seals PE seals (pack of 2) (0905-1420) Wash Seal PE (0905-1718) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 59: Optimizing Performance

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Optimizing Performance When to Use a Vacuum Degasser Operational Hints for the Vacuum Degasser When to Use the Active Seal Wash Option When to Use the Low Volume Mixer When to Remove Damper and Mixer...

  • Page 60: When To Use A Vacuum Degasser

    0.5 mL/min). • The binary pump is used with bypassed damper and mixer. The external 1260 Infinity II Degasser G7122A is recommended for use with applications using highly volatile solvents like Hexane or DCM, solvents with special characteristics like THF, or applications using refractive index detection.

  • Page 61: When To Use The Active Seal Wash Option

    The operation of the peristaltic pump can be controlled from the data system or the Instant Pilot. For adding a seal-wash option, please contact your local Agilent Technologies service representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 62: When To Use The Low Volume Mixer

    The Low volume mixer ( 200 μL) (5067-1565) is designed for use with the Agilent InfinityLab LC Series 1260 Infinity II Binary LC System in low delay volume mode. This configuration is typically used for 2.1 mm i.d., 1.8 μm particle size columns, where emphasis is put on S/N ratio.

  • Page 63: When To Remove Damper And Mixer

    For applications that require lowest delay volume (for example, fast gradient methods or gradient applications with low flow rates), damper and mixer can be bypassed. Figure 9 Flow path modifications of the Binary Pump InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 64: Convert The Binary Pump To Low Delay Volume Mode

    This paragraph shows how to bypass damper and mixer and convert the pump to low delay volume mode. Configurations where only damper or mixer are disconnected while the other part is still in line are not supported by Agilent Technologies. Tools required Description...
  • Page 65 Disconnect fitting A from outlet 1 of the mixer. Connect fitting A to port 2 of the pressure sensor. Seal port 1 of the mixer with a plastic blank nut. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 66: How To Optimize The Compressibility Compensation Setting

    400 bar binary pump, an average compressibility value for the solvent is sufficient. For the 600 bar 1260 Infinity II Binary Pump , the pressure-dependency of a solvent compressibility needs to be considered. It is determined at different pressures between 0 – 600 bar. The pump uses the obtained non-linear function to select the correct compressibility value for the actual pump pressure.

  • Page 67: Optimization Of Legacy Compressibility Settings

    10. The compressibility compensation setting that generates the smallest pressure ripple is the optimum value for your solvent composition. 6 Repeat step 1 through step 5 for the B channel of your binary pump. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 68 How to Optimize the Compressibility Compensation Setting Table 8 Solvent Compressibility Solvent (pure) Compressibility (10 /bar) Acetone Acetonitrile Benzene Carbon tetrachloride Chloroform Cyclohexane Ethanol Ethyl acetate Heptane Hexane Isobutanol Isopropanol Methanol 1-Propanol Toluene Water InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 69: Troubleshooting And Diagnostics

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Troubleshooting and Diagnostics Overview of the Module’s Indicators and Test Functions User Interfaces Agilent Lab Advisor Software Overview of the troubleshooting and diagnostic features. Agilent Technologies...

  • Page 70: Overview Of The Module's Indicators And Test Functions

    (i.e. the high pressure flow path between pump and column). After exchanging flow path components (e.g. pump seals or injection seal), use this test to verify the system is pressure tight, see “(System) Pressure Test” page 96. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 71 When a problem with the pump is suspected, use this test to help troubleshoot the pump and its pumping performance, see “Pump Leak Rate Test” on page 107. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 72: User Interfaces

    Depending on the user interface, the available tests vary. Some descriptions are only available in the Service Manual. Test Instant Pilot G4208A Agilent Lab Advisor Pressure Test Valve Test Solvent compressibility calibration Pump elasticity calibration InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 73: Agilent Lab Advisor Software

    The tests and diagnostic features that are provided by the Agilent Lab Advisor software may differ from the descriptions in this manual. For details, refer to the Agilent Lab Advisor software help files. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 74 Troubleshooting and Diagnostics Agilent Lab Advisor Software InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 75: Error Information

