Teledyne Tekmar Versa User Manual page 6

chapter 4: Versa teklInk
To Upgrade Versa Firmware .................................................................................................4-14
Installing the DFU Driver .......................................................................................................4-14
Preferences .................................................................................................................................4-16
Export Feature ..........................................................................................................................4-17
chapter 5: 21 cfr part 11 complIance
21 cfr part 11 features and compliance tools ....................................................... 5-2
First Login ..................................................................................................................................... 5-2
Change Password ......................................................................................................................5-2
User Manager .............................................................................................................................. 5-3
Setting Up User Accounts .......................................................................................................5-3
Data Versioning, History, and Archive ................................................................................5-6
View/Print System History and Error Logs ........................................................................5-6
Change Justification .................................................................................................................5-8
chapter 6: method deVelopment
Optimization Steps for Static Headspace Analysis ........................................................6-2
Sample Equilibration ................................................................................................................6-4
Universal Gas Law Parameters ..............................................................................................6-5
Miscellaneous Settings ............................................................................................................6-6
Additional Headspace References .......................................................................................6-7
Versa User Manual
table of contents
tm
System Properties - Connection Tab .............................................................................................................. 4-13
If you are running Windows XP ........................................................................................................................ 4-14
If you are running Windows Vista or Windows 7 ........................................................................................ 4-15
Preferences - General Tab ................................................................................................................................... 4-16
Preferences - E-mail Tab ...................................................................................................................................... 4-16
Accounts Tab ..............................................................................................................................................................5-3
Connections Tab .......................................................................................................................................................5-3
General Tab .................................................................................................................................................................5-3
Permissions Tab ........................................................................................................................................................5-4
Edit an Existing Account Permissions ...............................................................................................................5-5
Lockout ........................................................................................................................................................................5-5
Sample Preparation .................................................................................................................................................6-2
Salting Out ..................................................................................................................................................................6-2
pH ..................................................................................................................................................................................6-2
Derivatization ............................................................................................................................................................6-3
Phase Ratio .................................................................................................................................................................6-3
Diffusion Characteristics of Solid Samples......................................................................................................6-3
Reverse Solvent Dilution .......................................................................................................................................6-3
Platen/Sample Temperature ................................................................................................................................6-4
Platen/Sample Time ................................................................................................................................................6-4
Mix Time ......................................................................................................................................................................6-4
Mix Power and Agitation Mechanism ...............................................................................................................6-4
Mix Equilibration ......................................................................................................................................................6-4
Pressure .......................................................................................................................................................................6-5
Vial Pressurization ....................................................................................................................................................6-5
Loop Fill Pressure .....................................................................................................................................................6-6
Loop Size .....................................................................................................................................................................6-6
Valve Oven Temperature .......................................................................................................................................6-6
GC Cycle Time ............................................................................................................................................................6-6
System Pressure and Standby Flow ...................................................................................................................6-7
Transfer Line Temperature ....................................................................................................................................6-7
Platen Equilibration Time ......................................................................................................................................6-7
Inject Time ..................................................................................................................................................................6-7
2G (cont.)
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