Teledyne Tekmar Versa Headspace Sampler Manuals

Teledyne Tekmar Versa Headspace Sampler Manuals

Manuals and User Guides for Teledyne Tekmar Versa Headspace Sampler. We have 1 Teledyne Tekmar Versa Headspace Sampler manual available for free PDF download: User Manual

Teledyne Tekmar Versa User Manual

Teledyne Tekmar Versa User Manual (103 pages)

Brand: Teledyne | Category: Industrial Equipment | Size: 9 MB

Table of Contents

Table of Contents
4
Chapter 1: Introduction

8
- Essential Instructions
  
  9
- Warnings
  
  10
- Introduction
  
  11
  - Static Headspace
    11
    
    Sample Equilibration
    11
    
    Mass Balance Equation
    11
    
    Partition Coefficient
    12
    
    Mass Balance Equation Restated
    13
    
    Sampling
    13
    
    Injection
    14
- System Specifications
  
  14
- Component Overview
  
  15
  - Vials
    16
  - Vial Cover (Optional)
    16
  - Pressure Regulator
    16
  - Pressure Transducer
    16
  - Sample Loop
    16
  - Sample Needle
    17
  - Flow Restrictor
    17
  - Carousel Tray
    17
  - Gas Inlets and Outlets
    17
    
    Transfer Line
    17
    
    Pressure Sample Gas Inlet
    17
  - Headspace Valves
    18
    
    Pressurization Valve
    18
    
    Vent Valve
    18
  - Versa Heated Zones
    18
    
    Platen
    18
  - Versa Mechanisms
    19
    
    Carousel Drive Assembly
    19
    
    Sample/Elevator Mixer Assembly
    19
  - Electronic Connections
    20
    
    Power Entry Module
    20
    
    USB Connection
    20
    
    GC/IO Interface
    20
  - Circuit Boards
    20
Chapter 2: Installation

21
- Pre-Installation
  
  22
  - Operating Environment
    22
  - Location Selection
    22
  - Power Requirements
    22
  - Gas Supply Requirements
    22
  - Minimum Computer Requirements
    23
  - Required Tools and Supplies for Installation
    24
  - Unpacking the Versa
    24
- Installation
  
  25
  - Making Electronic Connections
    25
    
    Power Cord
    25
    
    GC/IO Interface Cable
    25
    
    USB Interface Cable
    25
  - Making Plumbing Connections
    26
    
    Pressurize Gas
    26
    
    Transfer Line Connections
    26
- Versa Teklink™2G Installation
  
  27
- Connecting to the Versa
  
  33
  - USB Driver Installation
    33
  - Selecting Your USB Connection
    35
Chapter 3: Basic Operation Basic Operation

36
- Sample Preparation
  37
  - Seal Quality Factors
    38
  - Prepare Vials for Sampling
    39
  - Spiking a Vial
    39
  - Spiking Prior to Capping
    40
  - Spiking after Capping
    40
  - Full Evaporation Technique
    40
- Mode Descriptions
  
  42
  - Modes
    42
  - Valves and Mechanisms
    43
Chapter 4: Versa Teklink

44
- Software Configuration
  
  45
  - Selecting an Instrument
    45
  - Configuring an Active Instrument
    46
  - VOC Teklink TM 2G Icons and Menus
    47
    