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Error Information What Are Error Messages General Error Messages Timeout Shutdown Remote Timeout Lost CAN Partner Leak Leak Sensor Open Leak Sensor Short Compensation Sensor Open Compensation Sensor Short Fan Failed...
  • Page 76 Degasser: Vacuum cannot be maintained Degasser: limit not reached This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 77: What Are Error Messages

    In all cases, error propagation is done via the CAN bus or via an APG/ERI remote cable (see documentation for the APG/ERI interface). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 78: General Error Messages

    Check the vacuum degasser for an error The degasser failed to generate sufficient condition. Refer to the Service Manual for the vacuum for solvent degassing. degasser or the pump that has the degasser built-in. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 79: Remote Timeout

    Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective main board in another module. determine which module or modules are not recognized by the system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 80: Leak

    If there are still signs of a leak, exchange the valve, or outlet valve. appropriate seal (purge valve, active inlet valve, outlet valve). Exchange the pump seals. Defective pump seals. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 81: Leak Sensor Open

    Leak sensor incorrectly routed, being pinched by a metal component. Please contact your Agilent service representative. Power switch assembly defective Please contact your Agilent service representative. Cable or contact problem. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 82: Compensation Sensor Open

    Probable cause Suggested actions Please contact your Agilent service Defective power switch assembly representative. Please contact your Agilent service Loose connection between the power representative. switch board and the main board InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 83: Fan Failed

    Please contact your Agilent service Defective fan. representative. Please contact your Agilent service Defective main board. representative. Please contact your Agilent service Improperly positioned cables or wires representative. obstructing fan blades. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 84: Module Error Messages

    (autosampler), sample loop (autosampler), column frits and capillaries with small internal diameters (e.g. 50 µm ID). Please contact your Agilent service representative. Defective pressure sensor. Please contact your Agilent service representative. Defective main board. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 85: Pressure Below Lower Limit

    -120 mV across the pressure sensor. Probable cause Suggested actions Please contact your Agilent service representative. Pressure sensor disconnected Please contact your Agilent service representative. Defective pressure sensor InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 86: Valve Failed

    Please contact your Agilent service Connection cable (inside instrument) not representative. connected. Please contact your Agilent service Connection cable (inside instrument) representative. defective. Exchange the solvent selection valve. Solvent selection valve defective. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 87: Electronic Fuse Of Ssv Open

    Please contact your Agilent service Defective connection cable (front panel to representative. main board). Please contact your Agilent service Defective main board. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 88: Motor-Drive Power

    Please contact your Agilent service Defective pump drive assembly. representative. Please contact your Agilent service Defective main board. representative. Exchange restriction capillary. Restriction capillary blocked at pre-mixing union. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 89: Encoder Missing

    Probable cause Suggested actions Please contact your Agilent service Defective or disconnected pump encoder representative. connector. Please contact your Agilent service Defective pump drive assembly. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 90: Servo Restart Failed

    Exchange the (passive or active) inlet valve. Blocked (passive or active) inlet valve. Please contact your Agilent service Defective pump drive assembly. representative. Please contact your Agilent service Defective main board. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 91: Pump Head Missing

    Irregular or sticking drive movement. pistons, and internal components for signs of wear, contamination or damage. Exchange components as required. Please contact your Agilent service Defective pump drive assembly. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 92: Index Adjustment

    Probable cause Suggested actions Please contact your Agilent service representative. Disconnected or defective encoder cable. Please contact your Agilent service representative. Defective pump drive assembly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 93: Initialization Failed

    • Measured pressure is higher than 32000 hPa Probable cause Suggested actions Please contact your Agilent service Degasser sensor defect representative. Please contact your Agilent service Degasser sensor not connected to main representative. board. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 94 Please contact your Agilent service Liquid in degasser tubing. representative. Please contact your Agilent service Leak in degasser tubing or chamber. representative. Please contact your Agilent service Degasser vacuum pump defect. representative. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 95: Test Functions And Calibration

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Test Functions and Calibration (System) Pressure Test Positioning the Blank Nut Running the System Pressure Test Evaluating the Results Valve Test Running the Valve Test Evaluating the Results Binary Pump Solvent Compressibility Calibration...

