Waters 3100 Manuals

Manuals and User Guides for Waters 3100. We have 1 Waters 3100 manual available for free PDF download: Operator's Manual

Waters 3100 Operator's Manual (220 pages)

Brand: Waters | Category: Security Sensors | Size: 1.63 MB

Copyright Notice
2
Trademarks
2
Customer Comments
3
Safety Considerations
4
Considerations Specific to the 3100 Detector
4
Operating this Instrument
7
Applicable Symbols
7
Intended Use
7
Calibrating
7
Quality Control
8
ISM Classification
9
EC Authorized Representative
9
Table of Contents
11
Waters 3100 Detector
18
Overview
18
Overview
19
Waters 3100 Detector
20
Software and Data System
20
Ionization Techniques and Source Probes
21
Electrospray Ionization (ESI)
21
Combined ESI and APCI (Esci)
21
Atmospheric Pressure Chemical Ionization
22
Atmospheric Pressure Photoionization
22
Ion Optics
23
MS Operating Modes
24
Sample Inlet
24
Vacuum System
24
Rear Panel
24
Intellistart Fluidics System
26
Overview
26
System Operation
27
Preparing for Operation
30
Starting the Instrument
30
Configuring Intellistart
32
Verifying the Instrument's State of Readiness
32
Tuning and Calibration Information
32
Monitoring the Instrument Leds
33
Preparing the Intellistart Fluidics System
34
Installing the Solvent Manifold Drip Tray
34
Installing the Reservoir Bottles
35
Diverter Valve Positions
36
Purging the Infusion Syringe
39
Rebooting the Instrument
39
Rebooting the Instrument by Pressing the Reset Button
39
Leaving the Mass Spectrometer Ready for Operation
40
Emergency Instrument Shutdown
40
ESI and Esci Modes of Operation
42
Introduction
42
Installing the ESI Probe
42
Installing the Corona Pin
46
Optimizing the ESI Probe for Esci Operation
48
Removing the Corona Pin
48
Removing the ESI Probe
50
Optional APCI Mode of Operation
54
Atmospheric Pressure Chemical Ionization
54
Ionsabre APCI Probe
54
Installing the Ionsabre APCI Probe
55
Installing the Corona Pin
58
Removing the Corona Pin
58
Removing the Ionsabre APCI Probe
59
Maintenance Procedures
61
Maintenance Schedule
63
Spare Parts
65
Safety and Handling
65
Preparing the Instrument for Work Performed on the Source
66
Operating the Source Isolation Valve
67
Removing O-Rings and Seals
69
Cleaning the Instrument's Exterior
70
Emptying the Exhaust Trap Bottle
70
Emptying the Roughing Pump Exhaust Liquid Trap Bottle
72
Gas Ballasting the Roughing Pump
74
Gas Ballasting a Pump Fitted with a Screwdriver-Operated Gas Ballast Valve
75
Gas Ballasting a Pump Fitted with a Handle-Operated Gas Ballast Valve
76
Checking the Roughing Pump Oil Level
77
Adding Oil to the Roughing Pump
77
Cleaning the Source Components
79
Cleaning the Sample Cone and Gas Cone
79
Removing the Cone Gas Assembly from the Source
79
Disassembling the Cone Gas Assembly
82
Cleaning the Sample Cone and Gas Cone
83
Assembling the Cone Gas Assembly
86
Fitting the Cone Gas Assembly to the Source
87
Cleaning the Ion Block, Isolation Valve, and Extraction Cone
89
Removing the Ion Block Assembly from the Source Assembly
89
Disassembling the Source Ion Block Assembly
91
Cleaning the Ion Block, Isolation Valve, and Extraction Cone
98
Assembling the Source Ion Block Assembly
100
Fitting the Ion Block Assembly to the Source Assembly
103
Cleaning the Source Hexapole Assembly
105
Removing the Ion Block Assembly, Ion Block Support, and Hexapole from the Source Assembly
105
Cleaning the Hexapole Assembly
107
Fitting the Hexapole Assembly, PEEK Ion Block Support, and Ion Block Assembly to the Source Assembly
110
Replacing the ESI Probe Tip
112
Replacing the ESI Probe Sample Capillary
113
Cleaning the Ionsabre APCI Probe Tip
120
Replacing the Ionsabre APCI Probe Sample Capillary
120
Removing the Existing Capillary
120
Installing the New Capillary
125
Cleaning or Replacing the Corona Pin
129
Replacing the APCI Probe Heater
130
Replacing the Ion Block Source Heater
132
Replacing the Source Assembly Seals
136
Removing the Source Enclosure from the Instrument
136
Disassembling the Source Enclosure and Probe Adjuster Assembly
139
Removing the Seals from the Source Enclosure and Probe Adjuster Assembly
140
Fitting the New Source Enclosure and Probe Adjuster Assembly Seals
143
Assembling the Probe Adjuster Assembly and Source Enclosure
144
Fitting the Source Enclosure to the Instrument
145
Maintaining the Instrument Air Filters
147
Cleaning the Air Filter Inside the Instrument's Lower Bezel
147
Replacing the Air Filter Inside the Lower Bezel
148
Cleaning the Air Filter Behind the Source Probe
149
Fit the Probe to the Source
150
Replacing the Air Filter Behind the Source Probe
151
Replacing the Roughing Pump Oil
152
If You Are Fitting an ESI Probe, See "Installing the ESI Probe" on Page
152
If You Are Fitting an Ionsabre APCI Probe, See "Installing the Ionsabre APCI Probe" on Page
152
Start the Instrument (See "Starting the Instrument
154
Replacing the Roughing Pump's Oil Demister Element
155
A Safety Advisories
162
Warning Symbols
162
Task-Specific Hazard Warnings
162
Specific Warnings
163
Caution Symbol
165
Warnings that Apply to All Waters Instruments
165
Electrical and Handling Symbols
171
Electrical Symbols
171
Handling Symbols
172
B External Connections
174
External Wiring and Vacuum Connections
174
Connecting the Oil-Filled Roughing Pump
175
Making the Electrical Connections for a Roughing Pump with an External Relay Box
180
Making the Electrical Connections for a Roughing Pump Without an External Relay Box
181
Connecting the Oil-Free Roughing Pump
182
Making the Electrical Connections for an Oil-Free Roughing Pump
189
Connecting to the Nitrogen Gas Supply
190
Connecting the Nitrogen Exhaust Line
192
Connecting the Liquid Waste Line
195
Connecting the Workstation
197
Connecting Ethernet Cables
198
I/O Signal Connectors
198
Signal Connections
200
Connecting to the Electricity Source
203
C Materials of Construction and Compliant Solvents
206
Preventing Contamination
206
Items Exposed to Solvent
206
Solvents Used to Prepare Mobile Phases
207
Assembling Required Materials
210
Preparing the Sulfadimethoxine Standard
210
Storing the Solutions
211
Using the Solution in an LC/MS System Check Run
211
Index
213

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