    File Menu
    47
    
    View Menu
    47
    
    Mode Menu
    48
    
    Tools Menu
    48
  - Method & Schedule Menus
    49
    
    Creating and Using Methods
    49
    
    Using the Method Editor
    49
    
    Updating an Active Method
    49
    
    Building and Editing Schedules
    50
    
    M.o.M. Builder
    51
    
    Schedule Editor
    52
    
    Updating an Active Schedule
    52
  - Software Features
    53
    
    Diagnostics
    53
    
    Valves & Flows Tab
    53
    
    Autosampler Tab
    53
    
    Communications Tab
    54
    
    Benchmark
    54
    
    History Logs
    54
    
    System Properties
    55
    
    System Properties - E-Mail Tab
    56
    
    System Properties - Data Tab
    56
    
    System Properties - Connection Tab
    56
    
    To Upgrade Versa Firmware
    57
    
    Installing the DFU Driver
    57
    
    If You Are Running Windows XP
    57
    
    If You Are Running Windows Vista or Windows 7
    58
    
    Preferences
    59
    
    Preferences - General Tab
    59
    
    Preferences - E-Mail Tab
    59
    
    Export Feature
    60
Chapter 5: 21 Cfr Part 11 Compliance

61
- 21 Cfr Part 11 Features and Compliance Tools
  
  62
  - First Login
    62
  - Change Password
    62
  - User Manager
    63
    
    Accounts Tab
    63
    
    Connections Tab
    63
  - Setting up User Accounts
    63
    
    General Tab
    63
    
    Permissions Tab
    64
    
    Edit an Existing Account Permissions
    65
    
    Lockout
    65
  - Data Versioning, History, and Archive
    66
  - View/Print System History and Error Logs
    66
  - Change Justification
    68
Chapter 6: Method Development

70
- Optimization Steps for Static Headspace Analysis
  71
  - Sample Preparation
    71
  - Salting out
    71
  - Derivatization
    72
  - Phase Ratio
    72
  - Diffusion Characteristics of Solid Samples
    72
  - Reverse Solvent Dilution
    72
  - Sample Equilibration
    73
    
    Platen/Sample Temperature
    73
    
    Platen/Sample Time
    73
    
    MIX Time
    73
    
    MIX Power and Agitation Mechanism
    73
    
    MIX Equilibration
    73
  - Universal Gas Law Parameters
    74
    
    Pressure
    74
    
    Vial Pressurization
    74
    
    Loop Fill Pressure
    75
    
    Loop Size
    75
    
    Valve Oven Temperature
    75
  - Miscellaneous Settings
    75
    
    GC Cycle Time
    75
    
    System Pressure and Standby Flow
    76
    
    Transfer Line Temperature
    76
    
    Platen Equilibration Time
    76
    
    Inject Time
    76
  - Additional Headspace References
    76
Chapter 7: Maintenance & Troubleshooting

77
- Service Contact Information
  
  78
- Routine Procedures
  
  78
  - Leak Check
    78
  - To Upgrade Versa Firmware
    79
  - Installing the DFU Driver
    79
    
    If You Are Running Windows XP
    79
    
    If You Are Running Windows Vista or Windows 7
    80
  - Setting/Checking Versa System Pressure
    81
  - Preventative Maintenance
    81
    
    Daily Maintenance Checks
    81
    
    Weekly Maintenance Checks
    81
    
    Monthly Maintenance Checks
    82
    
    Annual Maintenance Checks
    82
- Troubleshooting
  
  83
  - System will Not Power up
    84
  - Printed Circuit Boards
    85
    
    Temperature Control Board
    85
    
    Master Board
    85
    
    GCIO Board
    85
    
    Elevator Motor Board
    85
    
    Carousel Motor Board
    86
    
    24V DC Board
    86
    
    Pressure Transducer Board
    86
  - General Troubleshooting
    86
    
    Low Response Loop
    86
    
    Heater Failures
    87
    
    How to Clean Carousel
    87
    
    How to Align the Sample/Elevator Mixer Assembly
    89
  - Returning the Versa
    89
  - Unit and Parts Disposal
    89
  - Teledyne Tekmar Customer Support
    89
Chapter 8: Diagrams

90
- Detailed Plumbing
  
  91
- Standby/Ready, Sample Equilibrate, Mixing, and Stabilize
  
  92
- Raising Vial to Needle
  
  93
- Static Vial Pressure Reading
  
  94
- Pressurize
  
  95
- Pressure Equilibrate, Vial Pressure Reading
  
  96
- Loop Fill, Loop Fill Pressure Reading
  
  97
- Inject
  
  98
- Electrical Schematic
  
  99

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