  • Page 96: (System) Pressure Test

    When the system pressure reaches 600 bar, the pump continues to pump at a flow rate that keeps the pressure constant. The flow that is needed to keep the pressure constant is directly translated into a leak rate. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 97: Positioning The Blank Nut

    Pressure Test again. If the test passes, the defective component is located after the blank nut. Confirm the diagnosis by placing the blank nut immediately after the suspected component. The diagnosis is confirmed if the test fails. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 98: Running The System Pressure Test

    N O T E is caused by the abnormal termination during the operation of the test whereas a failure of a test indicates that the test results were not within the specified limits. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 99 Tighten the fitting or exchange the capillary. Damaged pump seals or pistons. Run the valve test to identify the defective component. Loose purge valve. Tighten the purge valve nut (14 mm wrench). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 100 Potential Cause (Column Compartment) Potential Cause (Column Compartment) Corrective Action Loose or leaky fitting. Tighten or exchange the fitting or capillary. Rotor seal (column switching valve). Exchange the rotor seal. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 101: Valve Test

    The procedure from step 1 is repeated on pump head B. Step 3 The data from step 1 and 2 are evaluated. In case test failed, a conclusion about the defective part is made. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 102: Running The Valve Test

    Make sure to release the pressure by opening the purge valve when the test has N O T E completed. Otherwise the pump may generate an overpressure error. Evaluating the Results Refer to the help file of the Agilent Lab Advisor for further details. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 103: Binary Pump Solvent Compressibility Calibration

    The compressibility data set for this solvent is stored in an XML-file on the desktop. It can be shared with other InfinityLab LC Series binary pumps via the controlling data system. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 104: Running The Solvent Compressibility Calibration

    2 Start the test and follow the instructions. Make sure to release the pressure by opening the purge valve when the test has N O T E completed. Otherwise the pump may generate an overpressure error. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 105: Pump Elasticity Calibration

    Solvent compressibility calibrations acquired with a miscalibrated pump will work, but they are not transferable to other pumps. A correct pump elasticity calibration is an essential prerequisite for successful solvent compressibility calibrations. ➔ Calibrate the pump elasticity correctly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 106: Running The Pump Elasticity Calibration

    2 Start the test and follow the instructions. Make sure to release the pressure by opening the purge valve when the test has N O T E completed. Otherwise the pump may generate an overpressure error. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 107: Pump Leak Rate Test

    1 Select the Pump Leak Rate Test from the Test Selection menu. 2 Start the test and follow the instructions. Make sure to release the pressure by slowly opening the purge valve when the test has N O T E finished. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 108: Evaluating The Results

    Results of the leak rate test are the leak rates measured for pistons 1 and 2 as described for the test principle. If any of the leak rates exceeds 3 μL/min, the test will fail. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 109: Potential Causes Of Leak Rate Test Failure

    Suggested actions Inspect piston, replace piston and/or seal Leak at piston 1 or seal in chamber 1 Replace inlet valve or inlet valve cartridge (AIV Leak at inlet valve only) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 110 Probable cause Suggested actions Replace the part which has failed and re-run Leak at outlet valve the test. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 111: Maintenance

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Maintenance Introduction to Maintenance Cautions and Warnings Cleaning the Module Overview of Maintenance and Simple Repairs Maintenance Procedures Remove and Install Doors Exchange the Purge Valve Frit or the Purge Valve...

  • Page 112: Introduction To Maintenance

    These procedures are described in “Overview of Maintenance and Simple Repairs” on page 116. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 113: Cautions And Warnings

    ➔ The volume of substances should be reduced to the minimum required for the analysis. ➔ Do not operate the instrument in an explosive atmosphere. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 114 If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 115: Cleaning The Module

    WA R N I N G hazard and damage the module ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any connections in the flow path. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 116: Overview Of Maintenance And Simple Repairs

    “Exchange the Active Inlet Valve (AIV) or its Cartridge” page 137 Pump head, see “Maintenance of a Pump Head with Seal Wash” on page 130 Solvent selection valve, see “Exchange the Solvent Selection Valve” on page 148 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 117: Maintenance Procedures

