Chapter 3 Maintenance; Flow Cell Maintenance; Flushing The Flow Cell - Waters 996 Operator's Manual

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3
Maintenance
This chapter covers maintenance of the Waters 996 Photodiode Array Detector flow cell,
lamp, and fuse.
Caution:
To avoid the possibility of electric shock, do not remove the 996 detector power
supply covers. The power supply does not contain user-serviceable components.

3.1 Flow Cell Maintenance

The flow cell requires maintenance when:
• The reference spectrum changes.
• The Lamp diagnostic (in the Millennium
lamp status light is on (see
• The 996 detector causes high backpressure.
Note:
Conditions other than a dirty flow cell may cause decreased lamp intensity. For
more information, refer to
Flow cell maintenance consists of:

• Flushing the flow cell

• Removing the flow cell
• Cleaning the flow cell
• Installing the flow cell assembly
3.1.1 Flushing the Flow Cell
Required Materials
HPLC grade water
HPLC grade methanol
If the flow cell requires cleaning, the first cleaning method to try is flushing the flow cell
with solvent.
32
PDA Diagnostics window) fails, and the
Table
2-1).
Chapter 2, Diagnostics and
Calibration.
Flow Cell Maintenance
3
33

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