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Teledyne Tekmar Versa manual available for free PDF download: User Manual
Teledyne Tekmar Versa User Manual (103 pages)
Brand:
Teledyne
| Category:
Industrial Equipment
| Size: 9.38 MB
Table of Contents
Table of Contents
4
Chapter 1: Introduction
8
Essential Instructions
9
Warnings
10
Introduction
11
Static Headspace
11
Sample Equilibration
11
Mass Balance Equation
11
Partition Coefficient
12
Mass Balance Equation Restated
13
Sampling
13
Injection
14
System Specifications
14
Component Overview
15
Vials
16
Vial Cover (Optional)
16
Pressure Regulator
16
Pressure Transducer
16
Sample Loop
16
Sample Needle
17
Flow Restrictor
17
Carousel Tray
17
Gas Inlets and Outlets
17
Transfer Line
17
Pressure Sample Gas Inlet
17
Headspace Valves
18
Pressurization Valve
18
Vent Valve
18
Versa Heated Zones
18
Platen
18
Versa Mechanisms
19
Carousel Drive Assembly
19
Sample/Elevator Mixer Assembly
19
Electronic Connections
20
Power Entry Module
20
USB Connection
20
GC/IO Interface
20
Circuit Boards
20
Chapter 2: Installation
21
Pre-Installation
22
Operating Environment
22
Location Selection
22
Power Requirements
22
Gas Supply Requirements
22
Minimum Computer Requirements
23
Required Tools and Supplies for Installation
24
Unpacking the Versa
24
Installation
25
Making Electronic Connections
25
Power Cord
25
GC/IO Interface Cable
25
USB Interface Cable
25
Making Plumbing Connections
26
Pressurize Gas
26
Transfer Line Connections
26
Versa Teklink™2G Installation
27
Connecting to the Versa
33
USB Driver Installation
33
Selecting Your USB Connection
35
Chapter 3: Basic Operation Basic Operation
36
Sample Preparation
37
Seal Quality Factors
38
Prepare Vials for Sampling
39
Spiking a Vial
39
Spiking Prior to Capping
40
Spiking after Capping
40
Full Evaporation Technique
40
Mode Descriptions
42
Modes
42
Valves and Mechanisms
43
Chapter 4: Versa Teklink
44
Software Configuration
45
Selecting an Instrument
45
Configuring an Active Instrument
46
VOC Teklink TM 2G Icons and Menus
47
File Menu
47
View Menu
47
Mode Menu
48
Tools Menu
48
Method & Schedule Menus
49
Creating and Using Methods
49
Using the Method Editor
49
Updating an Active Method
49
Building and Editing Schedules
50
M.o.M. Builder
51
Schedule Editor
52
Updating an Active Schedule
52
Software Features
53
Diagnostics
53
Valves & Flows Tab
53
Autosampler Tab
53
Communications Tab
54
Benchmark
54
History Logs
54
System Properties
55
System Properties - E-Mail Tab
56
System Properties - Data Tab
56
System Properties - Connection Tab
56
To Upgrade Versa Firmware
57
Installing the DFU Driver
57
If You Are Running Windows XP
57
If You Are Running Windows Vista or Windows 7
58
Preferences
59
Preferences - General Tab
59
Preferences - E-Mail Tab
59
Export Feature
60
Chapter 5: 21 Cfr Part 11 Compliance
61
21 Cfr Part 11 Features and Compliance Tools
62
First Login
62
Change Password
62
User Manager
63
Accounts Tab
63
Connections Tab
63
Setting up User Accounts
63
General Tab
63
Permissions Tab
64
Edit an Existing Account Permissions
65
Lockout
65
Data Versioning, History, and Archive
66
View/Print System History and Error Logs
66
Change Justification
68
Chapter 6: Method Development
70
Optimization Steps for Static Headspace Analysis
71
Sample Preparation
71
Salting out
71
Derivatization
72
Phase Ratio
72
Diffusion Characteristics of Solid Samples
72
Reverse Solvent Dilution
72
Sample Equilibration
73
Platen/Sample Temperature
73
Platen/Sample Time
73
MIX Time
73
MIX Power and Agitation Mechanism
73
MIX Equilibration
73
Universal Gas Law Parameters
74
Pressure
74
Vial Pressurization
74
Loop Fill Pressure
75
Loop Size
75
Valve Oven Temperature
75
Miscellaneous Settings
75
GC Cycle Time
75
System Pressure and Standby Flow
76
Transfer Line Temperature
76
Platen Equilibration Time
76
Inject Time
76
Additional Headspace References
76
Chapter 7: Maintenance & Troubleshooting
77
Service Contact Information
78
Routine Procedures
78
Leak Check
78
To Upgrade Versa Firmware
79
Installing the DFU Driver
79
If You Are Running Windows XP
79
If You Are Running Windows Vista or Windows 7
80
Setting/Checking Versa System Pressure
81
Preventative Maintenance
81
Daily Maintenance Checks
81
Weekly Maintenance Checks
81
Monthly Maintenance Checks
82
Annual Maintenance Checks
82
Troubleshooting
83
System will Not Power up
84
Printed Circuit Boards
85
Temperature Control Board
85
Master Board
85
GCIO Board
85
Elevator Motor Board
85
Carousel Motor Board
86
24V DC Board
86
Pressure Transducer Board
86
General Troubleshooting
86
Low Response Loop
86
Heater Failures
87
How to Clean Carousel
87
How to Align the Sample/Elevator Mixer Assembly
89
Returning the Versa
89
Unit and Parts Disposal
89
Teledyne Tekmar Customer Support
89
Chapter 8: Diagrams
90
Detailed Plumbing
91
Standby/Ready, Sample Equilibrate, Mixing, and Stabilize
92
Raising Vial to Needle
93
Static Vial Pressure Reading
94
Pressurize
95
Pressure Equilibrate, Vial Pressure Reading
96
Loop Fill, Loop Fill Pressure Reading
97
Inject
98
Electrical Schematic
99
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