    Pressure ripple unstable, run Pump Leak Rate Test for verification “Exchange the Solvent Selection Valve” If internally leaking Cross port flow page 148 If solenoid is defective Error message “Valve Failed” InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 118: Remove And Install Doors

    The figures shown in this procedure exemplarily show the Infinity II Multisampler module. N O T E The principle of how to remove and/or install doors works in the same way for all Infinity II modules. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 119 Press the release buttons and pull the front door out. For the Installation of the front door. Insert the hinges into their guides and move the door in until the release buttons click into their final position. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 120: Exchange The Purge Valve Frit Or The Purge Valve

    Using the 14 mm wrench, unscrew the purge valve and capillary from the purge valve. Disconnect the waste remove it from the purge valve holder. tube. Beware of leaking solvents due to hydrostatic pressure. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 121 (slit in frit points to the front). N O T E Before reinstallation always check the gold seal in the seal cap. A deformed seal cap should be exchanged. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 122 The rubber o-ring might break. ➔ Anticipate the correct position of the connections before tightening the valve. Tighten the purge valve and reconnect outlet capillary and waste tubing. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 123: Replace The O-Ring On The Purge Valve

    • Use an optional solvent shutoff valve or lift up solvent filters in solvent reservoirs for avoiding leakages. • Remove the purge valve from the pump head. Disassemble the purge valve. Remove the old o-ring from the purge valve. Clean the purge valve parts. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 124 Reinstall the seal cap including the gold seal. pump. The o-ring will take damage. N O T E Before reinstallation always check the gold seal in the seal cap. A deformed seal cap should be exchanged. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 125: Remove The Pump Head Assembly

    The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 126 Using a 4 mm hexagonal key stepwise loosen and Unplug the active inlet valve cable from the connector. remove the two pump head screws. Remove the pump head assembly from the module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 127: Maintenance Of A Pump Head Without Seal Wash

    The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 128 Using the steel side of the insert tool, carefully remove layers: clean the piston surface with abrasive paper and the seal from the pump housing. rinse with 2-propanol. Replace piston if scratched. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 129 Place the pump housing onto the piston housing. Insert the pistons and carefully press them into the seals. Tighten the lock screw. Install the pump head, see “Reinstall the Pump Head Assembly” on page 134. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 130: Maintenance Of A Pump Head With Seal Wash

    The following procedure describes the removal and disassembly of pump head A (left). For pump head B (right) proceed in the same way and skip steps that deal with the purge valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 131 Lift the housing away from the pistons. Check the piston surface and remove any deposits or layers: clean the piston surface with abrasive paper and rinse with 2-propanol. Replace piston if scratched. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 132 Place the support rings on the piston housing. Note the ring. Use a matching orientation of gasket and support correct position of the pins on the support ring. ring. Put the seal holder on top of the gasket. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 133 Place the pump housing onto the piston housing. Insert the pistons and carefully press them into the seals. Tighten the lock screw. Install the pump head, see “Reinstall the Pump Head Assembly” on page 134. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 134: Reinstall The Pump Head Assembly

    Slide the pump head assembly onto the pump drive. Using a 4 mm hexagonal key, tighten the pump head Reconnect the active inlet valve cable to the connector. screws stepwise with increasing torque. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 135 Maintenance Reinstall the Pump Head Assembly Reconnect all tubings and capillaries. Close the doors. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 136: Seal Wear-In Procedure

    Reconnect the intake tubing to the solvent selection valve and the connecting tube from the solvent selection valve (if installed) to the AIV. 7 Purge your system with the solvent used for your next application. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 137: Exchange The Active Inlet Valve (Aiv) Or Its Cartridge

    C AU T I O N Overtightening will destroy the active inlet valve cartridge. ➔ Tighten the active inlet valve properly. Open the doors. Unplug the active inlet valve cable from the connector. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 138 Screw the new valve into the pump head. With the Position the valve so that the solvent inlet tube 14 mm wrench, turn the nut until it is hand tight. connection points towards the front. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 139 N O T E in the current application before the flow stabilizes at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 140: Exchange The Seal Wash Cartridge

    Remove the wash solvent tubings from the support ring Unclip the peristaltic pump cartridge from the module outlet and from the adapter leading to the waste bottle. housing and remove it. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 141 Connect the peristaltic pump tubes to the support rings the pump motor and push the plastic clips into the outlet and to the adapter leading to the waste bottle. module housing. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 142: Replace Leak Handling System Parts

    (2.). Install the Leak Adapter by pressing it into the Main Insert the Tubing (approximately 85 mm required for Cover. replacement) between Leak Adapter outlet and Leak Panel. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 143 Maintenance Replace Leak Handling System Parts Close the doors. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 144: Exchange The Outlet Valve

    Unscrew the valve with the 14 mm wrench and remove it from the outlet valve. from the pump body. N O T E Do not disassemble the outlet valve, as this can damage the valve. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 145 Maintenance Exchange the Outlet Valve Reinstall the outlet valve and tighten it using a torque Reconnect the capillary. wrench (approx.12 Nm). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 146: Installation Of The Solvent Selection Valve Upgrade Kit

    Guide the SSV cable through the slots in the distance connection socket inside (behind the pump front metal sheet and route it through the slot in the pump front panel). metal panel to the internal connection socket. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 147 N O T E mL of solvent to get the flow stabilized at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 148: Exchange The Solvent Selection Valve

    Place the bottles back into the solvent cabinet. Using a screwdriver, loosen the holding screws of the Carefully pull the valve holder out. valve holder. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 149 Bend the cable at the connector of the new valve. Guide the cable and connector into the hole and push the connector into the socket. Exchange the defective solvent selection valve. Tighten the screws of the valve holder. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 150 After an exchange of the valve it may be required to pump several mL of solvent before the N O T E flow stabilizes at a pressure ripple as low as it used to be when the system was still working properly. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 151: Replacing Module Firmware

    Agilent web. http://www.agilent.com/en-us/firmwareDownload?whid=69761 2 For loading the firmware into the module follow the instructions in the documentation. Module Specific Information There is no specific information for this module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 152 Maintenance Replacing Module Firmware InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 153: Parts And Materials For Maintenance

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Parts and Materials for Maintenance Hydraulic Path with Solvent Selection Valve Hydraulic Path without Solvent Selection Valve Pump Head Assembly Without Seal Wash Pump Head Assembly with Seal Wash Option...

  • Page 154: Hydraulic Path With Solvent Selection Valve

    Capillary ST 0.17 mm x 900 mm SI/SX ps-ps 5064-5444 Peristaltic pump cartridge, silicone tubing 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m for seal wash option 5062-2461 Waste tube, 5 m (reorder pack) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 155 Parts and Materials for Maintenance Hydraulic Path with Solvent Selection Valve Figure 11 Hydraulic Path with Solvent Selection Valve InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 156: Hydraulic Path Without Solvent Selection Valve

    Capillary ST 0.17 mm x 900 mm SI/SX ps-ps 5065-4445 Peristaltic pump with Pharmed tubing 5062-2461 Waste tube, 5 m (reorder pack) 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m for seal wash option InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 157 Parts and Materials for Maintenance Hydraulic Path without Solvent Selection Valve Figure 12 Hydraulic Path without Solvent Selection Valve, with Active Seal Wash InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 158: Pump Head Assembly Without Seal Wash

    Lock screw 12 a G1312-60025 Active inlet valve body, without cartridge 12 b G1312-60020 Cartridge for active inlet valve 600 bar G1312-23201 Adapter 0515-2118 Pump head screw (M5, 60 mm) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 159 Parts and Materials for Maintenance Pump Head Assembly Without Seal Wash Figure 13 Pump Head Assembly Without Seal Wash InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 160: Pump Head Assembly With Seal Wash Option

    Lock screw G1311-25200 Pump chamber housing G1312-60025 Active inlet valve body, without cartridge G1312-60020 Cartridge for active inlet valve 600 bar G1312-23201 Adapter 0515-2118 Pump head screw (M5, 60 mm) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 161 Parts and Materials for Maintenance Pump Head Assembly with Seal Wash Option Figure 14 Pump Head Assembly with Seal Wash Option InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 162: Outlet Valve

    Parts and Materials for Maintenance Outlet Valve Outlet Valve Description G1312-60067 Outlet valve Figure 15 Outlet valve InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 163: Purge Valve Assembly

    Purge Valve Assembly Purge Valve Assembly Item Description G7111-60061 Purge valve 01018-22707 PTFE frits (pack of 5) 5067-4728 Seal cap 5067-6595 1260 PV O-ring FKM 5/pack Figure 16 Purge Valve Assembly InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 164: Active Inlet Valve Assembly

    Active Inlet Valve Assembly Active Inlet Valve Assembly Item Description G1312-60025 Active inlet valve body, without cartridge G1312-60020 Cartridge for active inlet valve 600 bar Figure 17 Active Inlet Valve Assembly InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 165: Hplc System Tool Kit

    Parts and Materials for Maintenance HPLC System Tool Kit HPLC System Tool Kit InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 166: Active Seal Wash Option

    Shock mount 1540-0455 Edge protector 5041-2120 Folding box 5065-4445 Peristaltic pump with Pharmed tubing 5042-6422 Tubing connector, 1 mm o.d. 5065-9943 Stepper Motor for the Peristaltic Pump G3010-01203 RFI Strip 10×30 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 167: Solvent Cabinet

    Parts and Materials for Maintenance Solvent Cabinet Solvent Cabinet Description 5067-5760 Solvent Cabinet Kit For details refer to: Usage Guideline for the Solvent Cabinet (01200-90150) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 168: Bottle Head Assembly

    5063-6599 Tube screw (10/Pk) Wire marker 5062-2483 Tube PTFE 1.5 mm x 5 m, 3 mm od 5062-8517 Inlet filter adapter (4/Pk) 5041-2168 Solvent inlet filter, 20 µm pore size InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 169: Cover Parts

    Door Assembly Infinity 180 Left 5043-1354 Name Plate 1290 Infinity 2 G7104-68713 Cabinet Kit 180 Infinity II (includes sides, bottom, top, leak adapter top and Status Indicator Insert) Figure 18 Cover Parts InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 170: Accessory Kit

    Algae note 5500-1169 Y Tube Connector ID 6.4 5500-1155 Tube Connector, 90 degree, ID 6.4 5043-1372 Tubing Connector Leak 3-1 5043-1373 Tubing Connector Leak Cap 0890-1195 PTFE tubing, 0.052 in i.d. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 171: Identifying Cables

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Identifying Cables Cable Overview Analog Cables Remote Cables CAN/LAN Cables RS-232 Cable Kit Agilent 1200 Module to Printer This chapter provides information on cables used with the Agilent InfinityLab LC Series modules.

  • Page 172: Cable Overview

    Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent 35900A A/D converter...
  • Page 173 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m USB cables Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 174: Analog Cables

    The other end depends on the instrument to which connection is being made. Agilent Module to 35900 A/D converters p/n 35900-60750 35900 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 175 Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 176: Remote Cables

    NOT USED pink SHUT DOWN blue START PREPARE black 1wire DATA violet DGND grey-pink +5V ERI out red-blue PGND white-green PGND brown-green +24V ERI out white-yellow +24V ERI out yellow-brown InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 177 • 5188-8045 ERI to APG (Connector D_Subminiature 15 pin (ERI), Connector D_Subminiature 9 pin (APG)) p/n 5188-8045 Pin (ERI) Signal Pin (APG) Active (TTL) Start Request Stop Ready High Power on High Future Shut Down Start Prepare Ground Cable Shielding InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 178 Ground Cable Shielding One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 179 Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 180: Can/Lan Cables

    CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 181: Rs-232 Cable Kit

    It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 182: Agilent 1200 Module To Printer

    To connect a USB Flash Drive use a USB OTG cable with Mini-B plug and A socket. Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 183: Hardware Information

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Hardware Information Firmware Description Electrical Connections Serial Number Information (ALL) Rear view of the module Interfaces Overview Interfaces ERI (Enhanced Remote Interface) USB (Universal Serial Bus) Setting the 6-bit Configuration Switch...

  • Page 184: Firmware Description

    • run synchronization through APG/ERI remote, • error handling, • diagnostic functions, • or module specific functions like • internal events such as lamp control, filter movements, • raw data collection and conversion to absorbance. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 185 Update of main system can be done in the resident system only. Update of the resident N O T E system can be done in the main system only. Main and resident firmware must be from the same set. Figure 19 Firmware Update Mechanism InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 186 All this specific information is described in the documentation provided with the firmware update tools. The firmware update tools, firmware and documentation are available from the Agilent web. • http://www.agilent.com/en-us/firmwareDownload?whid=69761 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 187: Electrical Connections

    There are no externally accessible fuses because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.

  • Page 188: Serial Number Information (All)

    (there can be more than one code for the same module) 00000 Serial number Rear view of the module Figure 20 Rear view of the pump – electrical connections and label InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 189: Interfaces

    Module RS-232 Analog APG (A) Special (on-board) / ERI (E) Pumps G7104A/C G7110B G7111A/B, G5654A G7112B G7120A G7161A/B Samplers G7129A/B/C G7167B/C, G5667A G7157A Detectors G7114A/B G7115A G7117A/B/C G7121A/B G7162A/B G7165A InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 190 • RS-232C as interface to a computer • USB (Universal Series Bus) as interface to a computer • REMOTE connector as interface to other Agilent products • Analog output connector(s) for signal output InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 191: Overview Interfaces

    “USB (Universal Serial Bus)” on page 196. Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s main board. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 192 Remote (ERI) The ERI (Enhanced Remote Interface) connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. It allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
  • Page 193 PREPARE (L) Request to prepare for analysis (for example, calibration, detector lamp on). Receiver is any module performing pre-analysis activities. Special Interfaces There is no special interface for this module. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 194: Eri (Enhanced Remote Interface)

    This way the interface can support various additional devices like sensors, triggers (in and out) and small controllers, etc. Figure 21 Location of the ERI interface (example shows a G7114A/B VWD) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 195 This serial line can be used to read out an EPROM or write into an EPROM of a connected ERI-device. The firmware can detect the connected type of device automatically and update information in the device (if required). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 196: Usb (Universal Serial Bus)

    • Short circuit will be detected through hardware. USB (Universal Serial Bus) USB (Universal Serial Bus) - replaces RS232, supports: • a PC with control software (for example Agilent Lab Advisor) • USB Flash Disk InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 197: Setting The 6-Bit Configuration Switch

    • For specific LAN modes switches 4-5 must be set as required. • For boot resident/cold start modes switches 1+2 or 6 must be UP. Figure 22 Location of Configuration switch (example shows a G7114A/B VWD) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 198 When selecting mode COM, settings are stored to non-volatile memory. When selecting mode TEST, COM settings are tak- en from non-volatile memory. not assigned - Always keep these switches on position ‘0’ (off) Default IP Address is 192.168.254.11 Host Name will be the MAC address. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 199: Special Settings

    Save your methods and data before executing a forced cold start. If you use the following switch settings and power the instrument up again, it will start as described above. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 200 Boot Main System / Keep Data Boot Resident System / Keep Data Boot Main System / Revert to Default Data Boot Resident System / Revert to Default Data Note: The setting '0' (down) is essential. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 201: Early Maintenance Feedback

    EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 202: Instrument Layout

    • the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 203 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual LAN Configuration What You Have to Do First TCP/IP parameter configuration Configuration Switches Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) Setup (DHCP) Manual Configuration With Telnet This chapter provides information on connecting the module to the Agilent ChemStation PC.

  • Page 204: Lan Configuration What You Have To Do First

    PC network card using a crossover network cable (point-to-point) or • a hub or switch using a standard LAN cable. Figure 24 Location of LAN interfaces and MAC label InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 205: Tcp/Ip Parameter Configuration

    TCP/IP parameters after power-on. The parameters may be derived non-volatile memory or initialized with known default values. The initialization mode is selected by the configuration switch, see Table 18 page 207. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 206: Configuration Switches

    The module is shipped with all switches set to OFF, as shown above. To perform any LAN configuration, SW1 and SW2 must be set to OFF. N O T E InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 207: Initialization Mode Selection

    The TCP/IP connection will be established using these parameters. The parameters were configured previously by one of the described methods. Figure 26 Using Stored (Principle) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 208 In the Using Default mode, the parameters stored in the memory of the module are not N O T E cleared automatically. If not changed by the user, they are still available, when switching back to the mode Using Stored. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 209: Dynamic Host Configuration Protocol (Dhcp)

    2 It may be necessary to fully qualify the hostname with the DNS suffix, e.g. 0030d3177321.country.company.com. 3 The DHCP server may reject the hostname proposed by the card and assign a name following local naming conventions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 210: Setup (Dhcp)

    0030d3177321. On the Local Controller the MAC address can be found under Details in the LAN section. Figure 29 LAN Setting on Instant Pilot InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 211 Lab Advisor, Firmware Update Tool) and use MAC address as host name, e.g. 0030d3177321. The LC system should become visible in the control software (see Note in section “General Information (DHCP)” on page 209). InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 212: Manual Configuration

    Telnet session. 1 Open the system (DOS) prompt window by clicking on Windows START button and select “Run...”. Type “cmd” and press OK. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 213 Handheld Controller, or the default IP address (see “Configuration Switches” on page 206). When the connection was established successfully, the module responds with the following: Figure 32 A connection to the module is made InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 214 Then press [Enter], where parameter refers to the configuration parameter you are defining, and value refers to the definitions you are assigning to that parameter. Each parameter entry is followed by a carriage return. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 215 Initialization mode is Using Stored active TCP/IP settings stored TCP/IP settings in non-volatile memory connected to PC with controller software (e.g. Agilent ChemStation), here not connected Figure 35 Telnet - Change IP settings InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 216 If the Initialization Mode Switch is changed now to “Using Stored” mode, the instrument N O T E will take the stored settings when the module is re-booted. In the example above it would be 192.168.254.12. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 217: Appendix

    InfinityLab LC Series 1260 Infinity II Binary Pump User Manual Appendix General Safety Information General Safety Information Safety Standards General Before Applying Power Ground the Instrument Do Not Operate in an Explosive Atmosphere Do Not Remove the Instrument Cover Do Not Modify the Instrument...

  • Page 218: General Safety Information

    Do not use this product in any manner not specified by the manufacturer. The protective features of this product may be impaired if it is used in a manner not specified in the operation instructions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 219: Before Applying Power

    Verify that the voltage range and frequency of your power distribution matches to the power specification of the individual instrument. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. ➔...

  • Page 220: Do Not Operate In An Explosive Atmosphere

    Personal injury (for example electrical shock, intoxication) ➔ Instruments that appear damaged or defective should be made inoperative and secured against unintended operation until they can be repaired by qualified service personnel. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 221: Solvents

    For details, see the usage guideline for the solvent cabinet. A printed copy of the guideline N O T E has been shipped with the solvent cabinet, electronic copies are available in the Agilent Information Center or via the Internet. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 222: Safety Symbols

    European Community directives. The European Declaration of Conformity is available at: http://regulations.corporate.agilent.com/DoC/search.htm Manufacturing date. Power symbol indicates On/Off. The apparatus is not completely disconnected from the mains supply when the power switch is in the Off position InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 223 ➔ Do not proceed beyond a caution until you have fully understood and met the indicated conditions. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 224: Waste Electrical And Electronic Equipment (Wee) Directive

    Do not dispose of in domestic household waste N O T E To return unwanted products, contact your local Agilent office, or see http://www.agilent.com for more information. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 225: Radio Interference

    If test and measurement equipment is operated with unscreened cables, or used for measurements on open set-ups, the user has to assure that under operating conditions the radio interference limits are still met within the premises. InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 226: Sound Emission

    This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...

  • Page 227: Agilent Technologies On The Internet

    Appendix Agilent Technologies on the Internet Agilent Technologies on the Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 228 CAN partner DHCP motor-drive power general information overview overpressure 102, 106, 104, setup RS-232 pressure above upper limit dimensions InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 229 TCP/IP parameter configuration minimum using default motor-drive power frequency range using stored InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 230 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 231 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual...
  • Page 232 In This Book This manual contains technical reference information about the Agilent 1260 Infinity II Binary Pump G7112B. The manual describes the following: • introduction, • site requirements and specifications, • using the binary pump, • optimizing performance, • troubleshooting and diagnostics, •...

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